公开(公告)号：US4207188A

公开(公告)日：1980-06-10

申请号：US938350

申请日：1978-08-31

申请人： Takao Tsuda ,  Kiyokatsu Hibi ,  Toyohide Takeuchi ,  Tomohiko Nakanishi ,  Daido Ishii ,  Koichi Mochizuki

发明人： Takao Tsuda ,  Kiyokatsu Hibi ,  Toyohide Takeuchi ,  Tomohiko Nakanishi ,  Daido Ishii ,  Koichi Mochizuki

IPC分类号： G01N30/60 ,  B01D15/08

CPC分类号： G01N30/482 ,  G01N30/6078 ,  B01J2220/54

摘要： An open tubular capillary column, for high-speed micro liquid chromatography made of a glass tube of the inner diameter not more than 0.10 mm, having the net inside capacity not less than 0.5 .mu.l, the inner surface of which hollow glass tube being chemically bonded, in order to provide a stationary phase there, with at least one silane or its derivative such as octadecylsilane to form a polymeric layer. This invention includes the manufacturing method of such a column.

摘要翻译： 一个开放的管状毛细管柱，用于由内径不大于0.10mm的玻璃管制成的高速微量液相色谱，其净内容不小于0.5μl，其中空玻璃管​​的内表面化学 键合，以便在其中提供至少一种硅烷或其衍生物如十八烷基硅烷的固定相以形成聚合物层。 本发明包括这种柱的制造方法。

公开(公告)号：US4346610A

公开(公告)日：1982-08-31

申请号：US139698

申请日：1980-04-11

申请人： Daido Ishii ,  Hideki Konishi

发明人： Daido Ishii ,  Hideki Konishi

IPC分类号： G01N1/00 ,  G01N30/20 ,  G01N1/20

CPC分类号： G01N35/1097 ,  G01N30/20

摘要： A sample introducing device, placed in the midway of an analyzing apparatus having a sample flowing route and a carrier fluid flowing route, in which device a valve disc rotatably disposed under urging force between a pair of supporting members, provided with a sample flowing passage and a carrier fluid flowing passage, in a sandwiched manner, is manually rotated with a handle so as to switch a sample flowing hole made in the valve disc for containing a predetermined amount of a sample to a position alignable with the carrier fluid flowing passage. By this simple operation of rotating the valve disc the desired amount of the sample can be transferred to the carrier fluid flowing passage, through the switching over of the sample flowing hole, for being flowed to an apparatus for analysis.

摘要翻译： 一种试样引入装置，放置在具有样品流动路径和载体流体流动路径的分析装置的中途，该装置中的阀盘可旋转地设置在一对支撑构件之间的推动力下，设置有样品流动通道和 以夹持方式将载体流体流动通道用手柄旋转，以将用于容纳预定量的样品的阀盘中形成的样品流动孔切换到与载体流体流动通道对准的位置。 通过旋转阀盘的这种简单的操作，通过切换样品流动孔，将所需量的样品转移到载体流体流动通道，以流动到用于分析的装置。