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1.发明授权Block copolymers of monovinylarenes and conjugated dienes containing two interior tapered blocks 失效含有两个内锥形嵌段的单乙烯基芳烃和共轭二烯的嵌段共聚物
公开(公告)号：US5399628A
公开(公告)日：1995-03-21
申请号：US162735
申请日：1993-12-02
IPC分类号： C08F297/02 , C08F297/04
CPC分类号： C08F297/044
摘要： A method for preparing tapered block copolymers in a polymerization process by sequentially charging: (1) an initiator and monovinylaromatic monomer in the presence of a randomizer; (2) an initiator and monovinylaromatic monomer; (3) a mixture of monovinylaromatic and conjugated diene monomers; (4) a mixture of monovinylaromatic and conjugated diene monomers; (5) conjugated diene monomer; and (6) a coupling agent; and the polymodal tapered block copolymers prepared thereby. The copolymers are particularly useful neat or in blends for applications such as packaging and food or drink containers which require transparency and good environmental stress crack resistance.
摘要翻译： 在聚合过程中通过顺序加入来制备渐缩嵌段共聚物的方法：（1）引发剂和单乙烯基芳族单体在无规发生剂存在下进行; （2）引发剂和单乙烯基芳族单体; （3）单乙烯基芳族化合物和共轭二烯单体的混合物; （4）单乙烯基芳族化合物和共轭二烯单体的混合物; （5）共轭二烯单体; 和（6）偶联剂; 和由此制备的多模式锥形嵌段共聚物。 共聚物特别适用于需要透明度和良好的耐环境应力开裂性的包装和食品或饮料容器等应用的混合物。
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公开(公告)号：US5270396A
公开(公告)日：1993-12-14
申请号：US885715
申请日：1992-05-18
IPC分类号： C08F297/04 , C08G81/02
CPC分类号： C08G81/022 , C08F297/044
摘要： A method for preparing resinous copolymers by sequential charge copolymerization of at least two charges, at least one being a conjugated diene and at least one being a monovinylarene; followed by a charge of a polyfunctional coupling agent; and the final charge being an essentially difunctional coupling agent. The copolymer made by this method and articles made from this copolymer are also provided.
摘要翻译： 一种通过至少两种电荷的顺序电荷共聚制备树脂共聚物的方法，至少一种是共轭二烯和至少一种是单乙烯基芳烃; 然后加入多官能偶联剂; 并且最终的电荷是基本上双官能的偶联剂。 还提供了由该方法制得的共聚物和由该共聚物制成的制品。
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公开(公告)号：US5227419A
公开(公告)日：1993-07-13
申请号：US632239
申请日：1990-12-20
IPC分类号： C08F297/04
CPC分类号： C08F297/04
摘要： A method for preparing tapered block copolymers in a polymerization process by charging an initiator and monomers sequentially with one or more charges of first one of the monomers, then with a mixture of the two monomers, and then with one or more charges of the first monomer to produce a polymodal tapered block copolymer. Suitable monomers include conjugated dienes and monovinylaromatic compounds. The copolymers are particularly useful for applications requiring environmental stress crack resistance.
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公开(公告)号：US5910546A
公开(公告)日：1999-06-08
申请号：US963964
申请日：1997-11-04
IPC分类号： C08F8/44 , C08F297/02 , C08F297/04 , C08G81/02 , C08L25/04 , C08L25/06 , C08L53/02
CPC分类号： C08L53/02 , C08F297/044 , C08G81/021 , C08G81/022 , C08L25/04 , C08L25/06
摘要： A method for preparing tapered block copolymers which are particularly useful for blend components in blends with polymers of styrene. In the first embodiment of this invention the copolymers are prepared in a polymerization process by sequentially charging: (1) an initiator and monovinylaromatic monomers in the presence of a randomizer; (2) an initiator and monovinylaromatic monomers; (3) a mixture of monovinylaromatic and conjugated diene monomers; and (4) a coupling agent; to produce a polymodal tapered block copolymer. In a second embodiment of the invention tapered block copolymers are prepared in a polymerization process by sequentially charging: (1) an initiator and monovinylaromatic monomers in the presence of a randomizer; (2) an initiator and monovinylaromatic monomers; (3) a mixture of monovinylaromatic and conjugated diene monomers; (4) a mixture of monovinylaromatic and conjugated diene monomers; and (5) a coupling agent; to produce a polymodal tapered block copolymer. The invention copolymers and blends of the invention copolymers with polymers of styrene are particularly useful for applications such as packaging and food or drink containers which require transparency, low blueness, colorlessness, good impact strength and ductility.
摘要翻译： 一种制备锥形嵌段共聚物的方法，其特别适用于与苯乙烯聚合物的共混物中的共混物组分。 在本发明的第一个实施方案中，共聚物在聚合过程中通过顺序加入来制备：（1）引发剂和单乙烯基芳族单体; （2）引发剂和单乙烯基芳族单体; （3）单乙烯基芳族化合物和共轭二烯单体的混合物; 和（4）偶联剂; 以制备多晶型锥形嵌段共聚物。 在本发明的第二个实施方案中，在聚合过程中通过顺序加入来制备渐缩嵌段共聚物：（1）引发剂和单乙烯基芳族单体; （2）引发剂和单乙烯基芳族单体; （3）单乙烯基芳族化合物和共轭二烯单体的混合物; （4）单乙烯基芳族化合物和共轭二烯单体的混合物; 和（5）偶联剂; 以制备多晶型锥形嵌段共聚物。 本发明的共聚物和本发明共聚物与苯乙烯聚合物的共混物特别适用于需要透明度，低蓝，无色度，良好的冲击强度和延展性的包装和食品或饮料容器等应用。
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5.发明授权Viscosity index improver soluble in synthetic poly(.alpha.-olefin) lubricants 失效粘度指数改进剂可溶于合成聚（α-烯烃）润滑剂
公开(公告)号：US4418234A
公开(公告)日：1983-11-29
申请号：US331413
申请日：1981-12-16
申请人： Sidney Schiff , William J. Trepka
发明人： Sidney Schiff , William J. Trepka
IPC分类号： C08C19/02 , C08F8/04 , C10M143/00 , C10M1/18
CPC分类号： C10M143/00 , C08C19/02 , C08F8/04 , C10M2205/00 , C10M2205/02 , C10M2205/04 , C10M2205/06
摘要： Hydrogenated completely random conjugated diene/monovinylarene copolymers with a conjugated diene content above about 50 weight percent, monovinylarene content below about 50 weight percent, vinyl unsaturation (normalized) at least about 25 weight percent, block polymonovinylarene below about 5 weight percent, and molecular weight M.sub.n in the range of about 30,000-200,000, are soluble in synthetic poly(.alpha.-olefin) lubricating oils providing therein effective viscosity index control, pour point, and shear loss at low concentrations.
摘要翻译： 氢化完全无规共轭二烯/单乙烯基芳烃共聚物，共轭二烯含量高于约50重量％，单乙烯基芳烃含量低于约50重量％，乙烯基不饱和度（归一化）至少约25重量％，嵌段聚单乙烯基芳烃低于约5重量％，分子量 在约30,000-200,000范围内的Mn可溶于合成聚（α-烯烃）润滑油，其中提供了低浓度下有效的粘度指数控制，倾点和剪切损失。
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公开(公告)号：US4238576A
公开(公告)日：1980-12-09
申请号：US5625
申请日：1979-01-22
申请人： William J. Trepka
发明人： William J. Trepka
CPC分类号： C08G81/022 , C08F8/00
摘要： Orthoesters are used to couple living homopolymers of monovinylarenes, and living copolymers of monovinylarenes and conjugated dienes. Novel coupled polymers are thereby produced.
摘要翻译： 邻苯二甲酸酯用于偶联单乙烯基芳烃的活性均聚物和单乙烯基芳烃和共轭二烯的活性共聚物。 由此产生新的偶联聚合物。
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公开(公告)号：US4076915A
公开(公告)日：1978-02-28
申请号：US694123
申请日：1976-06-08
申请人： William J. Trepka
发明人： William J. Trepka
摘要： Treating a silicon-coupled or germanium-coupled conjugated diene polymer with a hydrocarbonlithium, -sodium, -potassium, -calcium, -magnesium, -zinc or -aluminum compound after the coupling step and prior to hydrogenation.
摘要翻译： 在偶联步骤之后和氢化之前，用烃锂，钠，钾，钙，镁，锌或铝化合物处理硅偶联或锗偶联共轭二烯聚合物。
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公开(公告)号：US06265485B1
公开(公告)日：2001-07-24
申请号：US08968001
申请日：1997-11-12
IPC分类号： C08F29704
CPC分类号： C08L53/02 , C08F297/044 , C08G81/021 , C08G81/022 , C08L25/04 , C08L25/06 , C08L2666/24 , C08L91/06 , C08L2666/04
摘要： A method for preparing tapered block copolymers which are particularly useful for blend components in blends with polymers of styrene. In the first embodiment of this invention the copolymers are prepared in a polymerization process by sequentially charging: (1) an initiator and monovinylaromatic monomers in the presence of a randomizer; (2) an initiator and monovinylaromatic monomers; (3) a mixture of monovinylaromatic and conjugated diene monomers; and (4) a coupling agent; to produce a polymodal tapered block copolymer. In a second embodiment of the invention tapered block copolymers are prepared in a polymerization process by sequentially charging: (1) an initiator and monovinylaromatic monomers in the presence of a randomizer; (2) an initiator and monovinylaromatic monomers; (3) a mixture of monovinylaromatic and conjugated diene monomers; (4) a mixture of monovinylaromatic and conjugated diene monomers; and (5) a coupling agent; to produce a polymodal tapered block copolymer. The invention copolymers and blends of the invention copolymers with polymers of styrene are particularly useful for applications such as packaging and food or drink containers which require transparency, low blueness, colorlessness, good impact strength and ductility.
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10.发明授权Viscosity index improvers with dispersant properties prepared by reaction of lithiated hydrogenated copolymers with 4-substituted aminopyridines 失效具有分散性能的粘度指数改进剂，其通过锂化氢化共聚物与4-取代氨基吡啶反应制备
公开(公告)号：US4402843A
公开(公告)日：1983-09-06
申请号：US314296
申请日：1981-10-23
申请人： William J. Trepka
发明人： William J. Trepka
IPC分类号： C08C19/42 , C10M143/12 , C10M1/32 , C08F255/02
CPC分类号： C08C19/42 , C10M143/12 , C10M2205/04 , C10M2205/06 , C10M2215/221 , C10M2217/028 , C10M2217/06 , C10M2227/00
摘要： Nitrogen-containing copolymers useful as viscosity index improvers with dispersing characteristics are prepared by the reaction of lithiated hydrogenated conjugated diene-monovinylarene copolymers with substituted aminopyridine.
摘要翻译： 通过锂化氢化共轭二烯 - 一乙烯基芳烃共聚物与取代的氨基吡啶的反应制备可用作具有分散特性的粘度指数改进剂的含氮共聚物。
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