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公开(公告)号：US5482825A
公开(公告)日：1996-01-09
申请号：US362726
申请日：1994-12-23
申请人： Roger Lok , Carl R. Preddy , Xin Wen
发明人： Roger Lok , Carl R. Preddy , Xin Wen
CPC分类号： G03C1/07 , G03C1/10 , G03C1/34 , G03C1/0051
摘要： A method of making a silver halide emulsion comprising precipitating and chemically sensitizing the emulsion and further comprising adding to the emulsion a fused dihydropyrimidine compound represented by the following formula: ##STR1## wherein X is O, S or Se; R is a substituted or unsubstituted alkyl or aryl group; andZ contains the atoms necessary to form an aromatic group, a heteroaromatic group or a heterocyclic group and a silver halide emulsion made by this method.
摘要翻译： 一种制备卤化银乳剂的方法，其包括对所述乳液进行沉淀和化学增感，并且还包括向所述乳液中加入由下式表示的稠合二氢嘧啶化合物：其中X为O，S或Se; R是取代或未取代的烷基或芳基; Z包含形成芳族基团，杂芳族基团或杂环基团所需的原子和通过该方法制备的卤化银乳剂。
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公开(公告)号：US5491056A
公开(公告)日：1996-02-13
申请号：US296567
申请日：1994-08-26
摘要： A process is disclosed for preparing a photographic emulsion utilizing an alkynylamine compound as a grain growth modifier. Specifically, the present invention provides a process of preparing a photographic emulsion comprising:introducing silver ions, halide ions and a grain growth modifier having the structure ##STR1## wherein z represents atoms necessary to complete a five to nine-membered heterocyclic ring system, R.sup.1, R.sup.2 and R.sup.3 independently represent hydrogen or a lower alkyl of from 1 to 5 carbon atoms, and R.sup.4 represents hydrogen, or an aliphatic, carbocyclic, or heterocyclic group, which may be substituted or unsubstituted, into a dispersing medium containing silver halide seed grains; andmaintaining the dispersing medium containing the seed grains, silver ions, halide ions and grain growth modifier at a pH in the range from about 4.5 to about 10, and a pAg in the range from about 6.0 to about 9.5.Also disclosed is a photographic element comprising a support having incorporated thereon a silver halide emulsion layer, the silver halide emulsion layer comprising silver halide grains internally containing a compound of the structure ##STR2## wherein Z represents atoms necessary to complete a five to nine-membered heterocyclic ring system; R.sup.1, R.sup.2 and R.sup.3 independently represent hydrogen or a lower alkyl of from 1 to 5 carbon atoms, with the proviso that at least one of R.sup.1, R.sup.2 and R.sup.3 be a lower alkyl of from 1 to 5 carbon atoms; and R.sup.4 represents hydrogen, or an aliphatic, carbocyclic, or heterocyclic group, which may be substituted or unsubstituted.
摘要翻译： 公开了一种利用炔基胺化合物作为晶粒生长改性剂制备照相乳剂的方法。 具体地说，本发明提供一种制备照相乳剂的方法，其包括：引入银离子，卤离子和具有结构的晶粒生长改性剂，其中z表示完成五至九元杂环体系所需的原子，R1 ，R2和R3独立地表示氢或1〜5个碳原子的低级烷基，R4表示氢，或可被取代或未取代的脂族，碳环或杂环基团，形成含有卤化银种子颗粒的分散介质 ; 并且在约4.5至约10的pH范围内将含有种子晶粒，银离子，卤离子和晶粒生长调节剂的分散介质保持在约6.0至约9.5的范围内。 还公开了一种照相元件，其包括其上并入有卤化银乳剂层的载体，所述卤化银乳剂层包含卤化银颗粒，内部含有结构“IMAGE”的化合物，其中Z表示完成五至九元 杂环体系; R 1，R 2和R 3独立地表示氢或1至5个碳原子的低级烷基，条件是R 1，R 2和R 3中的至少一个为1至5个碳原子的低级烷基; 并且R 4表示氢，或可以被取代或未取代的脂族，碳环或杂环基。
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公开(公告)号：US06573038B2
公开(公告)日：2003-06-03
申请号：US09872669
申请日：2001-06-01
IPC分类号： G03C134
CPC分类号： G03C7/39252 , G03C1/34 , G03C7/3022 , G03C2001/03517
摘要： A silver halide photographic element comprising a silver halide emulsion which is greater than 50 mole % silver chloride and a pyrimidine compound represented by Formula I wherein R1, R2, and R3 are each independently a hydrogen atom or a hydroxy, alkoxy, amino, alkylamino, cyanoamino or alkyl group, and R4 is a hydroxy, alkoxy, amino, alkylamino, cyanoamino or alkyl group; provided that at least one of R1, R2, R3, and R4 is a hydroxy or an amino group.
摘要翻译： 一种卤化银照相元件，其包含大于50摩尔％氯化银的卤化银乳剂和由式I表示的嘧啶化合物，其中R1，R2和R3各自独立地为氢原子或羟基，烷氧基，氨基，烷基氨基，氰基氨基 或烷基，R4是羟基，烷氧基，氨基，烷基氨基，氰基氨基或烷基; 条件是R 1，R 2，R 3和R 4中的至少一个是羟基或氨基。
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公开(公告)号：US6034249A
公开(公告)日：2000-03-07
申请号：US964104
申请日：1997-11-06
申请人： Roger Lok , Weimar W. White , Brian P. Cleary
发明人： Roger Lok , Weimar W. White , Brian P. Cleary
IPC分类号： G03C1/09 , C07D233/84 , C07F1/00 , C07F1/12 , C07D257/04
CPC分类号： C07F1/005
摘要： This invention relates to an organomercapto Au(I) complex having the formula ##STR1## wherein M is a cationic counterion;SOL is a solubilizing group;A is a substituted or unsubstituted divalent organic linking group;and n is 1 to 4 and wherein the compound is symmetrical.It further relates to a method of manufacturing an organomercapto Au(I) complex comprising reacting an Au(I) complex with an organomercapto ligand and isolating the resulting organomercapto Au(I) complex from the reaction mixture.
摘要翻译： 本发明涉及具有下式的有机巯基Au（I）配合物，其中M是阳离子抗衡离子; SOL是增溶基团; A是取代或未取代的二价有机连接基团; 且n为1至4，并且其中该化合物是对称的。 本发明还涉及一种制备有机巯基Au（I）配合物的方法，包括使Au（I）配合物与有机巯基配体反应并从所述反应混合物中分离得到的有机巯基Au（I）配合物。
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公开(公告)号：US5700631A
公开(公告)日：1997-12-23
申请号：US672254
申请日：1996-06-28
申请人： Roger Lok , Weimar Weatherly White
发明人： Roger Lok , Weimar Weatherly White
摘要： A photographic element is provided comprising a support having situated thereon a silver halide emulsion layer, the emulsion layer comprising a compound of the formula: Z--SO.sub.2 S--Au(I)--L (I) wherein Z represents an alkyl, aryl, or heterocyclic group; and L represents a thioether, selenoether or telluroether containing ligand.
摘要翻译： 提供了一种照相元件，其中包括一个位于其上的卤化银乳剂层的载体，该乳剂层包含下式的化合物：Z-SO2S-Au（I）-L（Ⅰ），其中Z代表烷基，芳基或杂环 组; L代表含硫醚，硒醚或含曙红醚的配体。
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公开(公告)号：US5601970A
公开(公告)日：1997-02-11
申请号：US367961
申请日：1995-01-03
申请人： Roger Lok
发明人： Roger Lok
CPC分类号： G03C1/346 , G03C7/39288
摘要： This invention provides a photographic element comprising a support having thereon a silver halide emulsion layer which is greater than about 50 mole % silver chloride, wherein the emulsion layer contains a thiophosphate ester of the structure: ##STR1## wherein R.sup.1, R.sup.2 and R.sup.3 are independently selected from the group consisting of an aliphatic, carbocyclic or heterocyclic group.
摘要翻译： 本发明提供了一种照相元件，其中包含一种其上具有大于约50％（摩尔）氯化银的卤化银乳剂层的载体，其中该乳剂层含有以下结构的硫代磷酸酯：其中R1，R2和R3独立地为 选自脂族，碳环或杂环基。
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7.发明授权Heat stabilized silver chloride photographic emulsions containing sulfur donors and sulfinate compounds 失效含硫供体和亚磺酸盐化合物的热稳定氯化银照相乳剂
公开(公告)号：US5536633A
公开(公告)日：1996-07-16
申请号：US384200
申请日：1995-02-06
申请人： Roger Lok
发明人： Roger Lok
CPC分类号： G03C7/39296 , G03C1/346 , G03C7/39236 , G03C1/035
摘要： A silver halide photographic element comprising a silver halide emulsion which is greater than 50 mole % silver chloride, said emulsion being in reactive association with a sulfur donating compound, and a sulfinate compound represented by Formula (I)Z--SO.sub.2 M.sup.1 (I)wherein Z is a non-metallic aryl, alkyl or heterocyclic group, and M is a cationic counter ion;and wherein the sulfur donor is not a thiosulfonate or a diamino disulfide; and a method of making the emulsion.
摘要翻译： 一种卤化银照相元件，其包含大于50摩尔％氯化银的卤化银乳剂，所述乳液与供硫化合物反应结合，和由式（I）Z-SO 2 M 1（I）表示的亚磺酸盐化合物，其中Z 是非金属芳基，烷基或杂环基，M是阳离子抗衡离子; 并且其中所述硫供体不是硫代磺酸盐或二氨基二硫化物; 以及制造乳液的方法。
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8.发明授权Photographic sensitivity increasing alkynylamine compounds and photographic elements 失效摄影灵敏度增加炔基胺化合物和摄影元素
公开(公告)号：US5413905A
公开(公告)日：1995-05-09
申请号：US169833
申请日：1993-12-16
申请人： Roger Lok , Carl R. Preddy , John W. Harder
发明人： Roger Lok , Carl R. Preddy , John W. Harder
摘要： The present invention relates to water soluble photographic sensitivity increasing alkynylamine compounds. It also relates to photographic elements containing such compounds.
摘要翻译： 本发明涉及水溶性照相感光度增加的炔基胺化合物。 它还涉及含有这些化合物的照相元件。
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公开(公告)号：US5399479A
公开(公告)日：1995-03-21
申请号：US168892
申请日：1993-12-16
申请人： Roger Lok
发明人： Roger Lok
摘要： The present invention provides a photographic element comprising a support having thereon a silver halide emulsion layer. The emulsion layer contains an organic compound having a thiosulfonic acid substituent, an organic compound having a sulfinic acid substituent, and an alkynylamine.
摘要翻译： 本发明提供了一种照相元件，其包括其上具有卤化银乳剂层的载体。 乳剂层含有具有硫代磺酸取代基的有机化合物，具有亚磺酸取代基的有机化合物和炔基胺。
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公开(公告)号：US4948721A
公开(公告)日：1990-08-14
申请号：US385044
申请日：1989-07-26
申请人： Roger Lok , Ronald E. Leone
发明人： Roger Lok , Ronald E. Leone
IPC分类号： C07D277/62 , G03C1/34
CPC分类号： C07D277/62 , G03C1/34
摘要： Latent image stability is enhanced in photographic recording materials using N-alkyl- or N-alkenylbenzothiazolium or -benzoselenazolium salts.
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