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公开(公告)号：US4169705A
公开(公告)日：1979-10-02
申请号：US862428
申请日：1977-12-20
CPC分类号： D06P3/36 , D06P3/8238 , Y10S534/01
摘要： Process for the continuous coloration of aromatic polyester or cellulose triacetate textile materials and of unions of aromatic polyester with cellulose, by applying to the textile material for the polyester or triacetate a disperse azo dyestuff containing a single carboxylic acid ester group and at least two cyano groups, and for the cellulose component of a union a reactive or other dyestuff, followed by an alkaline rinse of the colored textile material.
摘要翻译： 通过将用于聚酯或三乙酸酯的纺织材料应用于含有单一羧酸酯基和至少两个氰基的分散偶氮染料，芳族聚酯或三乙酸纤维素纤维素纺织材料和芳族聚酯与纤维素的连接的连续着色的方法 ，并且对于联合体的纤维素组分为反应性或其它染料，接着是着色纺织材料的碱性漂洗。
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公开(公告)号：US4313874A
公开(公告)日：1982-02-02
申请号：US784330
申请日：1977-04-04
申请人： Violet Boyd , Brian R. Fishwick , Brian Glover
发明人： Violet Boyd , Brian R. Fishwick , Brian Glover
IPC分类号： C09B29/06 , C09B29/01 , C09B29/08 , C09B29/085 , C07C107/06 , C09B29/26
CPC分类号： C09B29/0003 , C09B29/08 , C09B29/0817
摘要： Disperse monoazo dyestuffs of the formula: ##STR1## wherein X is lower alkyl, n is 1, 2 or 3, Z is hydrogen, lower alkyl or lower alkoxy, Y is hydrogen, lower alkyl, lower alkoxy, chlorine, bromine, --NHCOX.sup.1 or --NHSO.sub.2 X.sup.2, X.sup.1 is lower alkyl, lower alkoxy, amino or N-lower alkylamino, X.sup.2 is lower alkyl, A.sup.1 and A.sup.2 are each independently lower alkylene, and R.sup.2 and R.sup.3 are each independently lower alkyl or hydroxyalkyl containing from 2 to 4 carbon atoms, together with a process of manufacture and the use of such dyestuffs for the coloration of synthetic polymeric materials particularly polyesters.
摘要翻译： 分散单偶氮染料，其分子式如下：其中X为低级烷基，n为1,2或3，Z为氢，低级烷基或低级烷氧基，Y为氢，低级烷基，低级烷氧基，氯，溴，-NHCOX1 或-NHSO 2 X 2，X 1为低级烷基，低级烷氧基，氨基或N-低级烷基氨基，X 2为低级烷基，A 1和A 2各自为低级亚烷基，R 2和R 3各自为含2-4个碳原子的低级烷基或羟烷基 原子，以及制造方法和使用这种染料来着色合成聚合物材料，特别是聚酯。
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公开(公告)号：US4153413A
公开(公告)日：1979-05-08
申请号：US862300
申请日：1977-12-19
摘要： Process for the continuous coloration of aromatic polyester or cellulose triacetate textile materials and of unions of aromatic polyester with cellulose, by applying to the textile material for the polyester or triacetate a disperse azo dyestuff containing a single carboxylic acid ester group and at least one group selected from primary, secondary or tertiary sulphamoyl or carbamoyl; imido (especially phthalimido), hydroxy, acyloxy, sulphone (especially alkylsulphonyl) and lactone groups, and for the cellulose component of a union a reactive or other dyestuff, followed by an alkaline rinse of the colored textile material.
摘要翻译： 芳族聚酯或三乙酸纤维素纤维素纺织材料和芳族聚酯与纤维素的连接物连续着色的方法，通过将聚酯或三乙酸酯的纺织材料应用于含有单个羧酸酯基团和至少一个选自下列的基团的分散偶氮染料 来自伯，仲或叔氨磺酰基或氨基甲酰基; 亚胺基（特别是邻苯二甲酰亚氨基），羟基，酰氧基，砜（特别是烷基磺酰基）和内酯基团，以及用于反应性或其它染料的联合的纤维素组分，然后是着色纺织材料的碱性漂洗。
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公开(公告)号：US4254027A
公开(公告)日：1981-03-03
申请号：US698584
申请日：1976-06-21
申请人： Violet Boyd , Brian R. Fishwick , Brian Glover
发明人： Violet Boyd , Brian R. Fishwick , Brian Glover
IPC分类号： C09B29/01 , C09B29/08 , C07C107/06 , C09B29/085 , C09B29/26
CPC分类号： C09B29/08 , C09B29/0003 , C09B29/0817
摘要： The disperse monoazo dyestuffs of the formula: ##STR1## wherein T.sup.1 and T.sup.2 are each independently hydrogen or lower alkyl, Z is hydrogen, lower alkyl, or lower alkoxy, Y is hydrogen, lower alkyl, lower alkoxy, chlorine, bromine, --NHCOX.sup.1 or --NHSO.sub.2 X.sup.2, X.sup.1 is lower alkyl, lower alkoxy, amino or N-lower alkylamino, X.sup.2 is lower alkyl, A.sup.1 and A.sup.2 are each independently lower alkylene, R.sup.1 and R.sup.2 are each independently lower alkyl or hydroxyalkyl containing from 2 to 4 carbon atoms, and the benzene ring B can contain additional susbstituents apart from sulphonic acid groups, a process for the manufacture of the said dyestuffs, and their use for coloring synthetic textile materials in yellow to blue shades.
摘要翻译： 下式的分散单偶氮染料其中T1和T2各自独立地为氢或低级烷基，Z为氢，低级烷基或低级烷氧基，Y为氢，低级烷基，低级烷氧基，氯，溴，-NHCOX1 或-NHSO 2 X 2，X 1是低级烷基，低级烷氧基，氨基或N-低级烷基氨基，X 2是低级烷基，A 1和A 2各自独立地是低级亚烷基，R 1和R 2各自独立地是含有2至4个碳原子的低级烷基或羟烷基 ，苯环B可以含有除磺酸基以外的其他成分，制造所述染料的方法，以及它们用于将合成纺织材料着色成黄色至蓝色的用途。
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公开(公告)号：US4134723A
公开(公告)日：1979-01-16
申请号：US847492
申请日：1977-11-01
申请人： Violet Boyd , Brian R. Fishwick , Brian Glover
发明人： Violet Boyd , Brian R. Fishwick , Brian Glover
CPC分类号： C09B29/363 , C09B29/0003 , D06P3/54 , D06P3/8219 , D06P3/8238 , D06P5/02
摘要： A process for the coloration of aromatic polyester textile materials which comprises applying to the said textile materials by an aqueous dyeing, padding or printing process a disperse monoazo dyestuff, free from carboxylic acid and sulphonic acid groups, which, in one of the possible tautomeric forms, is represented by the formula: ##STR1## wherein A is phenyl or phenyl which contains at least one substituent selected from chlorine, bromine, nitro, cyano, trifluoromethyl, thiocyano, lower alkyl, lower alkoxy, lower alkylcarbonyl, lower alkylsulphonyl, lower alkylcarbonylamino, carbamoyl and N-lower alkyl and N:N-di lower alkyl derivatives thereof, sulphamoyl and N-lower alkyl and N:N-di lower alkyl derivatives thereof, sulphamato and N-lower alkyl and N:N-di lower alkyl derivatives thereof, lower alkoxycarbonyl, lower alkoxy lower alkoxycarbonyl, lower alkoxy lower alkoxy lower alkoxycarbonyl, hydroxy lower alkoxycarbonyl, hydroxy lower alkoxy lower alkoxycarbonyl, and lower alkoxycarbonyl lower alkyl.X is hydrogen, lower alkyl, carbamoyl, cyano, chlorine, bromine, nitroso, nitro, lower alkylcarbonyl, sulphamoyl, lower alkylsulphonyl, lower alkylcarbonylamino or lower alkoxycarbonyl; andZ is hydrogen or lower alkyl;And subsequently giving the colored textile material a treatment in an aqueous alkaline bath at a pH above 8 and at a temperature between 50.degree. and 85.degree. C, whereby the textile materials are colored in greenish-yellow to red shades possessing excellent fastness properties.
摘要翻译： 一种用于着色芳族聚酯纺织材料的方法，其包括通过水性染色，填充或印刷方法将所述纺织材料施加到不含羧酸和磺酸基团的分散单偶氮染料中，所述分散单偶氮染料以可能的互变异构形式之一 其中A是苯基或苯基，其含有至少一个选自氯，溴，硝基，氰基，三氟甲基，硫代氰基，低级烷基，低级烷氧基，低级烷基羰基，低级烷基磺酰基，低级烷基羰基氨基 ，氨基甲酰基和N-低级烷基和N：N-二低级烷基衍生物，氨磺酰基和N-低级烷基及其N，N-二低级烷基衍生物，磺酰胺和N-低级烷基和N：N-二低级烷基衍生物 低级烷氧基羰基，低级烷氧基低级烷氧基羰基，低级烷氧基低级烷氧基低级烷氧基羰基，羟基低级烷氧基羰基，羟基低级烷氧基低级烷氧基羰基和低级烷氧基羰基 丁基低级烷基。
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6.发明授权Process for coloring aromatic polyester-cellulose unions with a reactive dyestuff and a disperse dyestuff containing at least two carboxylic acid ester groups 失效用活性染料和含有至少两个羧酸酯基的分散染料着色芳族聚酯 - 纤维素结合剂的方法
公开(公告)号：US3993438A
公开(公告)日：1976-11-23
申请号：US564899
申请日：1975-04-03
IPC分类号： C09B29/085 , C09B1/26 , C09B29/08 , C09B62/00 , C09B69/00 , D06P1/18 , D06P3/66 , D06P3/82 , D06P3/872 , D06P5/02
CPC分类号： D06P1/18 , C09B1/26 , C09B29/08 , C09B29/0816 , C09B62/00 , C09B69/00 , D06P3/66 , D06P3/8252 , Y10S8/922 , Y10S8/933 , Y10S8/937
摘要： An improved process for the continuous coloration of aromatic polyester/cellulose unions which comprises continuously applying to the said unions a reactive dyestuff and a disperse dyestuff containing at least two carboxylic acid ester groups, fixing the dyestuffs on the union, and thereafter subjecting the colored union to a treatment in an aqueous alkaline bath at a pH above 8.0 and at a temperature between 50.degree. and 85.degree. C, whereby the unions are padded or printed in a wide variety of shades possessing excellent fastness properties and there is little or no staining of any unprinted areas of the unions.
摘要翻译： 一种用于连续着色芳族聚酯/纤维素接头的改进方法，其包括连续地向所述接合体施加活性染料和含有至少两个羧酸酯基团的分散染料，将染料固定在接头上，然后使着色接合体 在pH 8.0以上，温度在50℃〜85℃之间的碱性水溶液中进行处理，由此将各种各样的色调填充或印刷，具有优异的牢固性，并且几乎没有染色 任何未印刷的工会区域。
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公开(公告)号：US4030881A
公开(公告)日：1977-06-21
申请号：US620694
申请日：1975-10-08
IPC分类号： D06P1/16 , C09B29/42 , D06P3/48 , D06P3/54 , D06P3/85 , D06P5/02 , D06P5/10 , C09B1/00 , C09B5/62
摘要： Process for the coloration of aromatic polyester or cellulose triacetate textile materials which comprises applying to the said textile material by an aqueous dyeing, padding or printing process a disperse dyestuff which contains at least two carboxylic acid ester groups and subsequently giving the colored textile material a treatment in an aqueous solution of an alkali having a pH above 8 and at a temperature between 50.degree. and 85.degree. C, whereby the textile materials are colored in a wide variety of shades possessing very good to excellent fastness properties.
摘要翻译： 用于着色芳族聚酯或三醋酸纤维素纺织材料的方法，其包括通过水性染色，填充或印刷方法施加到所述纺织材料上的分散染料，所述分散染料含有至少两个羧酸酯基团，并随后将着色纺织材料给予处理 在pH高于8且温度在50至85℃之间的碱的水溶液中，由此纺织材料以各种各样的色调着色，具有非常好至优异的牢度性能。
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公开(公告)号：US4029469A
公开(公告)日：1977-06-14
申请号：US620692
申请日：1975-10-08
CPC分类号： D06P5/10 , C09B29/08 , C09B29/0817 , C09B29/363 , D06P3/48 , D06P3/54 , Y10S8/922
摘要： Process for coloring aromatic polyester textile materials which comprises applying to the said textile material by an aqueous dyeing, padding or printing process an aqueous dispersion of a water-insoluble monoazo dyestuff of the formula:- ##STR1## wherein X is hydrogen or methyl, Y and Z are each independently chlorine or bromine, and R is lower alkyl, and subsequently subjecting the colored textile material to a treatment in an aqueous solution of sodium hydrosulphite whereby the aromatic polyester textile materials are colored in brown shades of excellent fastness properties.
摘要翻译： 用于着色芳族聚酯纺织材料的方法，其包括通过水性染色，填充或印刷方法将所述纺织材料施用于下式的水不溶性单偶氮染料的水分散体：其中X是氢或甲基，Y 和Z各自独立地为氯或溴，R为低级烷基，随后将着色纺织品进行在亚硫酸氢钠水溶液中的处理，由此使芳族聚酯纺织品以具有优异坚牢性的棕色色调着色。
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公开(公告)号：US4119624A
公开(公告)日：1978-10-10
申请号：US567404
申请日：1975-04-11
IPC分类号： C09B29/08
摘要： The disperse monoazo dyestuffs of the formula:- ##STR1## wherein U is hydrogen, chlorine, bromine, cyano, lower alkyl, lower alkoxy or a group of the formula --CONT.sup.1 T.sup.2, --COOT.sup.3 or --SO.sub.2 T.sup.3 ;V is hydrogen, chlorine, bromine, cyano or lower alkoxycarbonyl;W is hydrogen, cyano, nitro, thiocyano, chlorine, bromine or a group of the formula --SO.sub.2 NT.sup.1 T.sup.2, --COOT.sup.3 or --SO.sub.2 T.sup.3 ;Q is hydrogen, chlorine, bromine, lower alkoxy or a --COOT.sup.3 group;R is cyano lower alkyl;A and A.sup.1 each independently represent a lower alkylene radical;X is cyano, lower alkoxy, lower alkoxy lower alkoxy, lower alkoxy lower alkoxy lower alkoxy, chlorine, bromine, lower alkoxycarbonyl, lower alkylcarbonyl, optionally substituted phenoxy carbonyl or optionally substituted phenoxy;Y is lower alkoxycarbonyl, lower alkylcarbonyl, optionally substituted phenylcarbonyl, optionally substituted phenoxycarbonyl, phenyl lower alkoxycarbonyl, lower alkylsulphonyl, optionally substituted phenylsulphonyl or N-optionally substituted aminocarbonyl;T.sup.1 is hydrogen or alkyl;T.sup.2 is hydrogen, alkyl, phenyl, phenylalkyl or cycloalkyl; and T.sup.3 is alkyl, phenyl, phenylalkyl or cycloalkyl, a process for the manufacture of the said dyestuffs and their use for coloring synthetic textile materials. The said dyestuffs have excellent build-up properties on polyester textile material so that heavy depths of shade can be readily obtained and the resulting colorations have excellent fastness to light, to wet treatments and to dry heat treatments.
摘要翻译： 其中U是氢，氯，溴，氰基，低级烷基，低级烷氧基或式-CONT1T2，-COOT3或-SO2T3的基团的下式的分散单偶氮染料： V是氢，氯，溴，氰基或低级烷氧基羰基; W是氢，氰基，硝基，硫氰基，氯，溴或式-SO2NT1T2，-COOT3或-SO2T3的基团; Q是氢，氯，溴，低级烷氧基或-COOT3基团; R为氰基低级烷基; A和A1各自独立地表示低级亚烷基; X为氰基，低级烷氧基，低级烷氧基低级烷氧基，低级烷氧基低级烷氧基低级烷氧基，氯，溴，低级烷氧基羰基，低级烷基羰基，任意取代的苯氧基羰基或任意取代的苯氧基; Y是低级烷氧基羰基，低级烷基羰基，任选取代的苯基羰基，任意取代的苯氧基羰基，苯基低级烷氧基羰基，低级烷基磺酰基，任选取代的苯基磺酰基或N-任选取代的氨基羰基; T1是氢或烷基; T 2是氢，烷基，苯基，苯基烷基或环烷基; 并且T3是烷基，苯基，苯基烷基或环烷基，制备所述染料的方法及其用于着色合成纺织材料的用途。 所述染料在聚酯纺织材料上具有优异的聚集性能，因此可以容易地获得很深的色调，并且所得到的着色具有优异的耐光牢度，湿法处理和干热处理。
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