Process of producing copper phthalocyanine pigment having a bright tone
    1.
    发明授权
    Process of producing copper phthalocyanine pigment having a bright tone 失效
    具有亮色调的铜酞菁颜料的制造方法

    公开(公告)号:US5698023A

    公开(公告)日:1997-12-16

    申请号:US617154

    申请日:1996-03-18

    CPC分类号: C09B47/06 C09B47/067

    摘要: This invention provides a process for producing copper phthalocyanine pigments which comprises reacting either phthalic anhydride or its derivatives with urea and a copper-containing substance, or either phthalonitrile or its derivative with a copper-containing substance in a reaction solvent by heating characterized in that an alkylxylene ingredient having a branched C4 side-chain represented by the following formula (1) is used as the reaction solvent: ##STR1##

    摘要翻译: 本发明提供了一种生产铜酞菁颜料的方法,其包括使邻苯二甲酸酐或其衍生物与脲和含铜物质或邻苯二甲腈或其衍生物与含铜物质在反应溶剂中通过加热反应,其特征在于, 使用具有由下式(1)表示的支链C 4侧链的烷基二甲苯成分作为反应溶剂:(1)

    Electrical insulating oil composition and capacitors prepared therewith
    2.
    发明授权
    Electrical insulating oil composition and capacitors prepared therewith 失效
    电绝缘油组合物和电容器

    公开(公告)号:US5081757A

    公开(公告)日:1992-01-21

    申请号:US697197

    申请日:1991-05-08

    IPC分类号: H01B3/22 H01B3/44

    CPC分类号: H01B3/44 H01B3/22 Y10T29/43

    摘要: An electrical insulating oil composition having good low temperature characteristics which comprises at least 4 members selected from the group consisting of (a) m-ethylbiphenyl, (b) p-ethylbiphenyl, (c) o-benzyltoluene, (d) m-benzyltoluene, (e) p-benzyltoluene, (f) 1,1-diphenylethane, and (g) 1,1-diphenylethylene; and is characterized in that the proportion of solid phase at a temperature of -40.degree. C. of the electrical insulating oil composition is not more than 45% by weight and the proportion of the total quantity of solid phase is calculated according to the following general equation of solid-liquid equilibrium: ##EQU1## wherein X.sub.i is the equilibrium mole fraction of a component i in the liquid phase of the composition, .DELTA.H.sub.i.sup.f is the heat of fusion (cal.mol.sup.-1), T.sub.i.sup.f is the melting point (K), T is the temperature (K), and R is the gas constant (cal.mol.sup.-1.K.sup.-1).Electrical capacitors prepared with these electrical insulating oil compositions provide excellent operation at temperatures as low as -40.degree. C., preferably as low as -50.degree. C.

    METHOD FOR PRODUCTION OF CAROTENOID
    4.
    发明申请
    METHOD FOR PRODUCTION OF CAROTENOID 审中-公开
    生产CAROTENOID的方法

    公开(公告)号:US20100291251A1

    公开(公告)日:2010-11-18

    申请号:US12675174

    申请日:2008-08-29

    IPC分类号: A61K35/00 A23L1/48

    摘要: The present invention provides a composition comprising a high content of highly pure, low-cost, and safe carotenoid and a method for industrially producing the same. The present invention also provides functional food, a pharmaceutical composition and a cosmetic product comprising such a composition. The present invention further provides a method for producing a composition containing at least 80% of carotenoid, which is characterized in treating a microorganism culture with extraction using a lower alcohol at 80° C. at the lowest or a combination of water and a lower alcohol at 80° C. at the lowest, and then washing and filtrating the precipitate obtained from the extract solution with a combination of a lower alcohol and water.

    摘要翻译: 本发明提供包含高含量的高纯度,低成本和安全的类胡萝卜素的组合物及其工业生产方法。 本发明还提供功能食品,药物组合物和包含这种组合物的化妆品。 本发明还提供一种制备含有至少80%的类胡萝卜素的组合物的方法,其特征在于在80℃下使用低级醇或最低水或低级醇的组合处理微生物培养物 在最低的80℃下,然后用低级醇和水的组合洗涤并过滤从萃取液中得到的沉淀物。

    Apparatus and method for filling and impregnating capacitors with a
capacitor oil
    5.
    发明授权
    Apparatus and method for filling and impregnating capacitors with a capacitor oil 失效
    用电容器油填充和印制电容器的装置和方法

    公开(公告)号:US5241997A

    公开(公告)日:1993-09-07

    申请号:US747266

    申请日:1991-08-19

    IPC分类号: H01G4/22 H01G13/04

    CPC分类号: H01G13/04

    摘要: A plurality of capacitors of the type each including capacitor elements with a very small gap between adjacent electrodes are filled and impregnated with a capacitor oil with the aid of a capacitor oil filling/impregnating apparatus. The apparatus comprises an impregnating chamber including a capacitor oil supplying portion, a charging/discharging platform having a plurality of capacitors placed thereon, and distributing/supplying means arranged above the charging/discharging platform so as to allow the capacitor oil to be supplied to the respective capacitors from above by its free falling-down induced by a dead weight of the capacitor oil itself. A capacitor oil filling/impregnating method is practiced with the aid of the foregoing apparatus by way of the steps of heating the interior of the impregnating chamber under a high level of vacuum to dry the respective capacitors on the charging/discharging platform, cooling the capacitors after completion of the drying operation, supplying the capacitor oil to each capacitor from a capacitor oil refining/supplying system via the capacitor oil supplying portion, keeping the capacitors still for a predetermined period of time after completion of the capacitor oil supplying operation, and allowing the capacitors to be impregnated with the capacitor oil.

    Method for preparing diarylalkanes

    公开(公告)号:US07022887B2

    公开(公告)日:2006-04-04

    申请号:US10267470

    申请日:2002-10-09

    申请人: Hideyuki Dohi

    发明人: Hideyuki Dohi

    IPC分类号: C07C2/66

    CPC分类号: C07C2/66 C07C15/18

    摘要: Diarylalkanes are prepared by alkylating an aromatic compound with a styrene derivative in the presence of a catalyst of specific synthetic porous crystalline material. The aromatic compound can be, for example, benzene, toluene, xylene, ethylbenzene, cumene, etc. The styrene derivative can be, for example, styrene, methylstyrene or the like.

    Method for producing diarylmethane
    7.
    发明授权
    Method for producing diarylmethane 失效
    二芳基甲烷的制备方法

    公开(公告)号:US5880322A

    公开(公告)日:1999-03-09

    申请号:US988829

    申请日:1997-12-11

    IPC分类号: C07C2/86 C07C1/20 C07C2/66

    CPC分类号: C07C2/867 C07C2529/06

    摘要: A method for producing diarylalkanes at a high yield using an aromatic hydrocarbon and inexpensive formalin in the presence of an easily usable solid acid catalyst, and in the method, a mixture of an aromatic hydrocarbon and formalin, said mixture containing 1.5 to 12% by weight of water, is reacted at a temperature of 170 to 450.degree. C. under an elevated pressure in the presence of a zeolitic catalyst.

    摘要翻译: 在易于使用的固体酸催化剂的存在下,使用芳烃和廉价的福尔马林,以高收率生产二芳基烷烃的方法,在该方法中,芳族烃和福尔马林的混合物,所述混合物含有1.5-12重量% 的水在170-450℃的温度下在升高的压力下在沸石催化剂存在下反应。

    Electrical insulating oil composition and capacitors prepared therewith
    9.
    发明授权
    Electrical insulating oil composition and capacitors prepared therewith 失效
    电绝缘油组合物和电容器

    公开(公告)号:US5134761A

    公开(公告)日:1992-08-04

    申请号:US697199

    申请日:1991-05-08

    IPC分类号: H01B3/22 H01B3/44

    CPC分类号: H01B3/22 H01B3/44 Y10T29/43

    摘要: A new electrical insulating oil composition having improved low temperature characteristics which composition comprises a mixture of 40% by weight or more of benzyltoluene and the remainder of alkyl substituted diphenylmethane having 15 to 17 carbon atoms which is represented by the following general formula: ##STR1## wherein R.sub.1 and R.sub.2 are C.sub.1 to C.sub.4 alkyl groups and the total number of carbon atoms in R.sub.1 and R.sub.2 is 1 to 4, except that R.sub.1 and R.sub.2 are simultaneously methyl groups; and the proportion of the total quantity of solid phase calculated according to the following general solid-liquid equilibrium equation is 45% by weight or less relative to the total quantity of said composition at -40.degree. C.: ##EQU1## wherein X.sub.i is the equilibrium mole fraction of a component i, in the liquid phase, .DELTA.H.sub.i.sup.f is the heat of fusion (cal.mol.sup.-1), T.sub.i.sup.f is the melting point (K), T is the temperature (K) of the system, and R is the gas constant (cal.mol.sup.-1.K.sup.-1). Electrical capacitors prepared with these electrical insulating oil compositions provide excellent operation at temperatures as low as -40.degree. C., preferably as low as -50.degree. C.

    摘要翻译: 一种具有改进的低温特性的新的电绝缘油组合物,其组合物包含40重量%或更多的苄基甲苯和其余的具有15至17个碳原子的烷基取代的二苯基甲烷的混合物,其由以下通式表示: 其中R1和R2是C1-C4烷基,R1和R2中的总碳原子数为1〜4,除了R1和R2同时为甲基; 并且根据以下一般固 - 液平衡方程计算的固相总量的比例相对于所述组合物在-40℃下的总量为45重量%以下:其中,Xi为 组分i的平衡摩尔分数,在液相中,DELTA Hif是熔解热(cal.mol-1),Tif是熔点(K),T是系统的温度(K),R 是气体常数(cal.mol-1.K-1)。 使用这些电绝缘油组合物制备的电容器在低至-40℃,优选低至-50℃的温度下提供优异的操作。

    Electrical insulating oil composition
    10.
    发明授权
    Electrical insulating oil composition 失效
    电绝缘油组成

    公开(公告)号:US5017733A

    公开(公告)日:1991-05-21

    申请号:US93813

    申请日:1987-09-04

    IPC分类号: H01B3/22 H01B3/44 H01G4/22

    摘要: An electrical insulating oil composition which comprises 45% by weight or more of at least 2 members selected from the group consisting of (a) m-ethylbiphenyl, (b) p-ethylbiphenyl, (c) o-benzyltoluene, (d) m-benzyltoluene, (e) p-benzyltoluene, and (f) 1,1-diphenylethane; and the remainder of non-condensed bicyclic aromatic hydrocarbons having not more than 17 carbon atoms besides the above 6 components; and is characterized in that, when the temperature of the composition is -40.degree. C., (I) the total quantity of solid phase obtained by calculating according to the following solid-liquid equilibrium equation is 45% by weight or less relative to the total quantity of the composition, and (II) in the liquid phase composition calculated by the following solid-liquid equilibrium equation, the total quantity of the compounds (a) to (f) is 40% by weight or more and the viscosity of this liquid phase is 500 cSt or lower, ##EQU1## wherein X.sub.i is the equilibrium mole fraction of a component i in the liquid phase; .DELTA.H.sub.i.sup.f is a heat of fusion (cal.mol.sup.-1); T.sub.i.sup.f is a meltinig point (K); T is the temperature (K); and R is the gas constant (cal.mol.sup.-1.K.sup.-1).

    摘要翻译: 一种电绝缘油组合物,其包含45重量%以上至少2个选自(a)间 - 乙基联苯,(b)对乙基联苯,(c)邻 - 苄基甲苯,(d) 苄基甲苯,(e)对 - 苄基甲苯和(f)1,1-二苯基乙烷; 除了上述6种成分之外,剩余的具有不超过17个碳原子的非稠合双环芳烃; 其特征在于,当组合物的温度为-40℃时,(I)通过根据以下固液平衡方程式计算获得的固相的总量相对于下述固体 - 液体平衡方程为45重量%以下 组合物的总量和(II)在以下固体 - 液体平衡方程式计算的液相组合物中,化合物(a)至(f)的总量为40重量%以上,并且其粘度 液相500cSt或更低,其中Xi是液相中组分i的平衡摩尔分数; DELTA Hif是融合热(cal.mol-1); Tif是一个融合点(K); T是温度(K); R为气体常数(cal.mol-1.K-1)。