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1.发明授权Cladophora-form carbon comprising carbon nanomaterials radially grown on a spherical core, process for producing the same and production apparatus 失效包含在球形芯上径向生长的碳纳米材料的枝晶型碳，其制造方法和制造装置公开(公告)号：US07608331B2
公开(公告)日：2009-10-27
申请号：US11597361
申请日：2005-05-10
申请人： Toshihiro Ando , Kiyoharu Nakagawa , Mika Gamo , Hirokazu Oda
发明人： Toshihiro Ando , Kiyoharu Nakagawa , Mika Gamo , Hirokazu Oda
CPC分类号： B82Y30/00 , B01J23/44 , B01J23/75 , B01J23/755 , B82Y40/00 , C01B32/162 , D01F9/127 , Y10T428/2991
摘要： A fine spherical particle formed of diamond as a core and having carbon nano-materials radially grown therefrom is disclosed, which exhibits the appearance of a Marimo (Cladophora sauteri) particle. Fine diamond catalytic particles 2 whose surfaces are oxidized and treated to carry a transition metal catalyst are floated and stirred in a gas phase of hydrocarbon while being heated at a selected temperature to bring about a catalytic reaction which synthesizes carbon nano-materials and to grow them on the surface of said oxidized fine diamond particle. Nano fibers or filaments 32 of a nano size are grown from the fine diamond catalytic particle 31 as a core to form cladophora-form carbon. The carbon nano-materials if the supported transition metal is Ni or Co become carbon nano-tubes and if it is Pd become coin stacked carbon nano-graphite.
摘要翻译： 公开了一种由金刚石作为核并由其径向生长的碳纳米材料形成的细小球形颗粒，其显示出Marimo（Cladophora sauteri）颗粒的外观。 其表面被氧化并处理以携带过渡金属催化剂的细金刚石催化剂颗粒2在烃的气相中漂浮并搅拌，同时在选定的温度下加热以产生合成碳纳米材料并使其成长的催化反应 在所述氧化的细金刚石颗粒的表面上。 从作为芯的细金刚石催化剂粒子31生长纳米尺寸的纳米纤维或长丝32，以形成双峰型碳。 碳纳米材料如果负载的过渡金属是Ni或Co成为碳纳米管，如果是Pd，则成为硬币堆积的碳纳米石墨。
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2.发明申请Cladophora-Form Carbon, Process for Producing the Same and Production Apparatus 失效Cladophora-Carbon碳，生产工艺及生产设备公开(公告)号：US20080193764A1
公开(公告)日：2008-08-14
申请号：US11597361
申请日：2005-05-10
申请人： Toshihiro Ando , Kiyohara Nakagawa , Mika Gamo , Hirokazu Oda
发明人： Toshihiro Ando , Kiyohara Nakagawa , Mika Gamo , Hirokazu Oda
IPC分类号： C01B31/02 , B01J23/44 , B01J23/75 , B01J23/755 , C01B31/06
CPC分类号： B82Y30/00 , B01J23/44 , B01J23/75 , B01J23/755 , B82Y40/00 , C01B32/162 , D01F9/127 , Y10T428/2991
摘要： A fine spherical particle formed of diamond as a core and having carbon nano-materials radially grown therefrom is disclosed, which exhibits the appearance of a Marimo (Cladophora sauteri) particle. Fine diamond catalytic particles 2 whose surfaces are oxidized and treated to carry a transition metal catalyst are floated and stirred in a gas phase of hydrocarbon while being heated at a selected temperature to bring about a catalytic reaction which synthesizes carbon nano-materials and to grow them on the surface of said oxidized fine diamond particle. Nano fibers or filaments 32 of a nano size are grown from the fine diamond catalytic particle 31 as a core to form cladophora-form carbon. The carbon nano-materials if the supported transition metal is Ni or Co become carbon nano-tubes and if it is Pd become coin stacked carbon nano-graphite.
摘要翻译： 公开了一种由金刚石作为核并由其径向生长的碳纳米材料形成的细小球形颗粒，其显示出Marimo（Cladophora sauteri）颗粒的外观。 其表面被氧化并处理以携带过渡金属催化剂的细金刚石催化剂颗粒2在烃的气相中漂浮并搅拌，同时在选定的温度下加热以产生合成碳纳米材料并使其成长的催化反应 在所述氧化的细金刚石颗粒的表面上。 从作为芯的细金刚石催化剂粒子31生长纳米尺寸的纳米纤维或长丝32，以形成双峰型碳。 碳纳米材料如果负载的过渡金属是Ni或Co成为碳纳米管，如果是Pd，则成为硬币堆积的碳纳米石墨。
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