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1.发明申请公开(公告)号：US20090299075A1
公开(公告)日：2009-12-03
申请号：US11721378
申请日：2005-12-13
申请人： Yuuji Ishigiro , Yasuhiro Aizawa , Masahiro Aono
发明人： Yuuji Ishigiro , Yasuhiro Aizawa , Masahiro Aono
IPC分类号： C07D233/64
CPC分类号： C07D233/56
摘要： The industrial production of 4-(2-methyl-1-imidazolyl)-2,2-diphenylbutanamide, a urinary incontinence remedy, necessitates elimination of problems concerning the use of a synthetic adsorbent, e.g., HP-20, the efficiency of operation with the same, purification efficiency, etc. An acid salt, e.g., hydrochloride or phosphate, of 4-(2-methyl-1-imidazolyl)-2,2-diphenylbutanamide or a hydrate of any of these salts is used as an intermediate. This intermediate is neutralized and then purified. Thus, high-purity 4-(2-methyl-1-imidazolyl)-2,2-diphenylbutanamide is easily obtained in satisfactory yield. The industrial-scale production process has been thus established.
摘要翻译： 4-（2-甲基-1-咪唑基）-2,2-二苯基丁酰胺（尿失禁药物）的工业化生产需要消除使用合成吸附剂的问题，例如HP-20，操作效率 相同的，净化效率等。使用4-（2-甲基-1-咪唑基）-2,2-二苯基丁酰胺或任何这些盐的水合物的酸式盐，例如盐酸盐或磷酸盐作为中间体。 将该中间体中和，然后纯化。 因此，以良好的产率容易地获得高纯度的4-（2-甲基-1-咪唑基）-2,2-二苯基丁酰胺。 工业规模化生产过程已经形成。
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2.发明授权公开(公告)号：US07868183B2
公开(公告)日：2011-01-11
申请号：US11721378
申请日：2005-12-13
申请人： Yuuji Ishiguro , Yasuhiro Aizawa , Masahiro Aono
发明人： Yuuji Ishiguro , Yasuhiro Aizawa , Masahiro Aono
IPC分类号： C07D233/64
CPC分类号： C07D233/56
摘要： The industrial production of 4-(2-methyl-1-imidazolyl)-2,2-diphenylbutanamide, a urinary incontinence remedy, necessitates elimination of problems concerning the use of a synthetic adsorbent, e.g., HP-20, the efficiency of operation with the same, purification efficiency, etc. An acid salt, e.g., hydrochloride or phosphate, of 4-(2-methyl-1-imidazolyl)-2,2-diphenylbutanamide or a hydrate of any of these salts is used as an intermediate. This intermediate is neutralized and then purified. Thus, high-purity 4-(2-methyl-1-imidazolyl)-2,2-diphenylbutanamide is easily obtained in satisfactory yield. The industrial-scale production process has been thus established.
摘要翻译： 4-（2-甲基-1-咪唑基）-2,2-二苯基丁酰胺（尿失禁药物）的工业化生产需要消除使用合成吸附剂的问题，例如HP-20，操作效率 相同的，净化效率等。使用4-（2-甲基-1-咪唑基）-2,2-二苯基丁酰胺或任何这些盐的水合物的酸式盐，例如盐酸盐或磷酸盐作为中间体。 将该中间体中和，然后纯化。 因此，以良好的产率容易地获得高纯度的4-（2-甲基-1-咪唑基）-2,2-二苯基丁酰胺。 工业规模化生产过程已经形成。
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公开(公告)号：US20140021043A1
公开(公告)日：2014-01-23
申请号：US14008211
申请日：2012-03-15
IPC分类号： C23C14/34
CPC分类号： C23C14/3414 , B22F2998/10 , B22F2999/00 , C22C1/0466 , C22C5/04 , C22C33/0278 , C22C1/05 , B22F3/12 , B22F2201/03 , B22F1/0003 , B22F3/14
摘要： An FePt—C-based sputtering target contains Fe, Pt, and C and has a structure in which an FePt-based alloy phase and a C phase containing unavoidable impurities are mutually dispersed, the FePt-based alloy phase containing Pt in an amount of 40 at % or more and 60 at % or less with the balance being Fe and unavoidable impurities. The content of C is 21 at % or more and 70 at % or less based on the total amount of the target.
摘要翻译： FePt-C系的溅射靶含有Fe，Pt，C，具有FePt系合金相和含有不可避免的杂质的C相相互分散的结构，含有Pt量的FePt系合金相 40原子％以上且60原子％以下，余量为Fe和不可避免的杂质。 基于目标物的总量，C的含量为21原子％以上且70原子％以下。
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公开(公告)号：US08858674B2
公开(公告)日：2014-10-14
申请号：US14008211
申请日：2012-03-15
CPC分类号： C23C14/3414 , B22F2998/10 , B22F2999/00 , C22C1/0466 , C22C5/04 , C22C33/0278 , C22C1/05 , B22F3/12 , B22F2201/03 , B22F1/0003 , B22F3/14
摘要： An FePt—C-based sputtering target contains Fe, Pt, and C and has a structure in which an FePt-based alloy phase and a C phase containing unavoidable impurities are mutually dispersed, the FePt-based alloy phase containing Pt in an amount of 40 at % or more and 60 at % or less with the balance being Fe and unavoidable impurities. The content of C is 21 at % or more and 70 at % or less based on the total amount of the target.
摘要翻译： FePt-C系的溅射靶含有Fe，Pt，C，具有FePt系合金相和含有不可避免的杂质的C相相互分散的结构，含有Pt量的FePt系合金相 40原子％以上且60原子％以下，余量为Fe和不可避免的杂质。 C的含量相对于靶的总量为21原子％以上且70原子％以下。
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