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    Process for producing geranylgeraniol
    1.
    发明授权
    Process for producing geranylgeraniol 失效
    香叶基香叶醇的制备方法

    公开(公告)号：US5663461A

    公开(公告)日：1997-09-02

    申请号：US554405

    申请日：1995-11-06

    申请人： Toshiki Mori ,  Junko Sato ,  Takashi Fukumoto ,  Kozo Nakao ,  Yoshin Tamai

    发明人： Toshiki Mori ,  Junko Sato ,  Takashi Fukumoto ,  Kozo Nakao ,  Yoshin Tamai

    IPC分类号： C07C27/02 ,  C07C29/09 ,  C07C33/02 ,  C07C67/52

    CPC分类号： C07C33/02 ,  C07C201/16 ,  C07C29/095 ,  C07C67/52

    摘要： A process for producing geranylgeraniol is provided, which comprising the steps of subjecting a mixture of at least one ester derivative wherein one or more carbon-carbon double bonds in the molecule are in cis form represented by the general formula (1): ##STR1## wherein R represents an aromatic group which can be substituted with at least one substituent, or a higher aliphatic group having from 7 to 25 carbon atoms, and wavy lines, respectively, represent a state where each carbon-carbon double bond can be present in cis or trans form, and an ester derivative of the general formula (2): ##STR2## wherein R is as defined above, to crystallization to obtain the ester derivative of the formula (2) selectively, and hydrolyzing the thus obtained ester derivative.

    摘要翻译： 提供了一种制备香叶基香叶醇的方法，其包括使分子中一个或多个碳 - 碳双键为通式（1）表示的顺式的至少一种酯衍生物的混合物的步骤： （1）其中R表示可以被至少一个取代基取代的芳族基团或具有7-25个碳原子的高级脂族基团，波浪线分别表示每个碳 - 碳双键可以 （2）的酯衍生物：其中R如上所定义，结晶以选择性地得到式（2）的酯衍生物，并水解所述式 由此得到酯衍生物。

    Process for preparation of 4-n-substituted amino-2-aza-1-oxabicyclo[3.3.0] oct-2-ene-6-carboxylic acid esters and process for preparation of their intermediates
    3.
    发明授权
    Process for preparation of 4-n-substituted amino-2-aza-1-oxabicyclo[3.3.0] oct-2-ene-6-carboxylic acid esters and process for preparation of their intermediates 失效
    4-取代氨基-2-氮杂-1-氧杂双环[3.3.0]辛-2-烯-6-羧酸酯的制备方法及其中间体的制备方法

    公开(公告)号：US07038059B2

    公开(公告)日：2006-05-02

    申请号：US10399047

    申请日：2001-10-01

    申请人： Takashi Fukumoto ,  Masahiro Torihara ,  Yoshin Tamai

    发明人： Takashi Fukumoto ,  Masahiro Torihara ,  Yoshin Tamai

    IPC分类号： C07D261/20

    CPC分类号： C07C229/48 ,  C07C2601/10 ,  C07D261/20 ,  Y02P20/55

    摘要： 4-N-substituted amino-2-aza-1-oxabicyclo[3.3.0]oct-2-ene-6-carboxylic acid esters are produced by adding a Brønsted acid to a mixture of a 2-azabicyclo[2.2.1]hept-5-en-3-one and an alcohol, thereby causing these components to react with each other to give a salt of cis-4-amino-2-cyclopentene-1-carboxylic acid ester, then allowing the salt of cis-4-amino-2-cyclopentene-1-carboxylic acid ester thus obtained to react with an amino-protecting group introducing compound in the presence of a base, thereby giving cis-4-N-substituted amino-2-cyclopentene-1-carboxylic acid ester, and then allowing this cis-4-N-substituted amino-2-cyclopentene-1-carboxylic acid ester to react with a hypohalogenite and an aldoxime.

    摘要翻译： 4-N-取代的氨基-2-氮杂-1-氧杂双环[3.3.0]辛-2-烯-6-羧酸酯是通过将布朗斯台德酸加入到2-氮杂双环[2.2.1] 庚-5-烯-3-酮和醇，从而使这些组分彼此反应，得到顺式-4-氨基-2-环戊烯-1-羧酸酯的盐，然后使顺式-4- 4-氨基-2-环戊烯-1-羧酸酯在碱存在下与氨基保护基导入化合物反应，从而得到顺式-4-N-取代的氨基-2-环戊烯-1-羧酸 酸酯，然后使该顺式-4-N-取代的氨基-2-环戊烯-1-羧酸酯与次卤酸盐和醛肟反应。

    (METH)ACRYLATE DERIVATIVE, INTERMEDIATE THEREOF, AND POLYMER COMPOUND
    4.
    发明申请
    (METH)ACRYLATE DERIVATIVE, INTERMEDIATE THEREOF, AND POLYMER COMPOUND 有权
    （METH）丙烯酸酯衍生物，其中间体和聚合物化合物

    公开(公告)号：US20100331508A1

    公开(公告)日：2010-12-30

    申请号：US12918675

    申请日：2009-02-20

    申请人： Junko Sato ,  Osamu Nakayama ,  Takashi Fukumoto

    发明人： Junko Sato ,  Osamu Nakayama ,  Takashi Fukumoto

    IPC分类号： C08F228/06 ,  C07D339/08 ,  C07D327/06 ,  C07D319/12 ,  C07D339/00 ,  C07D327/00 ,  C07D323/00 ,  C08F224/00

    CPC分类号： C07D327/06 ,  C07D339/08 ,  C08F220/28 ,  C08F220/38 ,  G03F7/0395 ,  G03F7/0397 ,  C08F220/18 ,  C08F222/06 ,  C08F232/08

    摘要： Provided are a polymerizable compound shown below which is useful as a raw material for a polymer having less swelling in developing, a polymer obtained by polymerizing a raw material containing the above polymerizable compound, a photoresist composition which contains the above polymer and which is improved in LWR and an efficient production process for the polymerizable compound described above: wherein n represents an integer of 0 to 2; R1 represents a hydrogen atom, methyl or trifluoromethyl; R2, R3, R4, R5, R6, R7, R8, R9 and R10 represent a hydrogen atom, an alkyl group having 1 to 6 carbon atoms or the like; W represents an alkylene group having 1 to 10 carbon atoms or the like; and Y1 and Y2 represent an oxygen atom or a sulfur atom.

    摘要翻译： 提供下述可聚合化合物，其可用作显影时溶胀较小的聚合物的原料，通过聚合含有上述可聚合化合物的原料获得的聚合物，含有上述聚合物的光致抗蚀剂组合物， LWR和上述可聚合化合物的有效制备方法：其中n表示0至2的整数; R1表示氢原子，甲基或三氟甲基; R 2，R 3，R 4，R 5，R 6，R 7，R 8，R 9和R 10表示氢原子，碳原子数1〜6的烷基等; W表示碳原子数1〜10的亚烷基等; Y 1和Y 2表示氧原子或硫原子。

    Acrylate derivative, haloester derivative, polymer compound and photoresist composition
    5.
    发明授权
    Acrylate derivative, haloester derivative, polymer compound and photoresist composition 有权
    丙烯酸酯衍生物，卤代酯衍生物，高分子化合物和光致抗蚀剂组合物

    公开(公告)号：US08486606B2

    公开(公告)日：2013-07-16

    申请号：US13001738

    申请日：2009-06-30

    申请人： Junko Sato ,  Osamu Nakayama ,  Takashi Fukumoto

    发明人： Junko Sato ,  Osamu Nakayama ,  Takashi Fukumoto

    IPC分类号： G03F7/039 ,  C07D327/04 ,  C07D497/08 ,  C08F20/38

    CPC分类号： C07D327/04 ,  C07D497/18 ,  C08F220/38 ,  G03F7/0045 ,  G03F7/0397 ,  G03F7/085

    摘要： An acrylate derivative represented by the following general formula (1): (in the formula, R1 represents a hydrogen atom, a methyl group or a trifluoromethyl group; each of R2, R3, R5, R7, R8, R9 and R10 independently represents a hydrogen atom, an alkyl group, a cycloalkyl group or an alkoxy group; each of R4 and R6 independently represents a hydrogen atom, an alkyl group, a cycloalkyl group or an alkoxy group, or R4 and R6 are bonded to each other to represent an alkylene group, —O— or —S—; n represents 0, 1 or 2; and W represents an alkylene group or a cycloalkylene group); an intermediate thereof; a method for producing the same; a polymer compound which is obtainable from polymerization of a raw material containing the foregoing acrylate derivative and which is excellent in solubility in an organic solvent used for the preparation of a photoresist composition; and a photoresist composition containing the polymer compound, an organic solvent and a photo acid generator and having excellent adhesion to substrate and less pattern collapse, are provided.

    摘要翻译： 由以下通式（1）表示的丙烯酸酯衍生物：（式中，R1表示氢原子，甲基或三氟甲基; R2，R3，R5，R7，R8，R9和R10各自独立地表示 氢原子，烷基，环烷基或烷氧基; R 4和R 6各自独立地表示氢原子，烷基，环烷基或烷氧基，或者R 4和R 6相互键合，表示 亚烷基，-O-或-S-; n表示0,1或2; W表示亚烷基或亚环烷基）。 其中间体; 其制造方法; 可从含有上述丙烯酸酯衍生物的原料的聚合得到的聚合物化合物，其在用于制备光致抗蚀剂组合物的有机溶剂中的溶解性优异; 并且提供了含有高分子化合物，有机溶剂和光酸产生剂并且对基材具有优异粘附性和较少图案折叠的光致抗蚀剂组合物。

    Method for producing 2-isopropenyl-5-methyl-4-hexen-1-yl 3-methyl-2-butenoate
    6.
    发明授权
    Method for producing 2-isopropenyl-5-methyl-4-hexen-1-yl 3-methyl-2-butenoate 有权
    2-异丙烯基-5-甲基-4-己烯-1-基3-甲基-2-丁烯酸酯的制备方法

    公开(公告)号：US08097746B2

    公开(公告)日：2012-01-17

    申请号：US11910860

    申请日：2006-03-29

    申请人： Katsuji Ujita ,  Junko Sato ,  Takashi Fukumoto

    发明人： Katsuji Ujita ,  Junko Sato ,  Takashi Fukumoto

    IPC分类号： C07C309/67 ,  C07C67/00

    CPC分类号： C07C309/66 ,  C07C67/10 ,  C07C303/28 ,  C07C69/533 ,  C07C309/73

    摘要： The present invention provides a method of producing 2-isopropenyl-5-methyl-4-hexen-1-yl 3-methyl-2-butenoate industrially advantageously in a high yield. More particularly, the present invention provides a method of producing 2-isopropenyl-5-methyl-4-hexen-1-yl 3-methyl-2-butenoate represented by the following formula (IV): which comprises reacting 2-isopropenyl-5-methyl-4-hexen-1-ol with an organic sulfonyl halide in the presence of a basic substance to give a sulfonate compound represented by the following formula (III): wherein R is a hydrocarbon group, and reacting the obtained sulfonate compound with senecionic acid in the presence of a basic substance.

    摘要翻译： 本发明提供了在工业上有利地以高产率生产2-异丙烯基-5-甲基-4-己烯-1-基3-甲基-2-丁烯酸2-乙烯酯的方法。 更具体地说，本发明提供一种由下式（Ⅳ）表示的2-异丙烯基-5-甲基-4-己烯-1-基3-甲基-2-丁烯酸2-乙烯酯的制备方法：其包括使2-异丙烯基-5 - 甲基-4-己烯-1-醇与有机磺酰卤在碱性物质的存在下反应，得到下式（III）表示的磺酸盐化合物：其中R是烃基，并使得到的磺酸盐化合物与 在一种碱性物质的存在下的硫氰酸。

    ACRYLATE DERIVATIVE, HALOESTER DERIVATIVE, POLYMER COMPOUND AND PHOTORESIST COMPOSITION
    7.
    发明申请
    ACRYLATE DERIVATIVE, HALOESTER DERIVATIVE, POLYMER COMPOUND AND PHOTORESIST COMPOSITION 有权
    丙烯酸衍生物，阴离子衍生物，聚合物化合物和光电组合物

    公开(公告)号：US20110117497A1

    公开(公告)日：2011-05-19

    申请号：US13001738

    申请日：2009-06-30

    申请人： Junko Sato ,  Osamu Nakayama ,  Takashi Fukumoto

    发明人： Junko Sato ,  Osamu Nakayama ,  Takashi Fukumoto

    IPC分类号： G03F7/004 ,  C07D411/14 ,  C07D327/04 ,  C08F28/06

    CPC分类号： C07D327/04 ,  C07D497/18 ,  C08F220/38 ,  G03F7/0045 ,  G03F7/0397 ,  G03F7/085

    摘要： An acrylate derivative represented by the following general formula (1): (in the formula, R1 represents a hydrogen atom, a methyl group or a trifluoromethyl group; each of R2, R3, R5, R7, R8, R9 and R10 independently represents a hydrogen atom, an alkyl group, a cycloalkyl group or an alkoxy group; each of R4 and R6 independently represents a hydrogen atom, an alkyl group, a cycloalkyl group or an alkoxy group, or R4 and R6 are bonded to each other to represent an alkylene group, —O— or —S—; n represents 0, 1 or 2; and W represents an alkylene group or a cycloalkylene group); an intermediate thereof; a method for producing the same; a polymer compound which is obtainable from polymerization of a raw material containing the foregoing acrylate derivative and which is excellent in solubility in an organic solvent used for the preparation of a photoresist composition; and a photoresist composition containing the polymer compound, an organic solvent and a photo acid generator and having excellent adhesion to substrate and less pattern collapse, are provided.

    摘要翻译： 由以下通式（1）表示的丙烯酸酯衍生物：（式中，R1表示氢原子，甲基或三氟甲基; R2，R3，R5，R7，R8，R9和R10各自独立地表示 氢原子，烷基，环烷基或烷氧基; R 4和R 6各自独立地表示氢原子，烷基，环烷基或烷氧基，或者R 4和R 6相互键合，表示 亚烷基，-O-或-S-; n表示0,1或2; W表示亚烷基或亚环烷基）。 其中间体; 其制造方法; 可从含有上述丙烯酸酯衍生物的原料的聚合得到的聚合物化合物，其在用于制备光致抗蚀剂组合物的有机溶剂中的溶解性优异; 并且提供了含有高分子化合物，有机溶剂和光酸产生剂并且对基材具有优异粘附性和较少图案折叠的光致抗蚀剂组合物。

    (Meth)acrylate derivative, intermediate thereof, and polymer compound
    8.
    发明授权
    (Meth)acrylate derivative, intermediate thereof, and polymer compound 有权
    （甲基）丙烯酸酯衍生物，其中间体和高分子化合物

    公开(公告)号：US08492562B2

    公开(公告)日：2013-07-23

    申请号：US12918675

    申请日：2009-02-20

    申请人： Junko Sato ,  Osamu Nakayama ,  Takashi Fukumoto

    发明人： Junko Sato ,  Osamu Nakayama ,  Takashi Fukumoto

    IPC分类号： C07D327/06 ,  C07D497/00 ,  C07D327/02 ,  C07D339/08 ,  C07D339/00 ,  C07D321/02 ,  C07D321/12 ,  C07D319/06

    CPC分类号： C07D327/06 ,  C07D339/08 ,  C08F220/28 ,  C08F220/38 ,  G03F7/0395 ,  G03F7/0397 ,  C08F220/18 ,  C08F222/06 ,  C08F232/08

    摘要： Provided are a polymerizable compound shown below which is useful as a raw material for a polymer having less swelling in developing, a polymer obtained by polymerizing a raw material containing the above polymerizable compound, a photoresist composition which contains the above polymer and which is improved in LWR and an efficient production process for the polymerizable compound described above: wherein n represents an integer of 0 to 2; R1 represents a hydrogen atom, methyl or trifluoromethyl; R2, R3, R4, R5, R6, R7, R8, R9 and R10 represent a hydrogen atom, an alkyl group having 1 to 6 carbon atoms or the like; W represents an alkylene group having 1 to 10 carbon atoms or the like; and Y1 and Y2 represent an oxygen atom or a sulfur atom.

    摘要翻译： 提供下述可聚合化合物，其可用作显影时溶胀较小的聚合物的原料，通过聚合含有上述可聚合化合物的原料获得的聚合物，含有上述聚合物的光致抗蚀剂组合物， LWR和上述可聚合化合物的有效制备方法：其中n表示0至2的整数; R1表示氢原子，甲基或三氟甲基; R 2，R 3，R 4，R 5，R 6，R 7，R 8，R 9和R 10表示氢原子，碳原子数1〜6的烷基等; W表示碳原子数1〜10的亚烷基等; Y 1和Y 2表示氧原子或硫原子。

    METHOD FOR PRODUCING 2-ISOPROPENYL-5-METHYL-4-HEXEN-1-YL 3-METHYL-2-BUTENOATE
    9.
    发明申请
    METHOD FOR PRODUCING 2-ISOPROPENYL-5-METHYL-4-HEXEN-1-YL 3-METHYL-2-BUTENOATE 有权
    2-异丙烯基-5-甲基-4-十六烷-1-基-3-甲基-2-丁酮的制备方法

    公开(公告)号：US20090023941A1

    公开(公告)日：2009-01-22

    申请号：US11910860

    申请日：2006-03-29

    申请人： Katsuji Ujita ,  Junko Sato ,  Takashi Fukumoto

    发明人： Katsuji Ujita ,  Junko Sato ,  Takashi Fukumoto

    IPC分类号： C07C309/67 ,  C07C67/00

    CPC分类号： C07C309/66 ,  C07C67/10 ,  C07C303/28 ,  C07C69/533 ,  C07C309/73

    摘要： The present invention provides a method of producing 2-isopropenyl-5-methyl-4-hexen-1-yl 3-methyl-2-butenoate industrially advantageously in a high yield. More particularly, the present invention provides a method of producing 2-isopropenyl-5-methyl-4-hexen-1-yl 3-methyl-2-butenoate represented by the following formula (IV): which comprises reacting 2-isopropenyl-5-methyl-4-hexen-1-ol with an organic sulfonyl halide in the presence of a basic substance to give a sulfonate compound represented by the following formula (III): wherein R is a hydrocarbon group, and reacting the obtained sulfonate compound with senecionic acid in the presence of a basic substance.

    摘要翻译： 本发明提供了在工业上有利地以高产率生产2-异丙烯基-5-甲基-4-己烯-1-基3-甲基-2-丁烯酸2-乙烯酯的方法。 更具体地说，本发明提供由下式（Ⅳ）表示的2-异丙烯基-5-甲基-4-己烯-1-基3-甲基-2-丁烯酸2-乙烯酯的制备方法：其包括使2-异丙烯基-5 - 甲基-4-己烯-1-醇与有机磺酰卤在碱性物质的存在下反应，得到下式（III）表示的磺酸盐化合物：其中R是烃基，并使得到的磺酸盐化合物与 在一种碱性物质的存在下的硫氰酸。