Process for preparing perylene-3,4,9,10-tetracarboxylic diimide in transparent pigment form
    10.
    发明授权
    Process for preparing perylene-3,4,9,10-tetracarboxylic diimide in transparent pigment form 有权
    以透明颜料形式制备苝-3,4,9,10-四羧酸二酰亚胺的方法

    公开(公告)号:US06521756B2

    公开(公告)日:2003-02-18

    申请号:US09777211

    申请日:2001-02-05

    IPC分类号: C07D47106

    CPC分类号: C09B5/62 C09B67/0022

    摘要: The present invention provides a process for preparing transparent perylimide pigments of the formula (I) in which u is a number from 0 to 8 and, if u>0, E is a chlorine or bromine atom and, where u>1, may be a combination thereof, which comprises wet-grinding a crude perylimide pigment in a liquid medium in a stirred ballmill operated at a power density of from 1.0 kW per liter of milling space and at a stirrer tip speed of more than 12 m/s under the action of grinding media having a diameter of less than or equal to 0.9 mm, and isolating the resulting pigment.

    摘要翻译: 本发明提供制备式(I)的透明苝酰亚胺颜料的方法,其中0至8的数,如果u> 0,E是氯或溴原子,并且其中u> 1可以是 其组合包括在搅拌球磨机中在液体介质中湿法研磨粗己二酰亚胺颜料,该搅拌球磨机以每升研磨空间的功率密度为1.0kW,搅拌器末端速度大于12m / s 的直径小于或等于0.9mm的研磨介质,并分离所得颜料。