公开(公告)号：US20120100044A1

公开(公告)日：2012-04-26

申请号：US13343249

申请日：2012-01-04

申请人： Toshiyuki Ishii ,  Eiji Komai ,  Harumi Satoh

发明人： Toshiyuki Ishii ,  Eiji Komai ,  Harumi Satoh

IPC分类号： B01J19/00

CPC分类号： C01B33/107 ,  B01J19/006 ,  B01J19/1812 ,  B01J19/1843 ,  B01J19/2415 ,  B01J19/244 ,  B01J2219/00006 ,  B01J2219/00087 ,  B01J2219/00159 ,  B01J2219/00779 ,  C01B33/10757

摘要： An apparatus 1 for manufacturing trichlorosilane includes a decomposition furnace 2 into which polymers and hydrogen chloride are introduced, the decomposition furnace 2 includes: a heating device 11 which heats an interior of the decomposition furnace 2; a reaction chamber 4 which is formed in the decomposition furnace; a center tube 3 which is inserted in the reaction chamber 4 along a longitudinal direction of the reaction chamber and has a lower-end opening portion 3a; raw-material-supply pipes 5 and 6 which supplies the polymer and the hydrogen chloride to the reaction chamber 4 at an exterior of the center tube 3; and a gas-discharge pipe 7 which leads out reacted gas from the center tube 3, the apparatus 1 further includes a fin 14 that leads the polymer and the hydrogen chloride to the lower-end opening portion 3a of the center tube 3 so as to stir the polymer and the hydrogen chloride.

摘要翻译： 用于制造三氯硅烷的装置1包括分解炉2，其中引入聚合物和氯化氢，分解炉2包括：加热分解炉2内部的加热装置11; 在分解炉中形成的反应室4; 中心管3，其沿着反应室的长度方向插入反应室4中，并具有下端开口部3a; 在中心管3的外部向反应室4供给聚合物和氯化氢的原料供给管5,6; 以及从中心管3引出反应气体的气体排出管7，装置1还包括将聚合物和氯化氢引导到中心管3的下端开口部3a的翅片14，以便 搅拌聚合物和氯化氢。

公开(公告)号：US08529844B2

公开(公告)日：2013-09-10

申请号：US13345864

申请日：2012-01-09

申请人： Toshiyuki Ishii ,  Eiji Komai ,  Harumi Satoh

发明人： Toshiyuki Ishii ,  Eiji Komai ,  Harumi Satoh

IPC分类号： B01J19/00 ,  C01B33/107

CPC分类号： C01B33/107 ,  B01J19/006 ,  B01J19/1812 ,  B01J19/1843 ,  B01J19/2415 ,  B01J19/244 ,  B01J2219/00087 ,  B01J2219/00159 ,  B01J2219/00765 ,  B01J2219/00779 ,  Y02E60/324

摘要： An apparatus for producing trichlorosilane includes: a decomposing furnace, a heating unit heating the inside of the decomposing furnace, a raw material supplying tube for guiding polymer and hydrogen chloride to be guided to the inner bottom portion of the decomposing furnace, and a gas discharge tube for discharging reaction gas from the top of the reaction chamber provided between the outer peripheral surface of the raw material supplying tube and the inner peripheral surface of the decomposing furnace, a fin, which guides a fluid mixture of the polymer and the hydrogen chloride supplied from the lower end opening of the raw material supplying tube to be agitated and rise upward in the reaction chamber, and is formed integrally with at least one of the outer peripheral surface of the raw material supplying tube and the inner peripheral surface of the decomposing furnace.

摘要翻译： 三氯硅烷的制造装置具备：分解炉，加热分解炉内部的加热单元，将导向聚合物的原料供给管和被引导到分解炉的内底部的氯化氢，以及气体排出 用于从设置在原料供给管的外周面和分解炉的内周面之间的反应室顶部排出反应气体的管，引导聚合物和供给的氯化氢的流体混合物的翅片 从原料供给管的下端开口在反应室内被搅拌上升，与原料供给管的外周面和分解炉的内周面中的至少一个一体形成 。

公开(公告)号：US20100034722A1

公开(公告)日：2010-02-11

申请号：US12461148

申请日：2009-08-03

申请人： Toshiyuki Ishii ,  Eiji Komai ,  Harumi Satoh

发明人： Toshiyuki Ishii ,  Eiji Komai ,  Harumi Satoh

IPC分类号： C01B33/107 ,  B01J8/00

CPC分类号： C01B33/107 ,  B01J19/006 ,  B01J19/1812 ,  B01J19/1843 ,  B01J19/2415 ,  B01J19/244 ,  B01J2219/00087 ,  B01J2219/00159 ,  B01J2219/00765 ,  B01J2219/00779 ,  Y02E60/324

摘要： An apparatus for producing trichlorosilane includes: a decomposing furnace, a heating unit heating the inside of the decomposing furnace, a raw material supplying tube for guiding polymer and hydrogen chloride to be guided to the inner bottom portion of the decomposing furnace, and a gas discharge tube for discharging reaction gas from the top of the reaction chamber provided between the outer peripheral surface of the raw material supplying tube and the inner peripheral surface of the decomposing furnace, a fin, which guides a fluid mixture of the polymer and the hydrogen chloride supplied from the lower end opening of the raw material supplying tube to be agitated and rise upward in the reaction chamber, and is formed integrally with at least one of the outer peripheral surface of the raw material supplying tube and the inner peripheral surface of the decomposing furnace.

摘要翻译： 三氯硅烷的制造装置具备：分解炉，加热分解炉内部的加热单元，将导向聚合物的原料供给管和被引导到分解炉的内底部的氯化氢，以及气体排出 用于从设置在原料供给管的外周面和分解炉的内周面之间的反应室顶部排出反应气体的管，引导聚合物和供给的氯化氢的流体混合物的翅片 从原料供给管的下端开口在反应室内被搅拌上升，与原料供给管的外周面和分解炉的内周面中的至少一个一体形成 。

公开(公告)号：US08187552B2

公开(公告)日：2012-05-29

申请号：US12461148

申请日：2009-08-03

申请人： Toshiyuki Ishii ,  Eiji Komai ,  Harumi Satoh

发明人： Toshiyuki Ishii ,  Eiji Komai ,  Harumi Satoh

IPC分类号： B01J19/00 ,  C01B33/107

CPC分类号： C01B33/107 ,  B01J19/006 ,  B01J19/1812 ,  B01J19/1843 ,  B01J19/2415 ,  B01J19/244 ,  B01J2219/00087 ,  B01J2219/00159 ,  B01J2219/00765 ,  B01J2219/00779 ,  Y02E60/324

摘要： An apparatus for producing trichlorosilane includes: a decomposing furnace, a heating unit heating the inside of the decomposing furnace, a raw material supplying tube for guiding polymer and hydrogen chloride to be guided to the inner bottom portion of the decomposing furnace, and a gas discharge tube for discharging reaction gas from the top of the reaction chamber provided between the outer peripheral surface of the raw material supplying tube and the inner peripheral surface of the decomposing furnace, a fin, which guides a fluid mixture of the polymer and the hydrogen chloride supplied from the lower end opening of the raw material supplying tube to be agitated and rise upward in the reaction chamber, and is formed integrally with at least one of the outer peripheral surface of the raw material supplying tube and the inner peripheral surface of the decomposing furnace.

摘要翻译： 三氯硅烷的制造装置具备：分解炉，加热分解炉内部的加热单元，将导向聚合物的原料供给管和被引导到分解炉的内底部的氯化氢，以及气体排出 用于从设置在原料供给管的外周面和分解炉的内周面之间的反应室顶部排出反应气体的管，引导聚合物和供给的氯化氢的流体混合物的翅片 从原料供给管的下端开口在反应室内被搅拌上升，与原料供给管的外周面和分解炉的内周面中的至少一个一体形成 。

公开(公告)号：US08187551B2

公开(公告)日：2012-05-29

申请号：US12461147

申请日：2009-08-03

申请人： Toshiyuki Ishii ,  Eiji Komai ,  Harumi Satoh

发明人： Toshiyuki Ishii ,  Eiji Komai ,  Harumi Satoh

IPC分类号： B01J19/00 ,  C01B33/107

CPC分类号： C01B33/107 ,  B01J19/006 ,  B01J19/1812 ,  B01J19/1843 ,  B01J19/2415 ,  B01J19/244 ,  B01J2219/00006 ,  B01J2219/00087 ,  B01J2219/00159 ,  B01J2219/00779 ,  C01B33/10757

摘要： An apparatus 1 for manufacturing trichlorosilane includes a decomposition furnace 2 into which polymers and hydrogen chloride are introduced, the decomposition furnace 2 includes: a heating device 11 which heats an interior of the decomposition furnace 2; a reaction chamber 4 which is formed in the decomposition furnace; a center tube 3 which is inserted in the reaction chamber 4 along a longitudinal direction of the reaction chamber and has a lower-end opening portion 3a; raw-material-supply pipes 5 and 6 which supplies the polymer and the hydrogen chloride to the reaction chamber 4 at an exterior of the center tube 3; and a gas-discharge pipe 7 which leads out reacted gas from the center tube 3, the apparatus 1 further includes a fin 14 that leads the polymer and the hydrogen chloride to the lower-end opening portion 3a of the center tube 3 so as to stir the polymer and the hydrogen chloride.

摘要翻译： 用于制造三氯硅烷的装置1包括分解炉2，其中引入聚合物和氯化氢，分解炉2包括：加热分解炉2内部的加热装置11; 在分解炉中形成的反应室4; 中心管3，其沿着反应室的长度方向插入反应室4中，并具有下端开口部3a; 在中心管3的外部向反应室4供给聚合物和氯化氢的原料供给管5,6; 以及从中心管3引出反应气体的气体排出管7，装置1还包括将聚合物和氯化氢引导到中心管3的下端开口部3a的翅片14，以便 搅拌聚合物和氯化氢。

公开(公告)号：US20100034721A1

公开(公告)日：2010-02-11

申请号：US12461147

申请日：2009-08-03

申请人： Toshiyuki Ishii ,  Eiji Komai ,  Harumi Satoh

发明人： Toshiyuki Ishii ,  Eiji Komai ,  Harumi Satoh

IPC分类号： C01B33/08 ,  B01J19/24

CPC分类号： C01B33/107 ,  B01J19/006 ,  B01J19/1812 ,  B01J19/1843 ,  B01J19/2415 ,  B01J19/244 ,  B01J2219/00006 ,  B01J2219/00087 ,  B01J2219/00159 ,  B01J2219/00779 ,  C01B33/10757

摘要： An apparatus 1 for manufacturing trichlorosilane includes a decomposition furnace 2 into which polymers and hydrogen chloride are introduced, the decomposition furnace 2 includes: a heating device 11 which heats an interior of the decomposition furnace 2; a reaction chamber 4 which is formed in the decomposition furnace; a center tube 3 which is inserted in the reaction chamber 4 along a longitudinal direction of the reaction chamber and has a lower-end opening portion 3a; raw-material-supply pipes 5 and 6 which supplies the polymer and the hydrogen chloride to the reaction chamber 4 at an exterior of the center tube 3; and a gas-discharge pipe 7 which leads out reacted gas from the center tube 3, the apparatus 1 further includes a fin 14 that leads the polymer and the hydrogen chloride to the lower-end opening portion 3a of the center tube 3 so as to stir the polymer and the hydrogen chloride.

摘要翻译： 用于制造三氯硅烷的装置1包括分解炉2，其中引入聚合物和氯化氢，分解炉2包括：加热分解炉2内部的加热装置11; 在分解炉中形成的反应室4; 中心管3，其沿着反应室的长度方向插入反应室4中，并具有下端开口部3a; 在中心管3的外部向反应室4供给聚合物和氯化氢的原料供给管5,6; 以及从中心管3引出反应气体的气体排出管7，装置1还包括将聚合物和氯化氢引导到中心管3的下端开口部3a的翅片14，以便 搅拌聚合物和氯化氢。

公开(公告)号：US08980191B2

公开(公告)日：2015-03-17

申请号：US13343249

申请日：2012-01-04

申请人： Toshiyuki Ishii ,  Eiji Komai ,  Harumi Satoh

发明人： Toshiyuki Ishii ,  Eiji Komai ,  Harumi Satoh

IPC分类号： B01J19/00 ,  C01B33/107 ,  B01J19/18 ,  B01J19/24

CPC分类号： C01B33/107 ,  B01J19/006 ,  B01J19/1812 ,  B01J19/1843 ,  B01J19/2415 ,  B01J19/244 ,  B01J2219/00006 ,  B01J2219/00087 ,  B01J2219/00159 ,  B01J2219/00779 ,  C01B33/10757

摘要： An apparatus 1 for manufacturing trichlorosilane includes a decomposition furnace 2 into which polymers and hydrogen chloride are introduced, the decomposition furnace 2 includes: a heating device 11 which heats an interior of the decomposition furnace 2; a reaction chamber 4 which is formed in the decomposition furnace; a center tube 3 which is inserted in the reaction chamber 4 along a longitudinal direction of the reaction chamber and has a lower-end opening portion 3a; raw-material-supply pipes 5 and 6 which supplies the polymer and the hydrogen chloride to the reaction chamber 4 at an exterior of the center tube 3; and a gas-discharge pipe 7 which leads out reacted gas from the center tube 3, the apparatus 1 further includes a fin 14 that leads the polymer and the hydrogen chloride to the lower-end opening portion 3a of the center tube 3 so as to stir the polymer and the hydrogen chloride.

摘要翻译： 用于制造三氯硅烷的装置1包括分解炉2，其中引入聚合物和氯化氢，分解炉2包括：加热分解炉2内部的加热装置11; 在分解炉中形成的反应室4; 中心管3，其沿着反应室的长度方向插入反应室4中，并具有下端开口部3a; 在中心管3的外部向反应室4供给聚合物和氯化氢的原料供给管5,6; 以及从中心管3引出反应气体的气体排出管7，装置1还包括将聚合物和氯化氢引导到中心管3的下端开口部3a的翅片14，以便 搅拌聚合物和氯化氢。

公开(公告)号：US20120213687A1

公开(公告)日：2012-08-23

申请号：US13458130

申请日：2012-04-27

申请人： Toshiyuki Ishii ,  Eiji Komai ,  Harumi Satoh ,  Tetsuya Sato

发明人： Toshiyuki Ishii ,  Eiji Komai ,  Harumi Satoh ,  Tetsuya Sato

IPC分类号： C01B33/107

CPC分类号： B01J19/006 ,  B01J19/1812 ,  B01J19/1843 ,  B01J19/2415 ,  B01J19/244 ,  B01J2219/00006 ,  B01J2219/00087 ,  B01J2219/00159 ,  B01J2219/00779 ,  C01B33/107 ,  C01B33/10757

摘要： A method for manufacturing trichlorosilane in which hydrogen chloride and polymers including high-boiling chlorosilanes generated in a polycrystalline silicon manufacture process, a trichlorosilane manufacture process, or a conversion process are introduced into a decomposition furnace and are decomposition reacted at a high temperature, the method including: heating the decomposition furnace and a fin provided in the decomposition furnace; supplying the polymers and the hydrogen chloride to the decomposition furnace from an upper portion thereof so as to react the polymers and the hydrogen chloride by leading to an inner-bottom portion of the decomposition furnace while heating and stirring; and discharging a reacted gas from the inner-bottom portion upwardly above the decomposition furnace through a center of the decomposition furnace.

摘要翻译： 制造三氯硅烷的方法，其中将氯化氢和包含在多晶硅制造方法中产生的高沸点氯硅烷的聚合物，三氯硅烷制造方法或转化方法引入分解炉中并在高温下分解反应， 包括：加热分解炉和分解炉中设置的翅片; 从聚合物的上部向分解炉供给聚合物和氯化氢，使其在加热搅拌下通过导入分解炉的内底部而使聚合物和氯化氢反应; 并通过分解炉的中心将内反应气体从分解炉的上方向上排出。

公开(公告)号：US20120107190A1

公开(公告)日：2012-05-03

申请号：US13345864

申请日：2012-01-09

申请人： Toshiyuki Ishii ,  Eiji Komai ,  Harumi Satoh

发明人： Toshiyuki Ishii ,  Eiji Komai ,  Harumi Satoh

IPC分类号： B01J19/00 ,  B01J19/18

CPC分类号： C01B33/107 ,  B01J19/006 ,  B01J19/1812 ,  B01J19/1843 ,  B01J19/2415 ,  B01J19/244 ,  B01J2219/00087 ,  B01J2219/00159 ,  B01J2219/00765 ,  B01J2219/00779 ,  Y02E60/324

摘要： An apparatus for producing trichlorosilane includes: a decomposing furnace, a heating unit heating the inside of the decomposing furnace, a raw material supplying tube for guiding polymer and hydrogen chloride to be guided to the inner bottom portion of the decomposing furnace, and a gas discharge tube for discharging reaction gas from the top of the reaction chamber provided between the outer peripheral surface of the raw material supplying tube and the inner peripheral surface of the decomposing furnace, a fin, which guides a fluid mixture of the polymer and the hydrogen chloride supplied from the lower end opening of the raw material supplying tube to be agitated and rise upward in the reaction chamber, and is formed integrally with at least one of the outer peripheral surface of the raw material supplying tube and the inner peripheral surface of the decomposing furnace.

摘要翻译： 三氯硅烷的制造装置具备：分解炉，加热分解炉内部的加热单元，将导向聚合物的原料供给管和被引导到分解炉的内底部的氯化氢，以及气体排出 用于从设置在原料供给管的外周面和分解炉的内周面之间的反应室顶部排出反应气体的管，引导聚合物和供给的氯化氢的流体混合物的翅片 从原料供给管的下端开口在反应室内被搅拌上升，与原料供给管的外周面和分解炉的内周面中的至少一个一体形成 。

公开(公告)号：US10370465B2

公开(公告)日：2019-08-06

申请号：US12448983

申请日：2008-01-17

申请人： Keita Itakura ,  Toshiyuki Ishii ,  Rikuo Onishi ,  Satoshi Hashizume

发明人： Keita Itakura ,  Toshiyuki Ishii ,  Rikuo Onishi ,  Satoshi Hashizume

IPC分类号： C08L23/12 ,  C08F110/06 ,  C08F4/659 ,  C08K7/14 ,  C08L23/16

摘要： Propylene polymers and propylene resin compositions containing the polymers are used as molded articles used under stress for a long period such as automotive parts, housing parts, home appliance parts and electric power tool parts. Stress-resistant molded articles of the invention are obtained from these materials. A propylene homopolymer (A) satisfies the following requirements (1) to (3), and a polypropylene resin composition contains the propylene homopolymer (A). (1) The ratio (Mw/Mn) of weight average molecular weight (Mw) to number average molecular weight (Mn) according to GPC is in the range of 1.2 to 3.5. (2) Mn is in the range of 35,000 to 400,000. (3) The content of components soluble in o-dichlorobenzene at 90° C. is not more than 4 wt %.