Process for preparation of water soluble dyes containing lithium
sulfonate group or ammonium sulfonate group by cation exchange,
neutralization and reverse osmosis
    1.
    发明授权
    Process for preparation of water soluble dyes containing lithium sulfonate group or ammonium sulfonate group by cation exchange, neutralization and reverse osmosis 失效
    通过阳离子交换,中和和反渗透制备含有磺酸钠基或磺酸铵基团的水溶性染料的方法

    公开(公告)号:US4808192A

    公开(公告)日:1989-02-28

    申请号:US908023

    申请日:1986-09-15

    IPC分类号: C09B67/54 C09B69/02

    摘要: In accordance with this invention an aqueous solution of a water-soluble dye containing lithium sulfonate group or ammonium sulfonate group can be obtained by a very simple and economical process in such a way that an aqueous solution of a water-soluble dye containing sodium sulfonate group is fed to a packed column packed with acid type cation exchange resin (H-form) to form an aqueous solution of a dye containing a free sulfonic acid group, and after neutralizing the resulting solution with LiOH or NH.sub.4 OH, the aqueous solution of the dye thus obtained is concentrated according to a process for separation through reverse osmotic membrane.

    摘要翻译: 根据本发明,可以通过非常简单和经济的方法获得含有磺酸磺酸盐基团或磺酸铵基团的水溶性染料的水溶液,使得含有磺酸钠基团的水溶性染料的水溶液 进料到填充有酸型阳离子交换树脂(H型)的填充柱,以形成含有游离磺酸基团的染料的水溶液,并且在用LiOH或NH 4 OH中和所得溶液之后,将染料的水溶液 根据通过反渗透膜分离的方法浓缩。

    Recording liquid and ink-jet recording method
    2.
    发明授权
    Recording liquid and ink-jet recording method 失效
    记录液体和墨水记录方法

    公开(公告)号:US5127947A

    公开(公告)日:1992-07-07

    申请号:US597938

    申请日:1990-10-12

    IPC分类号: C09D11/00

    摘要: A recording liquid and an ink-jet recording method in which the recording liquid is used to record an image on a recording material comprising a substrate having provided thereon an ink-receiving layer containing a silicon-containing pigment and a binder resin by means of an ink-jet recording technique are disclosed, the recording liquid containing a solvent and at least one dye represented by formula (I): ##STR1## wherein A represents a substituted or unsubstituted phenyl, or naphthyl group; B represents a substituted or unsubstituted phenylene or naphthylene group; C represents an organic group as defined in the specification.

    Recording liquid
    5.
    发明授权
    Recording liquid 失效
    记录液体

    公开(公告)号:US5049188A

    公开(公告)日:1991-09-17

    申请号:US191254

    申请日:1988-05-06

    IPC分类号: C09D11/00 C09D11/16

    CPC分类号: C09D11/38 C09D11/16

    摘要: A recording liquid comprising from 0.2 to 12% by weight, based on the total weight of the recording liquid, of a water-soluble dyestuff, from 0.5 to 25% by weight, based on the total weight of the recording liquid, of at least one member selected from the group consisting of compounds of the following formulas I, II and III, and an aqueous medium: ##STR1## wherein l is a number of from 4 to 20, ##STR2## wherein R is a lower alkyl group or a phenyl group, and each of m and n is a number of from 4 to 20, and ##STR3## wherein X is a halogen atom, and p is a number of from 4 to 20.

    摘要翻译: 一种记录液体,其以基于记录液体的总重量的0.2至12重量%的水溶性染料为基础,至少为记录液体的总重量的0.5至25重量% 一种选自下列式I,II和III的化合物的组分和水性介质:其中l是4至20的数,其中R是 低级烷基或苯基,m和n分别为4〜20,X为卤素原子,p为4〜20的数。

    Recording liquid
    6.
    发明授权
    Recording liquid 失效
    记录液体

    公开(公告)号:US5599386A

    公开(公告)日:1997-02-04

    申请号:US445797

    申请日:1995-05-04

    IPC分类号: C09B29/30 C09D11/00 C09D11/02

    CPC分类号: C09D11/328 C09B29/30

    摘要: A recording liquid comprising an aqueous medium and at least one selected from the compounds whose free acid form is represented by the formula {1}: ##STR1## wherein, R.sup.1, R.sup.2 and R.sup.3 each independently represent a substituted or unsubstituted C.sub.1-9 alkyl group, a C.sub.1-9 alkoxy group, a halogen, hydrogen, a hydroxyl group, a substituted or unsubstituted carbamoyl group, a substituted or unsubstituted sulfamoyl group, a substituted or unsubstituted amino group, a nitro group, a sulfonic ester group, a C.sub.1-9 alkyl- or C.sub.6-15 aryl-sulfonyl group, a COOH group or a carboxylic ester group;m is a number of 0, 1 or 2; andR.sup.4, R.sup.5 and R.sup.6 each independently represent hydrogen, a C.sub.1-18 alkyl group, a C.sub.2-18 alkenyl group, an aryl group, an aralkyl group, an alicyclic group or a heterocyclic group, any of which groups except hydrogen may have a substituent.

    摘要翻译: 包含水性介质和选自游离酸形式的由式{1}表示的化合物中的至少一种的记录液体:其代表取代或未取代的C1-9烷基,C1-9烷氧基,卤素, 氢,羟基,取代或未取代的氨基甲酰基,取代或未取代的氨磺酰基,取代或未取代的氨基,硝基,磺酸酯基,C1-9烷基或C6-15芳基 - 磺酰基 ,COOH基或羧酸酯基; m是0,1或2的数字; R 4,R 5和R 6各自独立地表示氢,C 1-18烷基,C 2-18烯基,芳基,芳烷基,脂环族基或杂环基,除氢以外的基团可以具有 取代基。

    Recording liquid
    7.
    发明授权
    Recording liquid 失效
    记录液体

    公开(公告)号:US5478384A

    公开(公告)日:1995-12-26

    申请号:US238734

    申请日:1994-05-05

    摘要: A recording liquid excellent in print quality, light resistance, and water resistance which is characterized in that it contains an aqueous medium and at least one dye selected from the dyes represented by general formulae [I] to [V]: ##STR1## (wherein R.sub.1 and R.sub.2 each represents H, CH.sub.3, or OCH.sub.3 ; R.sub.3 represents H, Cl,CH.sub.3, or OCH.sub.3 ; R.sub.4 represents an alkyl group having 1 to 6 carbon atoms, a phenyl group, a tolyl group, or an anisyl group; R.sub.5 represents H, a phenyl group which may be substituted with a COOM group, or an alkyl group having 1 to 3 carbon atoms which is substituted with a COOM group; R.sub.6 represents H or an alkyl group having 1 to 3 carbon atoms which is substituted with a COOM group; X represents SO.sub.3 M or COOM; Y represents --CO-- or --SO.sub.2 --; m represents 1 or 2; n represents 0 or 1; A represents a phenylene group which may have one or more members selected from the group consisting of an alkyl group having 1 to 4 carbon atoms, an alkoxy group having 1 to 4 carbon atoms, an amino group, a --COOM group, a hydroxyl group, an --SO.sub.3 M group, and a halogen atom; and M represents an alkali metal, an ammonium group, or an organic amine salt.)

    摘要翻译: 印刷质量,耐光性和耐水性优异的记录液,其特征在于,其含有水性介质和选自通式[I]〜[V]表示的染料中的至少一种染料: (IV)其中R 1和R 2各自表示H,CH 3或OCH 3; R 3表示H,Cl,CH 3或 OCH 3; R 4表示碳原子数1〜6的烷基,苯基,甲苯基或茴香基; R 5表示H,可以被COOM基取代的苯基或具有1〜 被COOM基团取代的3个碳原子; R6表示H或被COOM基团取代的具有1至3个碳原子的烷基; X表示SO 3 M或COOM; Y表示-CO-或-SO 2 - ; m表示 1或2; n表示0或1; A表示可以具有一个或多个选自具有1至4个碳的烷基的一个或多个的亚苯基 具有1至4个碳原子的烷氧基,氨基,-COOM基,羟基,-SO 3 M基和卤素原子; M表示碱金属,铵基或有机胺盐。

    High-strength aluminum alloy extruded product exhibiting excellent corrosion resistance and method of manufacturing same
    10.
    发明申请
    High-strength aluminum alloy extruded product exhibiting excellent corrosion resistance and method of manufacturing same 有权
    具有优异的耐腐蚀性的高强度铝合金挤压制品及其制造方法

    公开(公告)号:US20110155291A1

    公开(公告)日:2011-06-30

    申请号:US12932634

    申请日:2011-03-02

    IPC分类号: C22F1/057

    摘要: The present invention provides a high-strength aluminum alloy extruded product exhibiting excellent corrosion resistance and secondary workability and suitably used as a structural material for transportation equipment such as automobiles, railroad vehicles, and aircrafts, and a method of manufacturing the same. The aluminum alloy extruded product has a composition containing 0.6 to 1.2% of Si, 0.8 to 1.3% of Mg, and 1.3 to 2.1% of Cu while satisfying the following conditional expressions (1), (2), (3) and (4), 3%≦Si %+Mg %+Cu %≦4%  (1) Mg %≦1.7×Si %  (2) Mg %+Si %≦2.7%  (3) Cu %/2≦Mg %≦(Cu %/2)+0.6%  (4) and further containing 0.04 to 0.35% of Cr, and 0.05% or less of Mn as an impurity, with the balance being aluminum and unavoidable impurities. The cross section of the extruded product has a recrystallized structure with an average grain size of 500 μm or less.

    摘要翻译: 本发明提供一种表现出优异的耐腐蚀性和二次加工性的高强度铝合金挤压产品及其制造方法,适用于运输设备如汽车,铁路车辆和飞机的结构材料。 (1),(2),(3)和(4)所述的铝合金挤压制品具有Si:0.6〜1.2%,Mg:0.8〜1.3%,Cu:1.3〜2.1% ),3%≦̸ Si%+ Mg%+ Cu%≦̸ 4%(1)Mg%≦̸ 1.7×Si%(2)Mg%+ Si%≦̸ 2.7%(3)Cu%/ 2& (Cu%/ 2)+0.6%(4),进一步含有0.04〜0.35%的Cr和0.05%以下的Mn作为杂质,余量为铝和不可避免的杂质。 挤出产品的横截面具有平均粒度为500μm以下的再结晶结构。