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    Binders water-dilutable by protonation with acid
    1.
    发明授权
    Binders water-dilutable by protonation with acid 失效
    通过用酸质子化可水稀释的粘合剂

    公开(公告)号：US4871808A

    公开(公告)日：1989-10-03

    申请号：US116868

    申请日：1987-11-05

    申请人： Thomas Schwerzel ,  Rolf Osterloh ,  Eberhard Schupp ,  Thomas Perner ,  Klaas Ahlers

    发明人： Thomas Schwerzel ,  Rolf Osterloh ,  Eberhard Schupp ,  Thomas Perner ,  Klaas Ahlers

    IPC分类号： C08G59/14 ,  C08G59/00 ,  C08G59/40 ,  C08G59/50 ,  C08L63/00 ,  C09D5/44 ,  C09D163/00

    CPC分类号： C09D5/4434 ,  C08G59/50 ,  C09D163/00

    摘要： A binder which is water-dilutable on protonation with acid and obtainable by a reaction of(A) an epoxy resin having an average molecular weight of from 300 to 6,000 and on average from 1.5 to 3.0 epoxide groups per molecule and(B) from 20 to 30 mol %, based on the amount of epoxide groups present in epoxy resin (A), of one or more secondary amine and/or alkanolamine of up to 40 carbon atomsand subsequent reaction with(C) a copolymer which is based on butadiene and acrylonitrile and contains primary and/or secondary amino groups, the amount of (C) being so dimensioned that the number of primary and secondary amino groups corresponds to from 1 to 50 mol % of the epoxide groups present in the epoxy resin (A), and also(D) with one or more primary and/or secondary amine to convert any epoxide groups still present, is usedin particular for cathodic electrocoating.

    摘要翻译： 可用酸质子化水可稀释的粘合剂，可通过（A）平均分子量为300〜6,000的环氧树脂和每分子平均1.5〜3.0个环氧基团的反应得到（B）20 至多30摩尔％，基于环氧树脂（A）中存在的环氧基团的量，至多40个碳原子的一种或多种仲胺和/或链烷醇胺，随后与（C）基于丁二烯的共聚物反应 和丙烯腈，并且包含伯和/或仲氨基，（C）的量的尺寸使得伯和仲氨基的数量对应于环氧树脂（A）中存在的环氧基团的1至50摩尔％ ，以及（D）与一种或多种伯和/或仲胺以转化仍存在的任何环氧基团，特别用于阴极电涂覆。

    Synthetic resin with basic nitrogen groups, preparation and use thereof
    5.
    发明授权
    Synthetic resin with basic nitrogen groups, preparation and use thereof 失效
    具有碱性氮基团的合成树脂，其制备和用途

    公开(公告)号：US4981884A

    公开(公告)日：1991-01-01

    申请号：US210502

    申请日：1988-06-23

    申请人： Thomas Perner ,  Rolf Osterloh ,  Eberhard Schupp ,  Thomas Schwerzel ,  Klaas Ahlers

    发明人： Thomas Perner ,  Rolf Osterloh ,  Eberhard Schupp ,  Thomas Schwerzel ,  Klaas Ahlers

    IPC分类号： C08L63/00 ,  C08G59/00 ,  C08G59/28 ,  C09D5/44 ,  C09D163/00

    CPC分类号： C09D5/4473 ,  C09D5/4434

    摘要： A synthetic resin which carries basic nitrogen groups and is water-dilutable by protonation with an acid, containing(A) a chain-extended, amine-modified epoxy resin obtainable by reacting(a.sub.1) an epoxy resin having an average molecular weight M.sub.n of from 300 to 6,000 and on average from 1.5 to 3.0 epoxy groups per molecule with(a.sub.2) a diketimine of a diprimary diamine, which diprimary diamine contains no further groups reactive with epoxy groups under mild conditions and(B) an amino-modified epoxy resin obtainable by reactingb.sub.1) an epoxy resin having an average molecular weight M.sub.n of from 800 to 6,000 and on average from 1.5 to 3.0 epoxy groups per molecule with(b.sub.2) a secondary amine or a secondary-tertiary diamine, a ketimine of a primary monoamine or a ketimine of a primary/tertiary diamine or a mixture of these (b.sub.2) components, with the proviso that (A) and (B) are different.

    摘要翻译： 一种合成树脂，其承载碱性氮基团并且可通过用酸质子化而进行水稀释，所述合成树脂含有（A）伸长的胺改性的环氧树脂，其通过使（a1）平均分子量Mn为 300〜6000，平均每个分子具有1.5〜3.0个环氧基，（a2）二元二胺的二酮亚胺，该二元二胺在温和条件下不含有与环氧基反应的其它基团，（B）可得到的氨基改性环氧树脂 通过使b1）平均分子量Mn为800至6000，平均每分子具有1.5至3.0个环氧基的环氧树脂与（b2）仲胺或仲叔胺，伯胺的酮亚胺或 伯（叔）二胺的酮亚胺或这些（b2）成分的混合物，条件是（A）和（B）不同。

    Binder which is rendered water-dilutable by protonation with an acid, from carboxyl terminated butadiene/acrylonitrile copolymers
    6.
    发明授权
    Binder which is rendered water-dilutable by protonation with an acid, from carboxyl terminated butadiene/acrylonitrile copolymers 失效
    由羧基封端的丁二烯/丙烯腈共聚物通过酸质子化而使水可稀释的粘合剂

    公开(公告)号：US4769420A

    公开(公告)日：1988-09-06

    申请号：US934562

    申请日：1986-11-25

    申请人： Thomas Schwerzel ,  Rolf Osterloh ,  Eberhard Schupp ,  Klaas Ahlers

    发明人： Thomas Schwerzel ,  Rolf Osterloh ,  Eberhard Schupp ,  Klaas Ahlers

    IPC分类号： C08G59/42 ,  C08G59/58 ,  C09D5/44 ,  C09D151/00 ,  C09D163/00 ,  B05D1/28 ,  B05D7/02

    CPC分类号： C09D5/4488 ,  C08G59/4292 ,  C08G59/58 ,  C09D163/00

    摘要： Binders which are rendered water-dilutable by protonation with an acid, a process for their preparation and their use.These binders are obtainable by reacting a(A) Reaction product of a(a) carboxyl-containing component, consisting of a(a1) carboxyl-containing butadiene/acrylonitrile copolymer having a molecular weight of from 500 to 8,000, if necessary as a mixture with(a2) a dicarboxylic acid which differs from (a1) and, if appropriate,(a3) a monocarboxylic acid and(b) a diprimary and/or primary/secondary amine, with the proviso that from 0.7 to 5 moles of the said amine are used per mole of carboxyl groups of component (a), with one or more(B) epoxy resins having a mean molecular weight from 300 to 6,000 and containing on average from 1.5 to 3.0 epoxide groups per molecule and, if required,(C) an aliphatic or cycloaliphatic secondary amine.In combination with a crosslinking agent, they are useful as coating materials, in particular for cathodic electrocoating.

    摘要翻译： 通过用酸质子化可水稀释的粘合剂，其制备方法及其用途。 这些粘合剂可以通过使（A）含羧基组分的反应产物（如有必要）与由（a1）分子量为500-8,000的（a1）含羧基的丁二烯/丙烯腈共聚物组成的混合物 与（a1）和（a1）不同的二羧酸和（a3）一元羧酸和（b）二原子和/或伯/仲胺，如果合适的话，条件是0.7-5摩尔所述 胺组分（a）的每摩尔羧基使用，一种或多种（B）环氧树脂的平均分子量为300至6,000，每分子平均含有1.5至3.0个环氧基团，如果需要，（ C）脂族或脂环族仲胺。 与交联剂组合，它们可用作涂料，特别是用于阴极电泳涂覆。

    Cathodic electrocoating binders
    7.
    发明授权
    Cathodic electrocoating binders 失效
    阴极电泳粘合剂

    公开(公告)号：US4594136A

    公开(公告)日：1986-06-10

    申请号：US755725

    申请日：1985-07-17

    申请人： Eberhard Schupp ,  Werner Loch ,  Rolf Osterloh ,  Klaas Ahlers

    发明人： Eberhard Schupp ,  Werner Loch ,  Rolf Osterloh ,  Klaas Ahlers

    IPC分类号： C08G18/64 ,  C08G18/67 ,  C08G18/81 ,  C09D5/44 ,  C25D13/00

    CPC分类号： C09D5/4419 ,  C08G18/643 ,  C08G18/6705 ,  C08G18/8158 ,  Y10S524/901

    摘要： Binders useful for cathodic electrocoating are water-dilutable on addition of acid and comprise a mixture of(A) a polyadduct which carries basic nitrogen groups and contains groups of the formula (I) and/or (II) ##STR1## where R.sup.1 and R.sup.2 are hydrogen or methyl and R.sup.3 and R.sup.4 are alkyl or hydroxyalkyl or together are a 5- or 6-membered ring, and(B) a reaction product of a polyisocyanate and an olefinically unsaturated amine which carries a secondary amino group and a methacrylamide or methacrylate group.

    摘要翻译： 用于阴极电泳的粘合剂在加入酸时是可水稀释的，并且包含（A）含有碱性氮基团并含有式（I）和/或（II）的基团的多加成物的混合物。 （II）其中R1和R2是氢或甲基，R3和R4是烷基或羟基烷基或一起是5-或6-元环，和（B）多异氰酸酯和烯属不饱和胺的反应产物，其携带 仲氨基和甲基丙烯酰胺或甲基丙烯酸酯基。

    Synthetic resin carrying basic nitrogen groups, its preparation, coating materials produced using this resin, and cathodic electrocoating
    9.
    发明授权
    Synthetic resin carrying basic nitrogen groups, its preparation, coating materials produced using this resin, and cathodic electrocoating 失效
    携带碱性氮基团的合成树脂，其制备方法，使用该树脂制备的涂料，以及阴极电泳涂料

    公开(公告)号：US4699937A

    公开(公告)日：1987-10-13

    申请号：US808281

    申请日：1985-12-12

    申请人： Werner Loch ,  Eberhard Schupp ,  Rolf Osterloh ,  Klaas Ahlers

    发明人： Werner Loch ,  Eberhard Schupp ,  Rolf Osterloh ,  Klaas Ahlers

    IPC分类号： C08G59/40 ,  C08G59/56 ,  C09D5/44 ,  C08G59/46

    CPC分类号： C09D5/4434 ,  C08G59/4042 ,  C08G59/56

    摘要： A synthetic resin carrying basic nitrogen groups, its preparation, coating materials prepared from this resin, and a process for cathodic electrocoating.This synthetic resin is obtained by reacting(A) an epoxy resin which(B) a diketimine of a diprimary amineand, if required,(C) with a secondary amine, which may additionally contain a tertiary amino group, with a ketimine of a primary monoamine and/or with a ketimine of a primary/tertiary diamine,a diketimine obtained from(B.sub.1) a ketone and(B.sub.2) a branched aliphatic diprimary diamine of 5 to 9 carbon atoms and/or(B.sub.3) one or more diaminodiamides which are obtained by condensation of 2 moles of diamine (B.sub.2) and 1 mole of a dicarboxylic acidbeing employed as component (B).After protonation with an acid, this synthetic resin is useful as a binder for cathodic electrocoating.

    摘要翻译： 携带碱性氮基团的合成树脂，其制备方法，由该树脂制备的涂料，以及阴极电泳方法。 该合成树脂通过使（A）环氧树脂与（B）二胺的二酮亚胺和（如果需要的话）（C）与另外含有叔氨基的仲胺和 （B1）酮和（B2）碳原子数为5〜9的支链脂肪族二元二胺和/或（B3）一种或多种二氨基二胺的二酮亚胺，其主要单胺和/或与伯/叔二胺的酮亚胺， 通过2摩尔二胺（B2）和1摩尔作为组分（B）的二羧酸的缩合获得。 在用酸质子化后，该合成树脂可用作阴极电涂层的粘合剂。

    Synthetic resin carrying basic nitrogen groups, and its preparation
    10.
    发明授权
    Synthetic resin carrying basic nitrogen groups, and its preparation 失效
    携带碱性氮基的合成树脂及其制备方法

    公开(公告)号：US4557814A

    公开(公告)日：1985-12-10

    申请号：US629762

    申请日：1984-07-11

    申请人： Eberhard Schupp ,  Werner Loch ,  Rolf Osterloh ,  Klaas Ahlers

    发明人： Eberhard Schupp ,  Werner Loch ,  Rolf Osterloh ,  Klaas Ahlers

    IPC分类号： C08G18/00 ,  C08G18/58 ,  C08G59/00 ,  C08G59/14 ,  C08G59/40 ,  C09D5/44 ,  C09D163/00 ,  C09D175/00 ,  C08G59/50

    CPC分类号： C09D5/4438 ,  C08G59/4028 ,  C08G59/4042 ,  C09D163/00

    摘要： A synthetic resin which carries basic nitrogen groups and can be diluted with water as a result of protonation with an acid can be obtained by reacting an epoxy resin, having a mean molecular weight M.sub.n of from 300 to 6,000 and containing on average from 1.5 to 3.0 epoxide groups per molecule, with a diketimine of a primary diamine and, if appropriate, a secondary amine, which may additionally contain a tertiary amino group, a ketimine of a primary monoamine and/or a ketimine of a primary/tertiary diamine.These resins are useful as binders for coating agents, in particular for the cathodic electrocoating of electrically conductive substrates.

    摘要翻译： 携带碱性氮基并可用酸质子化的水稀释的合成树脂可以通过使平均分子量＆Upbar＆Mn的平均分子量＆Mn> 300至6,000并且平均含有1.5的环氧树脂与 每个分子具有3.0个环氧基团，与一个二胺的二酮亚胺和如果合适的话，可以另外含有叔氨基的仲胺，伯/叔二胺的伯胺和/或酮亚胺的酮亚胺。 这些树脂可用作涂层剂的粘合剂，特别是用于导电基材的阴极电涂层。