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公开(公告)号：US06136777A
公开(公告)日：2000-10-24
申请号：US269848
申请日：1999-04-01
Applicant: Angela Gloria Del Greco , Wayne Edward Beimesch , Manivannan Kandasamy
Inventor： Angela Gloria Del Greco , Wayne Edward Beimesch , Manivannan Kandasamy
CPC classification number: C11D17/065 , C11D11/0082 , C11D11/0088 , C11D11/02 , C11D17/0039
Abstract: A non-tower process for continuously preparing granular detergent composition having a density of at least about 600 g/l is provided. The process comprises the overall steps of: (a) dispersing a surfactant, and coating the surfactant with fine powder in a mixer, wherein first agglomerates are formed; (b) spraying finely atomized liquid onto the first agglomerates in a mixer, wherein second agglomerates are formed; and (c) granulating the third agglomerates in one or more fluidizing apparatus. The process is improved by further step (b'), by thoroughly mixing the second agglomerates in a mixer, between step (b) and step (c), wherein, in step (b'), choppers are used to reduce the amount of oversized agglomerates.
Abstract translation: PCT No.PCT / US97 / 09796 Sec。 371日期1999年4月1日 102（e）1999年4月1日PCT 1997年6月5日PCT公布。 公开号WO98 / 14558 日期1998年4月9日提供了一种用于连续制备密度为至少约600g / l的颗粒洗涤剂组合物的非塔式方法。 该方法包括以下步骤：（a）分散表面活性剂，并在混合器中用细粉末涂覆表面活性剂，其中形成第一附聚物; （b）在混合器中将精细雾化的液体喷雾到第一附聚物上，其中形成第二附聚物; 和（c）在一个或多个流化装置中造粒第三附聚物。 通过进一步的步骤（b'），通过在步骤（b）和步骤（c）中将混合器中的第二附聚物充分混合，其中在步骤（b'）中，使用斩波器来减少 超大的聚集体。
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2.发明授权Process for making a low density detergent composition by agglomeration followed by dielectric heating 失效通过聚集然后进行介电加热制备低密度洗涤剂组合物的方法
公开(公告)号：US06063751A
公开(公告)日：2000-05-16
申请号：US180678
申请日：1999-04-05
Applicant: Paul Amaat France , Larry Rudolph Genskow , Wayne Edward Beimesch
Inventor： Paul Amaat France , Larry Rudolph Genskow , Wayne Edward Beimesch
CPC classification number: C11D11/0082 , C11D11/007 , C11D17/06
Abstract: A process for preparing a low density detergent composition is disclosed. The process includes the steps of agglomerating a detergent surfactant paste and dry starting detergent material in a high speed mixer to obtain detergent agglomerates wherein the detergent agglomerates include at least 3% by weight water and dielectrically heating the detergent agglomerates so as to form the detergent composition having a density of below 600 g/l.
Abstract translation: PCT No.PCT / US97 / 07205 Sec。 371日期1999年4月5日 102（e）日期1999年4月5日PCT提交1997年5月1日PCT公布。 第WO97 / 43399号公报 日期：1997年11月20日公开了一种制备低密度洗涤剂组合物的方法。 该方法包括以下步骤：在高速混合器中将洗涤剂表面活性剂浆料和干燥的起始洗涤剂材料附聚在一起，以获得洗涤剂附聚物，其中洗涤剂团聚体包含至少3重量％的水，并介电地加热洗涤剂附聚物以形成洗涤剂组合物 密度低于600g / l。
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3.发明授权Process for making a low density detergent composition by agglomeration with an inorganic double salt 失效通过与无机双重盐结合制备低密度洗涤剂组合物的方法
公开(公告)号：US5668099A
公开(公告)日：1997-09-16
申请号：US601638
申请日：1996-02-14
Applicant: Benjamin Edgar Chapman , Steven Barrett Rogers , Paul Amaat France , Wayne Edward Beimesch
Inventor： Benjamin Edgar Chapman , Steven Barrett Rogers , Paul Amaat France , Wayne Edward Beimesch
CPC classification number: C11D3/046 , C11D11/0082 , C11D11/02 , C11D17/06 , C11D3/10
Abstract: A process for continuously preparing low density detergent agglomerates is provided. The process comprises the steps of: (a) spray drying an aqueous mixture of sodium sulfate, sodium carbonate and a minor amount of a surfactant so as to form spray dried granules containing an inorganic double salt having the formula Na.sub.2 SO.sub.4 .multidot.Na.sub.2 CO.sub.3 and a minor amount of the surfactant; (b) agglomerating the spray dried granules with a detergent surfactant paste or precursor thereof and adjunct detergent material initially in a high speed mixer and subsequently in a moderate speed mixer to obtain detergent agglomerates, wherein the adjunct detergent material includes an adjunct sodium carbonate material; and (c) drying or cooling the detergent agglomerates so as to form the detergent composition having a density of below about 500 g/l.
Abstract translation: 提供连续制备低密度洗涤剂团块的方法。 该方法包括以下步骤：（a）将硫酸钠，碳酸钠和少量表面活性剂的水性混合物喷雾干燥，以形成含有下式的无机复盐的喷雾干燥颗粒：Na 2 SO 4 x Na 2 CO 3和少量的 表面活性剂 （b）最初在高速混合器中随后用中速混合器将具有洗涤剂表面活性剂浆料或其前体和辅助洗涤剂的喷雾干燥颗粒附聚在一起以获得洗涤剂附聚物，其中辅助洗涤剂材料包括辅助碳酸钠材料; 和（c）干燥或冷却洗涤剂附聚物，以形成密度低于约500g / l的洗涤剂组合物。
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公开(公告)号：US08883129B2
公开(公告)日：2014-11-11
申请号：US11034477
申请日：2005-01-13
Applicant: David Frederick Swaile , Wayne Edward Beimesch , David Good , Scott Edward Smith
Inventor： David Frederick Swaile , Wayne Edward Beimesch , David Good , Scott Edward Smith
Abstract: An enhanced efficacy aluminum only salt active. The method for making such active comprises the steps of (a) providing an aqueous solution of an aluminum salt having a Band III polymer concentration of at least about 20%; (b) adding to the aqueous solution of step (a) an aqueous solution of a monomeric aluminum salt to form a mixture; and (c) rapidly drying the mixture to form a product powder. The active comprises an aluminum only salt having a Band III polymer concentration of at least about 20%, an aluminum to anion ratio of from about 1.1:1 to about 1.8:1 and a level of monomeric aluminum of from about 2% to about 20% of the total aluminum.
Abstract translation: 增强功效铝只有盐活性。 制备这种活性物质的方法包括以下步骤：（a）提供具有至少约20％的Band III聚合物浓度的铝盐水溶液; （b）向步骤（a）的水溶液中加入单体铝盐的水溶液以形成混合物; 和（c）快速干燥混合物以形成产物粉末。 该活性物质包括仅具有III族聚合物浓度至少为约20％，铝与阴离子比为约1.1:1至约1.8:1的铝盐，单体铝含量为约2％至约20 占总铝的百分比。
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公开(公告)号：US06790821B1
公开(公告)日：2004-09-14
申请号：US09980327
申请日：2001-11-30
Applicant: Matthew Israel Wasserman , Mark William Ridyard , Scott William Capeci , Wayne Edward Beimesch , Paul R Mort, III
Inventor： Matthew Israel Wasserman , Mark William Ridyard , Scott William Capeci , Wayne Edward Beimesch , Paul R Mort, III
IPC: C11D1700
CPC classification number: B01J2/006 , B01J2/16 , C11D11/0088 , C11D17/0039 , Y10T428/12625
Abstract: A process for preparing coated detergent granules in a fluidized bed is provided. The fluidized bed is operated at a flux number of at least about 3.5 and/or a Stokes Number of greater than 1.0. Upon drying, the resultant detergent particles have improved appearance and flow properties and may be packaged and sold as a detergent material or mixed with various other detergent ingredients to provide a fully formulated detergent composition.
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Patent Agency Ranking
公开(公告)号：US6143711A
公开(公告)日：2000-11-07
申请号：US269853
申请日：1999-04-01
Applicant: Angela Gloria Del Greco , Wayne Edward Beimesch
Inventor： Angela Gloria Del Greco , Wayne Edward Beimesch
CPC classification number: C11D11/0082 , C11D11/0088 , C11D11/02 , C11D17/0039 , C11D17/065
Abstract: A non-tower process for continuously preparing granular detergent composition having a density of at least about 600 g/l is provided. The process comprises the steps of (a) dispersing a surfactant and coating the surfactant with fine powder having a diameter from 0.1 to 500 microns in a mixer fitted with choppers, and (b) granulating the agglomerates in one or more fluidizing apparatus, wherein finely atomized liquid is sprayed onto the first agglomerates in a mixer between step (a) and (b).
Abstract translation: PCT No.PCT / US97 / 09789第 371日期1999年4月1日 102（e）1999年4月1日PCT 1997年6月5日PCT公布。 公开号WO98 / 14551 日期1998年4月9日提供了一种用于连续制备密度为至少约600g / l的颗粒洗涤剂组合物的非塔式方法。 该方法包括以下步骤：（a）分散表面活性剂并用直径为0.1-500微米的细粉末涂覆表面活性剂，并在（b）在一个或多个流化设备中制粒附聚物，其中精细 将雾化液体在步骤（a）和（b）之间的混合器中喷洒到第一附聚物上。
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公开(公告)号：US06211138B1
公开(公告)日：2001-04-03
申请号：US09269856
申请日：1999-04-01
Applicant: Wayne Edward Beimesch
Inventor： Wayne Edward Beimesch
IPC: C11D1100
CPC classification number: C11D17/0039 , C11D1/146 , C11D1/22 , C11D1/29 , C11D11/00 , C11D11/0082 , C11D11/0088 , C11D11/02 , C11D17/06 , C11D17/065
Abstract: A non-tower process for continuously preparing granular detergent compositions having a density of at least of about 600 g/l comprises the steps of (a) dispersing a surfactant, and coating the surfactant with fine powder having a diameter from 0.1 to 500 microns, while wetting the surfactant coated with the fine powder with finely atomized liquid, in a mixer, wherein first agglomerates are formed and (b) granulating the first agglomerates in one or more fluidizing apparatus.
Abstract translation: 用于连续制备具有至少约600g / l密度的颗粒洗涤剂组合物的非塔式方法包括以下步骤：（a）分散表面活性剂，并用0.1至500微米直径的细粉末涂覆表面活性剂， 同时在混合器中润湿具有细粉末的细粉末的表面活性剂，其中形成第一附聚物，和（b）在一个或多个流化装置中造粒第一附聚物。
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公开(公告)号：US06211137B1
公开(公告)日：2001-04-03
申请号：US09269850
申请日：1999-04-01
Applicant: Wayne Edward Beimesch , Jose Francisco Correa Romo , Steven Barrett Rogers
IPC: C11D1100
CPC classification number: C11D11/0088 , C11D11/0082 , C11D11/02 , C11D17/065
Abstract: A non-tower process for continuously preparing granular detergent compositions having a density of at least of about 600 g/l comprises the steps of (a) dispersing a surfactant, and coating the surfactant with fine powder having a diameter from 0.1 to 500 microns, in a mixer, wherein first agglomerates are formed and (b) granulating the first agglomerates in one or more fluidizing apparatus.
Abstract translation: 用于连续制备具有至少约600g / l密度的颗粒洗涤剂组合物的非塔式方法包括以下步骤：（a）分散表面活性剂，并用0.1至500微米直径的细粉末涂覆表面活性剂， 在混合器中，其中形成第一附聚物和（b）在一个或多个流化装置中对第一附聚物进行造粒。
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9.发明授权Process for making a low density detergent composition by agglomeration with a hydrated salt 失效通过用水合盐凝聚制备低密度洗涤剂组合物的方法
公开(公告)号：US5665691A
公开(公告)日：1997-09-09
申请号：US539036
申请日：1995-10-04
Applicant: Paul Amatt France , Larry Rudolph Genskow , Wayne Edward Beimesch
Inventor： Paul Amatt France , Larry Rudolph Genskow , Wayne Edward Beimesch
CPC classification number: C11D11/0082 , C11D17/06 , C11D3/1233
Abstract: A process for continuously preparing low density detergent agglomerate is provided. The process comprises the steps of: (a) agglomerating a detergent surfactant paste and dry starting detergent material in a high speed mixer to obtain detergent agglomerates, wherein the dry starting detergent material includes a hydrated salt; and (b) drying the detergent agglomerates so as to form the detergent composition having a density of less than about 600 g/l.
Abstract translation: 提供连续制备低密度洗涤剂团块的方法。 该方法包括以下步骤：（a）在高速混合器中使洗涤剂表面活性剂浆料和干燥的起始洗涤剂物质凝聚，得到洗涤剂附聚物，其中干起始洗涤剂材料包括水合盐; 和（b）干燥洗涤剂附聚物以形成密度小于约600g / l的洗涤剂组合物。
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公开(公告)号：US06900169B2
公开(公告)日：2005-05-31
申请号：US10880689
申请日：2004-06-30
Applicant: Matthew Israel Wasserman , Mark William Ridyard , Scott William Capeci , Wayne Edward Beimesch , Paul R Mort, III
Inventor： Matthew Israel Wasserman , Mark William Ridyard , Scott William Capeci , Wayne Edward Beimesch , Paul R Mort, III
CPC classification number: B01J2/006 , B01J2/16 , C11D11/0088 , C11D17/0039 , Y10T428/12625
Abstract: A process for preparing coated detergent granules in a fluidized bed. The fluidized bed is operated at a flux number of at least about 4 and at a Stokes Number of 10 to about 1000 using a coating solution or slurry having a viscosity from about 300 to about 100,000 centipoise, measured at 60° C. Upon drying, the resultant detergent particles have improved appearance and flow properties and may be packaged and sold as a detergent material or mixed with various other detergent ingredients to provide a fully formulated detergent composition.
Abstract translation: 一种在流化床中制备包衣洗涤剂颗粒的方法。 使用在60℃下测量的具有约300至约100,000厘泊的粘度的涂布溶液或浆料，流化床以至少约4的通量数和斯托克斯数为10至约1000的速率操作。干燥时， 所得的洗涤剂颗粒具有改善的外观和流动性能，并且可以作为洗涤剂材料包装和出售或与各种其它洗涤剂成分混合以提供完全配制的洗涤剂组合物。
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