公开(公告)号：US06761803B2

公开(公告)日：2004-07-13

申请号：US10023418

申请日：2001-12-17

申请人： Shuit-Tong Lee ,  Igor Bello ,  Chun-Sing Lee ,  Quan Li ,  Naigui Shang

发明人： Shuit-Tong Lee ,  Igor Bello ,  Chun-Sing Lee ,  Quan Li ,  Naigui Shang

IPC分类号： C23C1434

CPC分类号： H01J9/025 ,  H01J2237/3151

摘要： A method and an apparatus have been developed to fabricate large area uniform silicon cone arrays using different kinds of ion-beam sputtering methods. The apparatus includes silicon substrate as the silicon source, and metal foils are used as catalyst. Methods of surface modification of the as-synthesized silicon cones for field emission application have also been developed, including hydrofluoric acid etching, annealing and low work-function metal coating. Nano-structure modification based on silicon cones takes advantage of the fact that the cone tip consists of metal/metal siliside, which can be used as catalyst and template for nanowires growth. A method and an apparatus have been developed to grow silicon oxide/silicon nanowires on tips of the silicon cones.

摘要翻译： 已经开发了使用不同种类的离子束溅射方法制造大面积均匀硅锥阵列的方法和装置。 该装置包括作为硅源的硅衬底，并且使用金属箔作为催化剂。 还开发了用于场致发射应用的合成硅锥体的表面改性方法，包括氢氟酸蚀刻，退火和低功函数金属涂层。 基于硅锥的纳米结构改性利用了锥尖由金属/金属硅化物组成的事实，其可以用作纳米线生长的催化剂和模板。 已经开发了一种在硅锥顶端生长氧化硅/硅纳米线的方法和装置。

公开(公告)号：US09139439B2

公开(公告)日：2015-09-22

申请号：US14002399

申请日：2012-03-01

申请人： Pagona Papakonstantinou ,  Naigui Shang

发明人： Pagona Papakonstantinou ,  Naigui Shang

IPC分类号： C01B31/04 ,  B82Y30/00 ,  B82Y40/00

CPC分类号： C01B31/0469 ,  B82Y30/00 ,  B82Y40/00 ,  C01B32/182 ,  C01B32/19 ,  C01B2204/04 ,  C01B2204/22 ,  C01B2204/30 ,  C01B2204/32 ,  Y10S977/734 ,  Y10S977/842 ,  Y10T428/2982

摘要： The present invention provides a process for the preparation of graphene or graphene-like fragments of another layered structure, said process comprising the step of mixing and grinding graphite or said other layered structure with at least one ionic liquid. The invention also provides the use of grinding in ionic liquids in such a process and products formed or formable by such methods.

摘要翻译： 本发明提供了制备另一层状结构的石墨烯或类似石墨烯片段的方法，所述方法包括用至少一种离子液体混合和研磨石墨或所述其它层状结构的步骤。 本发明还提供了在这种方法中的离子液体中研磨的用途以及通过这些方法形成或可形成的产品。

公开(公告)号：US20140044968A1

公开(公告)日：2014-02-13

申请号：US14002399

申请日：2012-03-01

申请人： Pagona Papakonstantinou ,  Naigui Shang

发明人： Pagona Papakonstantinou ,  Naigui Shang

IPC分类号： C01B31/04

CPC分类号： C01B31/0469 ,  B82Y30/00 ,  B82Y40/00 ,  C01B32/182 ,  C01B32/19 ,  C01B2204/04 ,  C01B2204/22 ,  C01B2204/30 ,  C01B2204/32 ,  Y10S977/734 ,  Y10S977/842 ,  Y10T428/2982

摘要： The present invention provides a process for the preparation of graphene or graphene-like fragments of another layered structure, said process comprising the step of mixing and grinding graphite or said other layered structure with at least one ionic liquid. The invention also provides the use of grinding in ionic liquids in such a process and products formed or formable by such methods.

摘要翻译： 本发明提供了制备另一层状结构的石墨烯或类似石墨烯片段的方法，所述方法包括用至少一种离子液体混合和研磨石墨或所述其它层状结构的步骤。 本发明还提供了在这种方法中的离子液体中研磨的用途以及通过这些方法形成或可形成的产品。