公开(公告)号：US20160357200A1

公开(公告)日：2016-12-08

申请号：US14732916

申请日：2015-06-08

Applicant: SHIMADZU CORPORATION

Inventor： Michiaki OWA

IPC: G05D23/19 ,  B01D1/00 ,  H05B1/02

CPC classification number: H05B1/0247 ,  G05D23/1919

Abstract: When a solid product of a target component is obtained by heating a container in which a solution containing a target component is housed with a heater and evaporating the solvent in the solution, the amount of heating by the heater is controlled based on the detection results of the temperature of the container detected by a temperature detection part so that the temperature of the container approaches a target temperature. At least one of a starting timing T2 and an ending timing T4 is then discriminated based on the amount of heating by the heater. Since the amount of heating by the heater varies while being sensitively affected by the vaporization heat generated when the solvent evaporates, the starting timing T2 or the ending timing T4 can be accurately discriminated by using the amount of heating by the heater as a discrimination criterion.

Abstract translation: 当通过加热含有目标成分的溶液的容器中加热器并蒸发溶液中的溶剂来获得目标成分的固体产物时，基于加热器的检测结果来控制加热器的加热量 由温度检测部检测到的容器的温度，使得容器的温度接近目标温度。 然后基于加热器的加热量来判别启动时刻T2和结束时刻T4中的至少一个。 由于加热器的加热量在溶剂蒸发时产生的汽化热敏感地受到影响的同时发生变化，所以可以通过利用加热器的加热量作为判别标准来准确地识别启动时刻T2或结束时刻T4。

公开(公告)号：US20220229023A1

公开(公告)日：2022-07-21

申请号：US17616657

申请日：2019-06-11

Applicant: SHIMADZU CORPORATION

Inventor： Michiaki OWA

IPC: G01N30/28

Abstract: A supercritical fluid apparatus includes a solvent supplier that supplies a solvent, a pressure control device provided in a flow path for a solvent supplied by the solvent supplier, and a controller that controls the pressure control device. The controller includes a first controller that increases a pressure in the flow path, puts the solvent in a supercritical fluid state and maintains an environment for execution of a predetermined process by controlling the pressure control device, and a second controller that sets an intermediate target value for a pressure in the flow path and controls a pressure in the flow path in order to get the pressure to reach the intermediate target value, when ending the environment for execution of a predetermined process.

公开(公告)号：US20160064445A1

公开(公告)日：2016-03-03

申请号：US14474391

申请日：2014-09-02

Applicant: SHIMADZU CORPORATION

Inventor： Michiaki OWA

IPC: H01L27/146

CPC classification number: H01L27/14601 ,  G01J3/2803

Abstract: A photodiode array detector used for detecting light which has undergone wavelength separation by a spectroscopic element, the photodiode array detector including: a light receiving element array wherein, taking a plurality of light receiving elements which detect light of the same wavelength range as one unit, a plurality of such units are arrayed in the direction of dispersion of said wavelength; and a charge accumulation time setting unit which sets different charge accumulation times for the plurality of light receiving elements within the one unit.

Abstract translation: 一种用于检测由分光元件进行波长分离的光的光电二极管阵列检测器，所述光电二极管阵列检测器包括：受光元件阵列，其中，取多个光检测与一个单位相同波长范围的光的光接收元件， 多个这样的单元沿所述波长的分散方向排列; 以及电荷累积时间设定单元，其对于一个单位内的多个光接收元件设定不同的电荷累积时间。

公开(公告)号：US20220137007A1

公开(公告)日：2022-05-05

申请号：US17433261

申请日：2019-03-06

Applicant: SHIMADZU CORPORATION

Inventor： Michiaki OWA

IPC: G01N30/20 ,  G01N30/06

Abstract: A preparative chromatograph system includes a sample injector (10) that injects a sample into a separation flow path (8) through which a mobile phase flows, a separation column (12) that is provided on the separation flow path (8) and is to separate a sample injected into the separation flow path (8) into components, a detector (14) that is provided at a position farther downstream than the separation column (12) on the separation flow path (8) and is to detect sample components obtained by separation in the separation column (12), a collector (18, 18′) having a plurality of collection containers (22) for collecting part of an eluate eluted from the separation column (12) and a switch mechanism (20, 30, 32) configured to be capable of selectively connecting a downstream end of the separation flow path (8) to any one of the collection containers (22), a collection setter (26) configured to set a portion, to be collected in each of the collection containers (22), of an eluate eluted from the separation column (12) using a pre-acquired chromatogram of a sample, and a collection setter (26) configured to be capable of setting a portion, including a sample component, of an eluate eluted from the separation column (12), and a portion, between two sample components that are adjacent to each other on the chromatogram, of an eluate eluted from the separation column (12), as the portion to be collected, and a controller (28) configured to control an operation of the switch mechanism (20, 30, 32) of the collector (18, 18′) and collect the portion, which is to be collected and is set by the connection setter (26), in the predetermined collection container (22).

公开(公告)号：US20160061662A1

公开(公告)日：2016-03-03

申请号：US14474986

申请日：2014-09-02

Applicant: SHIMADZU CORPORATION

Inventor： Michiaki OWA

IPC: G01J3/42 ,  G01J3/02

CPC classification number: G01J3/42 ,  G01J3/02 ,  G01J3/027 ,  G01J3/28

Abstract: A stray light ratio computation unit computes the stray light ratio at a specified wavelength based on the quantity of light at the specified wavelength computed by light quantity computation unit in a state where there is no sample having absorption in the light path and the quantity of light at the specified wavelength computed by light quantity computation unit when the light is transmitted through a sample having absorption at the specified wavelength. Stray light quantity computation unit computes the quantity of stray light at each wavelength through computations using the stray light ratio at the specified wavelength and different unique values for each wavelength (for example, different coefficients for each wavelength, stored in coefficient storage unit).

Abstract translation: 杂散光比计算单元基于在光路中没有吸收样品的状态下的光量计算单元计算的指定波长处的光量和光量来计算指定波长处的杂散光比 当光通过具有指定波长的吸收的样品透射时，由光量计算单元计算出的指定波长。 杂散光量计算单元通过使用指定波长的杂散光比和每个波长的不同唯一值（例如，存储在系数存储单元中的每个波长的不同系数）通过计算来计算每个波长的杂散光量。

公开(公告)号：US20140063496A1

公开(公告)日：2014-03-06

申请号：US14011982

申请日：2013-08-28

Applicant: SHIMADZU CORPORATION

Inventor： Michiaki OWA

IPC: G01J3/02

CPC classification number: G01J3/0286

Abstract: Provided is a spectrophotometer capable of further reducing a change in temperature of a spectroscopic unit that houses a spectroscopic element, a sample, and the like therein, compared with conventional spectrophotometers. A spectrophotometer 1 includes: a light source chamber 10; a spectroscopic chamber 20 separated from the light source chamber 10 with a heat insulating section located therebetween, the spectroscopic chamber 20 including at least a spectroscopic element 24, a sample chamber 22, and a detector 25; a temperature measurer 40 measuring a temperature inside of the spectroscopic chamber 20; a temperature regulator 50 heating and/or cooling the inside of the spectroscopic chamber 20; and a controller 31 acquiring temperature information from the temperature measurer 40 and controlling the temperature regulator 50 to operate so as to keep the inside of the spectroscopic chamber 20 at a predetermined preset temperature.

Abstract translation: 本发明提供一种分光光度计，其与传统的分光光度计相比能够进一步降低容纳分光元件，样品等的分光单元的温度变化。 分光光度计1包括：光源室10; 分离室20与光源室10分离，隔热部分位于它们之间，分光室20至少包括分光元件24，样品室22和检测器25; 测量分光室20内的温度的温度测量器40; 温度调节器50加热和/或冷却分光室20的内部; 以及控制器31，从温度测量器40获取温度信息，并控制温度调节器50的操作，以使分光室20的内部保持在预定的预设温度。

公开(公告)号：US20210025856A1

公开(公告)日：2021-01-28

申请号：US16968855

申请日：2018-09-13

Applicant: SHIMADZU CORPORATION

Inventor： Michiaki OWA

IPC: G01N30/54 ,  B01D11/02

Abstract: A supercritical fluid separation apparatus performs feedback control of output of a heater so that a separation part temperature becomes a set temperature, based on both output of a first temperature sensor that measures a heating block temperature and output of a second temperature sensor that measures the separation part temperature. When a difference between the separation part temperature and the set temperature is large (equal to or more than a predetermined value), output of the heater is adjusted based on the heating block temperature. When a difference between the separation part temperature and the set temperature becomes small (less than a predetermined value), the output of the heater is adjusted based on the difference.

公开(公告)号：US20190078697A1

公开(公告)日：2019-03-14

申请号：US16072921

申请日：2016-01-27

Applicant: SHIMADZU CORPORATION

Inventor： Chihiro KORA ,  Takao OKADO ,  Michiaki OWA ,  Yosuke IWATA

IPC: F16K25/00 ,  G01N30/32 ,  G01N30/20 ,  B01D15/40

Abstract: A pressure control valve is provided with a pressure control block. The pressure control block has a pressure control block having an opening portion provided on one outer surface, a pressure control surface provided as a plane at a bottom portion of the opening portion, and two internal channels having openings at the respective end portions of the pressure control surface. A sheet-like valve body having elasticity and arranged so as to cover the pressure control surface is provided in the opening portion of the pressure control block. A valve body driving portion is provided on a side opposite to the pressure control surface with the valve body interposed therebetween that adjusts an amount of a gap between the valve body and the pressure control surface by pressing the valve body in a direction perpendicular to the pressure control surface. The pressure control surface has higher hardness than a hard material.