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公开(公告)号：US07842131B2
公开(公告)日：2010-11-30
申请号：US11668629
申请日：2007-01-30
CPC分类号： C09C1/3661 , C01P2006/12 , Y10T428/24372 , Y10T428/2438 , Y10T428/24388 , Y10T428/2991 , Y10T428/2993
摘要： The invention relates to a rutile titanium dioxide pigment for use in decorative laminating papers that yields higher opacity of the papers compared to the prior art, as well as a method for its manufacture. The pigment displays a surface coating that contains aluminum phosphate, aluminum oxide, silicon oxide and titanium oxide. The silicon oxide is precipitated in fluffy form. The coated particles display a BET value of at least 15 m2/g.The manufacturing method is characterized in that an aluminum and a phosphorus component are first added to a TiO2 suspension. Thereafter, an alkaline silicon component, an acid-reacting titanium component and, optionally, a further pH-regulating component are added, the pH value being set in the range from 4 to 9 in this context.
摘要翻译： 本发明涉及一种用于装饰层压纸的金红石二氧化钛颜料，其与现有技术相比产生较高的不透明度，以及其制造方法。 颜料显示含有磷酸铝，氧化铝，氧化硅和氧化钛的表面涂层。 氧化硅以蓬松形式沉淀。 涂覆的颗粒的BET值至少为15m 2 / g。 该制造方法的特征在于首先将铝和磷成分加入到TiO 2悬浮液中。 此后，加入碱性硅成分，酸反应钛成分和任选的其他pH调节成分，在此上下文中将pH值设定在4〜9的范围内。
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2.发明申请Titanium dioxide pigment particles with doped, dense SiO2 skin and methods for their manufacture 有权具有掺杂，致密SiO 2皮肤的二氧化钛颜料颗粒及其制造方法公开(公告)号：US20100282128A1
公开(公告)日：2010-11-11
申请号：US12843077
申请日：2010-07-26
CPC分类号： C09C1/3661 , C01P2002/52 , C01P2002/54 , C01P2004/84 , Y10T428/24372 , Y10T428/2438 , Y10T428/24388 , Y10T428/2991
摘要： A method of predicting photostability of coatings with various dopants on titanium dioxide pigment particles is disclosed. Calculations of the density of states show that a doped coating which reduces the density of states near the band edge or increases the density of states within the band gap of the pigment particles increases the photostability of the doped pigment.
摘要翻译： 公开了一种用二氧化钛颜料颗粒预测各种掺杂剂涂层的光稳定性的方法。 状态密度的计算表明，降低带边缘附近状态密度或增加颜料颗粒带隙内状态密度的掺杂涂层增加了掺杂颜料的光稳定性。
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3.发明授权公开(公告)号：US07763110B2
公开(公告)日：2010-07-27
申请号：US11668692
申请日：2007-01-30
IPC分类号： C01G23/047 , C09C1/36 , E01F9/04 , E04D7/00 , B32B5/16 , B32B9/00 , B32B15/02 , B32B17/02 , B32B19/00 , B32B21/02 , B32B23/02
CPC分类号： C09C1/3661 , C01P2002/52 , C01P2002/84 , C01P2004/84 , Y10T428/24372 , Y10T428/2438 , Y10T428/24388 , Y10T428/2991 , Y10T428/2993
摘要： A method of predicting photostability of coatings with various dopants on titanium dioxide pigment particles is disclosed. Calculations of the density of states show that a doped coating which reduces the density of states near the band edge or increases the density of states within the band gap of the pigment particles increases the photostability of the doped pigment.
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4.发明申请Surface-Treated Titanium Dioxide Pigments for Plastics and Method for Production 审中-公开用于塑料的表面处理二氧化钛颜料和生产方法公开(公告)号：US20100125117A1
公开(公告)日：2010-05-20
申请号：US12619834
申请日：2009-11-17
CPC分类号： C09C1/3692 , C01P2006/12 , C09C1/3661 , C09C1/3684
摘要： A weather-resistant titanium dioxide pigment particularly suitable for use in engineering plastics, as well as to a method for its manufacture and to polymers containing the pigment. The titanium dioxide is provided with a surface coating that, from the inside to the outside, displays a SiO2 layer, an Al2O3 layer and an organic layer, where the maximum total Al2O3 content is 2.4% by weight and the organic layer contains at least one compound from the group comprising H-siloxanes, silicone oils and organically functionalised polysiloxanes. The manufacturing method is characterised in that an aqueous suspension of Al-doped titanium dioxide particles is milled in an agitator mill, and a SiO2 layer and an Al2O3 layer are then applied in batch mode, after which an organic layer is applied that contains at least one compound from the group comprising H-siloxanes, silicone oils and organically functionalised polysiloxanes.
摘要翻译： 特别适用于工程塑料的耐候性二氧化钛颜料，以及其制造方法和含有颜料的聚合物。 二氧化钛被提供有表面涂层，其从内到外显示SiO 2层，Al 2 O 3层和有机层，其中最大总Al 2 O 3含量为2.4重量％，并且有机层包含至少一个 化合物由包含H-硅氧烷，硅油和有机官能化的聚硅氧烷组成。 该制造方法的特征在于，在搅拌机中研磨掺杂Al的二氧化钛颗粒的水性悬浮液，然后分批施加SiO 2层和Al 2 O 3层，然后施加至少含有有机层 一种来自包含H-硅氧烷，硅油和有机官能化聚硅氧烷的化合物。
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5.发明申请公开(公告)号：US20070175365A1
公开(公告)日：2007-08-02
申请号：US11668729
申请日：2007-01-30
CPC分类号： C09C1/3661 , C01G23/07 , C01P2002/52 , C01P2002/84 , C01P2004/84 , Y10T428/24372 , Y10T428/2438 , Y10T428/24388 , Y10T428/2991 , Y10T428/2993
摘要： A method of predicting photostability of coatings with various dopants on titanium dioxide pigment particles is disclosed. Calculations of the density of states show that a doped coating which reduces the density of states near the band edge or increases the density of states within the band gap of the pigment particles increases the photostability of the doped pigment.
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6.发明授权公开(公告)号：US07988780B2
公开(公告)日：2011-08-02
申请号：US12843077
申请日：2010-07-26
IPC分类号： C09C1/36 , C01G23/047 , D06N7/04 , E01F9/04 , E04D7/00 , B32B5/16 , B32B9/00 , B32B15/02 , B32B17/02 , B32B19/00 , B32B21/02 , B32B23/02 , B32B27/02
CPC分类号： C09C1/3661 , C01P2002/52 , C01P2002/54 , C01P2004/84 , Y10T428/24372 , Y10T428/2438 , Y10T428/24388 , Y10T428/2991
摘要： A method of predicting photostability of coatings with various dopants on titanium dioxide pigment particles is disclosed. Calculations of the density of states show that a doped coating which reduces the density of states near the band edge or increases the density of states within the band gap of the pigment particles increases the photostability of the doped pigment.
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7.发明申请Method for the Surface Treatment of Solid Particles, Particularly Titanium Dioxide Pigment Particles 审中-公开固体颗粒，特别是二氧化钛颜料颗粒的表面处理方法公开(公告)号：US20080141905A1
公开(公告)日：2008-06-19
申请号：US11941156
申请日：2007-11-16
CPC分类号： C09C1/3661 , B82Y30/00 , C01P2004/04 , C01P2004/61 , C01P2004/62 , C01P2004/64 , C09C3/063
摘要： A method for manufacturing inorganic solid particles, particularly titanium dioxide pigment particles, with a smooth and homogeneous surface coating in an aqueous suspension.
摘要翻译： 一种在水性悬浮液中制备具有光滑均匀的表面涂层的无机固体颗粒，特别是二氧化钛颜料颗粒的方法。
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公开(公告)号：US07166157B2
公开(公告)日：2007-01-23
申请号：US10638154
申请日：2003-08-08
IPC分类号： C09C1/36 , C01G23/047 , B32B5/16 , B32B9/06
CPC分类号： C09C1/3661 , C01P2006/60 , Y10T428/2982 , Y10T428/2991 , Y10T428/31851
摘要： A method and material for improved TiO2 pigment for paper and laminates is described. Phosphorous, titanium, and aluminum compounds are successively added to a TiO2 pigment suspension. Resulting pigments show improved greying resistance and hiding power over prior art pigments, and show improved results as pigments in tests of paper and laminates.
摘要翻译： 描述了用于纸和层压材料的用于改进TiO 2颜料的方法和材料。 将磷，钛和铝化合物依次加入到TiO 2颜料悬浮液中。 所得颜料显示出比现有技术的颜料改善的耐灰色性和遮盖力，并且在纸和层压材料的测试中显示出改善的结果作为颜料。
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公开(公告)号：US07147702B2
公开(公告)日：2006-12-12
申请号：US10889287
申请日：2004-07-12
IPC分类号： C09C1/36 , C01G23/047 , B32B5/16
CPC分类号： D21H17/69 , C01P2006/62 , C01P2006/63 , C01P2006/64 , C09C1/3661 , D21H17/675 , Y10T428/2991
摘要： The invention relates to a method for the surface treatment of a titanium dioxide that leads to pigments with improved retention and improved opacity, where consistently high opacity can be obtained using less pigment. The method is characterised in that an aluminium component and a phosphorus component are first added to a TiO2 suspension, during which process its pH value does not drop below 10. The pH value of the suspension is subsequently lowered to below 9 by adding an acid component. The pigment produced by the method according to the invention is eminently suited to use in decorative laminating paper.
摘要翻译： 本发明涉及一种用于表面处理二氧化钛的方法，其导致颜料具有改善的保留性和改善的不透明度，其中可以使用较少的颜料获得一致的高不透明度。 该方法的特征在于首先将铝组分和磷组分加入到TiO 2悬浮液中，在此过程中，其pH值不降至10以下。随后降低悬浮液的pH值 通过加入酸组分至低于9。 通过根据本发明的方法生产的颜料非常适合用于装饰层压纸。
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公开(公告)号：US07135065B2
公开(公告)日：2006-11-14
申请号：US11179985
申请日：2005-07-12
IPC分类号： C09C1/36 , C01G23/047 , C01G23/08
CPC分类号： C09C1/3661 , C01P2002/30 , C01P2004/84 , C01P2006/64 , C08K3/22 , C08K9/02 , C09D7/62
摘要： The invention relates to a method for the post-treatment of titanium dioxide, in order to produce particularly weather-resistant titanium dioxide pigments with good optical properties. The method is characterized in that, together with the hydrous oxides of tin and zirconium, at least one other from the group comprising aluminium, silicon and titanium is additionally precipitated onto the particle surface. The post-treatment components are added to the aqueous TiO2 suspension either in the acidic range (pH value of 3 at most) or in the alkaline range (pH value of 10 at least). The pH value is subsequently set to between 6 and 8. Final tempering of the pigment at elevated temperatures from over 125° C. to up to 500° C. can improve the tone b. The pigment is particularly suitable for use in paints, coatings and plastics.
摘要翻译： 本发明涉及一种后处理二氧化钛的方法，以便制备具有良好光学性能的特别耐候的二氧化钛颜料。 该方法的特征在于，与锡和锆的水合氧化物一起，还包括从铝，硅和钛组成的组中的至少一种另外沉淀到颗粒表面上。 将后处理组分在酸性范围（pH值为3以下）或碱性范围（至少为pH值为10）中添加到TiO 2水溶液中。 pH值随后设定在6和8之间。颜料在高于125℃至高达500℃的高温下进行最终回火可改善色调b。 该颜料特别适用于油漆，涂料和塑料。
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