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    Process for dyeing polyolefin fiber materials
    1.
    发明授权
    Process for dyeing polyolefin fiber materials 失效
    聚烯烃纤维材料染色工艺

    公开(公告)号：US4411666A

    公开(公告)日：1983-10-25

    申请号：US346537

    申请日：1982-02-08

    申请人： Shuhei Hashizume ,  Sadaharu Abeta ,  Tadayuki Ohmae ,  Hajime Nishibara

    发明人： Shuhei Hashizume ,  Sadaharu Abeta ,  Tadayuki Ohmae ,  Hajime Nishibara

    IPC分类号： D06P1/653 ,  D06P3/79 ,  D06P3/82 ,  D06P5/12 ,  D06P1/39 ,  D06P3/85

    CPC分类号： D06P1/653 ,  D06P3/791 ,  D06P3/8204 ,  D06P5/12

    摘要： A process for dyeing polyolefin fiber materials, which comprises contacting a polyolefin fiber material obtained by melt-spinning a mixture of crystalline polyolefin and 0.1 to 30% by weight based on the weight of the polyolefin of a copolymer of ethylene and an aminoalkyl acrylate compound represented by the formula, ##STR1## wherein R.sub.1 represents hydrogen atom or methyl group, R.sub.2 and R.sub.3 each represents hydrogen atom or an alkyl group having 1 to 4 carbon atoms, and n represents an integer from 1 to 4, or a blend product of the said polyolefin fiber material and a polyamide fiber material, with a dye bath containing an anionic dye and at least one carboxylic acid selected from the group consisting of benzoic acid, salicylic acid, p-chlorobenzoic acid and 5-chlorosalicylic acid.

    摘要翻译： 一种用于染色聚烯烃纤维材料的方法，其包括将通过将结晶聚烯烃的混合物熔融纺丝而获得的聚烯烃纤维材料与基于乙烯和丙烯酸氨基烷基酯化合物的共聚物的聚烯烃的重量为0.1-30重量％ 式中，R 1表示氢原子或甲基，R 2和R 3各自表示氢原子或碳原子数1〜4的烷基，n表示1〜4的整数，或者 所述聚烯烃纤维材料和聚酰胺纤维材料，其中含有阴离子染料和至少一种选自苯甲酸，水杨酸，对氯苯甲酸和5-氯水杨酸的羧酸的染浴。

    Compositions containing benzodifuranone compounds and methods for dyeing hydrophobic materials using the same
    4.
    发明授权
    Compositions containing benzodifuranone compounds and methods for dyeing hydrophobic materials using the same 失效
    含有苯并呋喃酮化合物的组合物和使用其的疏水性材料的染色方法

    公开(公告)号：US5547478A

    公开(公告)日：1996-08-20

    申请号：US167019

    申请日：1993-12-16

    申请人： Toshinori Fukui ,  Nobuyuki Katsuda ,  Shinichi Yabushita ,  Shuhei Hashizume

    发明人： Toshinori Fukui ,  Nobuyuki Katsuda ,  Shinichi Yabushita ,  Shuhei Hashizume

    IPC分类号： C09B67/22 ,  D06P3/52 ,  D06P1/20 ,  C07D493/04

    CPC分类号： C09B67/0033 ,  Y10S8/922

    摘要： The invention is to provide a composition made by blending a benzodifuranone compound of the formula (I): ##STR1## wherein R.sub.1 represents a methylene or straight or branched C.sub.2 -C.sub.6 alkylene group optionally substituted with a hydroxy, C.sub.1 -C.sub.4 alkoxy or C.sub.1 -C.sub.4 alkylcarbonyloxy group; and Q represents 5- or 6-membered saturated or unsaturated heterocyclic ring residue, with an anthraquinone compound of the formula (II): ##STR2## wherein R.sub.2 represents an optionally substituted C.sub.1 -C.sub.6 alkyl, optionally substituted phenyl or C.sub.1 -C.sub.4 alkoxyphenylsulfonyl group, and a method for dyeing hydrophobic materials using the composition to obtain red dyed products with excellent pH dependency and fastnesses to light and washing.

    摘要翻译： 本发明提供通过将式（I）的苯并二呋喃酮化合物：其中R 1表示任选被羟基，C 1 -C 4烷氧基或C 1 -C 4烷氧基取代的亚甲基或直链或支链C 2 -C 6亚烷基 -C 1-4烷基羰氧基 和Q表示5-或6-元饱和或不饱和杂环残基，与式（II）的蒽醌化合物反应：其中R 2表示任选取代的C 1 -C 6烷基，任选取代的苯基或C 1 -C 4烷氧基苯磺酰基 以及使用该组合物染色疏水性材料的方法，以获得具有优异的pH依赖性和耐光性和洗涤性的红染色产品。

    Trichromatic fiber reactive dye composition and method for dyeing or printing fiber materials using the composition
    6.
    发明授权
    Trichromatic fiber reactive dye composition and method for dyeing or printing fiber materials using the composition 失效
    三色纤维活性染料组合物和使用该组合物染色或印花纤维材料的方法

    公开(公告)号：US5254136A

    公开(公告)日：1993-10-19

    申请号：US921702

    申请日：1992-07-30

    申请人： Miwako Fujii ,  Naoki Harada ,  Shuhei Hashizume

    发明人： Miwako Fujii ,  Naoki Harada ,  Shuhei Hashizume

    IPC分类号： C09B62/503 ,  C09B62/505 ,  C09B62/51 ,  C09B67/22 ,  D06P1/38 ,  D06P3/60 ,  D06P3/66 ,  C09B62/04 ,  C09B62/20 ,  C09B62/343

    CPC分类号： C09B67/0041 ,  C09B67/0042 ,  C09B67/0052 ,  Y10S8/918

    摘要： Provided is a fiber reactive dye composition which can dye or print cellulose based fiber materials or materials containing the fiber materials uniformly with good build-up property and reproducibility and give dyed or printed products excellent in various fastness properties.A fiber reactive dye composition which comprises at least five reactive dyes selected from the groups of reactive dyes represented by the following formulas (I) to (VII) respectively in the form of free acid: ##STR1## wherein R.sub.1 and R.sub.2 are each hydrogen, alkyl, ureido or the like, R.sub.5 and R.sub.6 are each hydrogen, sulfo or the like, R.sub.3, R.sub.4, R.sub.7 to R.sub.13 and R.sub.15 to R.sub.18 are each hydrogen, alkyl or the like, R.sub.14 is --O-- or ##STR2## A, B, D, E, G, J and L are each phenylene or the like, X.sub.1 to X.sub.6 are each halogen, Y.sub.1 to Y.sub.7 are each --SO.sub.2 CH.dbd.CH.sub.2 or --SO.sub.2 C.sub.2 H.sub.4 Z, Z being a group capable of being split off by the action of an alkali, m.sub.1 to m.sub.4 are each an integer of 1-3, and n is 0 or 1, provided that the composition contains respectively at least one yellow dye selected from those of the formulas (I) and (II), red dye selected from those of the formulas (III) and (IV) and blue dye selected from those of the formulas (V) to (VII).

    Reactive dye composition and a method for dyeing or printing of fiber materials using the same
    7.
    发明授权
    Reactive dye composition and a method for dyeing or printing of fiber materials using the same 失效
    活性染料组合物和使用其的纤维材料的染色或印花方法

    公开(公告)号：US5536277A

    公开(公告)日：1996-07-16

    申请号：US361498

    申请日：1994-12-22

    申请人： Mitsuo Shimode ,  Nobuaki Kawamura ,  Shinichi Yabushita ,  Shuhei Hashizume

    发明人： Mitsuo Shimode ,  Nobuaki Kawamura ,  Shinichi Yabushita ,  Shuhei Hashizume

    IPC分类号： C09B67/22 ,  C09B62/505

    CPC分类号： C09B67/0038

    摘要： A reactive dye composition which contains a dye mixture comprising; at least one reactive dye selected from dyes represented by the following formula (I): ##STR1## in which Q is --SO.sub.2 CH.sub.2 CH.sub.2 Z in which Z is a group splittable by the action of alkali or --SO.sub.2 CH.dbd.CH.sub.2, and M.sup.1 is hydrogen, an alkali metal or an alkaline earth metal, and at least one anthraquinone compound usable as an acid dye; and a process for dyeing or printing a fiber material using the reactive dye composition.

    摘要翻译： 一种活性染料组合物，其含有染料混合物， 选自由下式（I）表示的染料中的至少一种活性染料：其中Q是-SO 2 CH 2 CH 2 Z，其中Z是可以通过碱或-SO 2 CH = CH 2的作用分裂的基团，M1是 氢，碱金属或碱土金属和至少一种可用作酸性染料的蒽醌化合物; 以及使用活性染料组合物染色或印刷纤维材料的方法。

    Reactive dye composition and method for dyeing or printing cellulose fiber material using the same
    8.
    发明授权
    Reactive dye composition and method for dyeing or printing cellulose fiber material using the same 失效
    活性染料组合物和使用其的染色或印花纤维素纤维材料的方法

    公开(公告)号：US5456726A

    公开(公告)日：1995-10-10

    申请号：US230003

    申请日：1994-04-19

    申请人： Shigeru Kawabata ,  Naoki Harada ,  Shuhei Hashizume

    发明人： Shigeru Kawabata ,  Naoki Harada ,  Shuhei Hashizume

    IPC分类号： C09B62/44 ,  C09B62/503 ,  C09B67/22 ,  D06P1/38

    CPC分类号： C09B62/4401 ,  C09B62/503 ,  C09B67/004

    摘要： A reactive dye composition containing at least one dioxazine compound of the formula (I) in the free acid form: ##STR1## wherein R.sub.1, R.sub.2, R.sub.3, Z.sub.1, m, Y.sub.1, Z.sub.1, Q.sub.1 and Q.sub.2 are as defined in the claims, or at least one dioxazine compound of the formula (II) in the free acid form: ##STR2## wherein R.sub.8, R.sub.9, R.sub.10, X.sub.2, n, Y.sub.2, Z.sub.2, Z.sub.3 and Q.sub.3 are as defined in the claims, or a mixture of at least one dioxazine compound of the formula (I) and at least one dioxazine compound of the formula (II); and at least one anthraquinone compound of the formula (III) in the free acid form: ##STR3## wherein Z.sub.4 is as defined in the claims; can dye a cellulose fiber material or a fiber material containing cellulose fiber uniformly blue, with a small amount of salt, with a good build-up property, in a high reproducibility.

    摘要翻译： 含有游离酸形式的至少一种式（I）的二恶嗪化合物的活性染料组合物：其中R1，R2，R3，Z1，m，Y1，Z1，Q1和 Q2如权利要求中所定义，或至少一种游离酸形式的式（II）的二恶嗪化合物：其中R8，R9，R10，X2，n，Y2， Z2，Z3和Q3如权利要求中所定义，或至少一种式（I）的二恶嗪化合物与至少一种式（II）的二恶嗪化合物的混合物; 和至少一种游离酸形式的式（III）的蒽醌化合物：其中Z4如权利要求中所定义; 可以以高再现性将纤维素纤维材料或含有纤维素纤维的纤维素纤维以少量的盐均匀地染色，具有良好的聚集性能。

    Reactive dye composition and dyeing or printing process using the same
    10.
    发明授权
    Reactive dye composition and dyeing or printing process using the same 失效
    活性染料组合物和染色或印刷方法使用相同

    公开(公告)号：US5324329A

    公开(公告)日：1994-06-28

    申请号：US76962

    申请日：1993-06-16

    申请人： Takeshi Washimi ,  Naoki Harada ,  Shuhei Hashizume ,  Takashi Omura

    发明人： Takeshi Washimi ,  Naoki Harada ,  Shuhei Hashizume ,  Takashi Omura

    IPC分类号： C09B67/24 ,  C09B62/44 ,  C09B67/22 ,  D06P1/384 ,  D06P3/66 ,  C09B62/00

    CPC分类号： C09B67/0052 ,  C09B62/4413 ,  Y10S8/918

    摘要： A reactive dye composition containing at least one dye of the formula (I) in the free acid form: ##STR1## wherein m is zero or 1; R.sub.1 is hydrogen, lower alkyl or lower alkoxy; R.sub.2 and R.sub.3 are independently hydrogen or substituted or unsubstituted lower alkyl; A is substituted or unsubstituted phenylene or naphthylene; X.sub.1 is halogen, --N(R.sub.4)R.sub.5 or --OR.sub.6 in which R.sub.4, R.sub.5 and R.sub.6 are independently hydrogen or substituted or unsubstituted alkyl, phenyl or naphthyl; and Y.sub.1 is the group --SO.sub.2 CH.dbd.CH.sub.2 or the group --SO.sub.2 CH.sub.2 CH.sub.2 Z.sub.1 in which Z.sub.1 is a group splittable by the action of an alkali, and at least one dye of the formula (II) in the free acid form: ##STR2## wherein n is zero, 1 or 2; one of W.sub.1 and W.sub.2 is hydrogen and the other is sulfo; R.sub.7 is hydrogen or substituted or unsubstituted lower alkyl; B is substituted or unsubstituted phenylene or naphthylene; X.sub.2 is --N(R.sub.8)R.sub.9, --OR.sub.10 in which R.sub.8, R.sub.9 and R.sub.10 are independently hydrogen or substituted or unsubstituted alkyl, phenyl, naphthyl, pyridinio, morpholino or piperidino; and Y.sub.2 is the group --SO.sub.2 CH.dbd.CH.sub.2 or the group --SO.sub.2 CH.sub.2 CH.sub.2 Z.sub.2 in which Z.sub.2 is a group splittable by the action of an alkali, dyes or prints cellulose fiber materials or fiber materials containing a cellulose fiber to give a vivid, deep and highly fast red color.

    摘要翻译： 含有游离酸形式的至少一种式（I）染料的活性染料组合物：其中m为0或1; R1是氢，低级烷基或低级烷氧基; R2和R3独立地为氢或取代或未取代的低级烷基; A是取代或未取代的亚苯基或亚萘基; X 1是卤素，-N（R 4）R 5或-OR 6，其中R 4，R 5和R 6独立地是氢或取代或未取代的烷基，苯基或萘基; Y1是基团-SO2CH = CH2或基团-SO2CH2CH2Z1，其中Z1是可以通过碱作用而分裂的基团，以及至少一种游离酸形式的式（II）染料：II ）其中n为0,1或2; W1和W2之一是氢，另一个是磺基; R7是氢或取代或未取代的低级烷基; B是取代或未取代的亚苯基或亚萘基; X 2是-N（R 8）R 9，-OR 10，其中R 8，R 9和R 10独立地是氢或取代或未取代的烷基，苯基，萘基，吡啶基，吗啉代或哌啶子基; 并且Y2是基团-SO 2 CH = CH 2或基团-SO 2 CH 2 CH 2 Z 2，其中Z 2是可以通过碱的作用而分裂的基团，染料或印刷含纤维素纤维的纤维素纤维材料或纤维材料，以产生生动，深度和高度快速 红色。