摘要:
This invention provides a process for producing copper phthalocyanine pigments which comprises reacting either phthalic anhydride or its derivatives with urea and a copper-containing substance, or either phthalonitrile or its derivative with a copper-containing substance in a reaction solvent by heating characterized in that an alkylxylene ingredient having a branched C4 side-chain represented by the following formula (1) is used as the reaction solvent: ##STR1##
摘要:
An electrical insulating oil composition having good low temperature characteristics which comprises at least 4 members selected from the group consisting of (a) m-ethylbiphenyl, (b) p-ethylbiphenyl, (c) o-benzyltoluene, (d) m-benzyltoluene, (e) p-benzyltoluene, (f) 1,1-diphenylethane, and (g) 1,1-diphenylethylene; and is characterized in that the proportion of solid phase at a temperature of -40.degree. C. of the electrical insulating oil composition is not more than 45% by weight and the proportion of the total quantity of solid phase is calculated according to the following general equation of solid-liquid equilibrium: ##EQU1## wherein X.sub.i is the equilibrium mole fraction of a component i in the liquid phase of the composition, .DELTA.H.sub.i.sup.f is the heat of fusion (cal.mol.sup.-1), T.sub.i.sup.f is the melting point (K), T is the temperature (K), and R is the gas constant (cal.mol.sup.-1.K.sup.-1).Electrical capacitors prepared with these electrical insulating oil compositions provide excellent operation at temperatures as low as -40.degree. C., preferably as low as -50.degree. C.
摘要:
A method for producing m-benzyltoluene with a high yield and excellent selectivity without producing undesirable heavier by-products. The method is characterized in that toluene and diphenylmethane are allowed to react at a reaction temperature in the range of 170.degree. to 400.degree. C. in the presence of a crystalline synthetic zeolite catalyst in which the molar ratio of SiO.sub.2 /Al.sub.2 O.sub.3 is 20 or higher and the openings of main pores are formed by ten-membered oxygen rings.
摘要:
The present invention provides a composition comprising a high content of highly pure, low-cost, and safe carotenoid and a method for industrially producing the same. The present invention also provides functional food, a pharmaceutical composition and a cosmetic product comprising such a composition. The present invention further provides a method for producing a composition containing at least 80% of carotenoid, which is characterized in treating a microorganism culture with extraction using a lower alcohol at 80° C. at the lowest or a combination of water and a lower alcohol at 80° C. at the lowest, and then washing and filtrating the precipitate obtained from the extract solution with a combination of a lower alcohol and water.
摘要:
A plurality of capacitors of the type each including capacitor elements with a very small gap between adjacent electrodes are filled and impregnated with a capacitor oil with the aid of a capacitor oil filling/impregnating apparatus. The apparatus comprises an impregnating chamber including a capacitor oil supplying portion, a charging/discharging platform having a plurality of capacitors placed thereon, and distributing/supplying means arranged above the charging/discharging platform so as to allow the capacitor oil to be supplied to the respective capacitors from above by its free falling-down induced by a dead weight of the capacitor oil itself. A capacitor oil filling/impregnating method is practiced with the aid of the foregoing apparatus by way of the steps of heating the interior of the impregnating chamber under a high level of vacuum to dry the respective capacitors on the charging/discharging platform, cooling the capacitors after completion of the drying operation, supplying the capacitor oil to each capacitor from a capacitor oil refining/supplying system via the capacitor oil supplying portion, keeping the capacitors still for a predetermined period of time after completion of the capacitor oil supplying operation, and allowing the capacitors to be impregnated with the capacitor oil.
摘要:
Diarylalkanes are prepared by alkylating an aromatic compound with a styrene derivative in the presence of a catalyst of specific synthetic porous crystalline material. The aromatic compound can be, for example, benzene, toluene, xylene, ethylbenzene, cumene, etc. The styrene derivative can be, for example, styrene, methylstyrene or the like.
摘要:
A method for producing diarylalkanes at a high yield using an aromatic hydrocarbon and inexpensive formalin in the presence of an easily usable solid acid catalyst, and in the method, a mixture of an aromatic hydrocarbon and formalin, said mixture containing 1.5 to 12% by weight of water, is reacted at a temperature of 170 to 450.degree. C. under an elevated pressure in the presence of a zeolitic catalyst.
摘要:
A method for producing diphenylmethane from 1,1-diphenylethane with a high yield and selectivity, wherein the 1,1-diphenylethane is reacted with hydrogen and/or water.
摘要:
A new electrical insulating oil composition having improved low temperature characteristics which composition comprises a mixture of 40% by weight or more of benzyltoluene and the remainder of alkyl substituted diphenylmethane having 15 to 17 carbon atoms which is represented by the following general formula: ##STR1## wherein R.sub.1 and R.sub.2 are C.sub.1 to C.sub.4 alkyl groups and the total number of carbon atoms in R.sub.1 and R.sub.2 is 1 to 4, except that R.sub.1 and R.sub.2 are simultaneously methyl groups; and the proportion of the total quantity of solid phase calculated according to the following general solid-liquid equilibrium equation is 45% by weight or less relative to the total quantity of said composition at -40.degree. C.: ##EQU1## wherein X.sub.i is the equilibrium mole fraction of a component i, in the liquid phase, .DELTA.H.sub.i.sup.f is the heat of fusion (cal.mol.sup.-1), T.sub.i.sup.f is the melting point (K), T is the temperature (K) of the system, and R is the gas constant (cal.mol.sup.-1.K.sup.-1). Electrical capacitors prepared with these electrical insulating oil compositions provide excellent operation at temperatures as low as -40.degree. C., preferably as low as -50.degree. C.
摘要:
An electrical insulating oil composition which comprises 45% by weight or more of at least 2 members selected from the group consisting of (a) m-ethylbiphenyl, (b) p-ethylbiphenyl, (c) o-benzyltoluene, (d) m-benzyltoluene, (e) p-benzyltoluene, and (f) 1,1-diphenylethane; and the remainder of non-condensed bicyclic aromatic hydrocarbons having not more than 17 carbon atoms besides the above 6 components; and is characterized in that, when the temperature of the composition is -40.degree. C., (I) the total quantity of solid phase obtained by calculating according to the following solid-liquid equilibrium equation is 45% by weight or less relative to the total quantity of the composition, and (II) in the liquid phase composition calculated by the following solid-liquid equilibrium equation, the total quantity of the compounds (a) to (f) is 40% by weight or more and the viscosity of this liquid phase is 500 cSt or lower, ##EQU1## wherein X.sub.i is the equilibrium mole fraction of a component i in the liquid phase; .DELTA.H.sub.i.sup.f is a heat of fusion (cal.mol.sup.-1); T.sub.i.sup.f is a meltinig point (K); T is the temperature (K); and R is the gas constant (cal.mol.sup.-1.K.sup.-1).