摘要:
The particle components may be collected by using a phenomenon that the particle components in the aqueous phase aggregate at the liquid-to-liquid interface. Both of the particle components and the dissolved components in the aqueous phase may be simultaneously collected if combined with liquid-liquid extraction phenomenon that the dissolved components in the aqueous phase are collected into the solvent phase through the liquid-to-liquid interface. The aggregation phenomenon of the particle components at the liquid-to-liquid interface may be promoted by using an emulsion flow method, a method of applying mechanical external forces (such as stirring and vibrating) or another method combining both the above-mentioned methods.
摘要:
A method for separating and recovering trivalent and tetravalent actinoids in a simple and less costly manner without using an organophosphorus compound is provided. This method selectively separates and recovers the tetravalent actinoid plutonium Pu (IV) and the trivalent actinoids americium Am (III) and curium Cm (III) from trivalent lanthanoids Ln (III), etc. with the use of an extractant having a functional group with neutral multidentate ligand activity which is a hybrid donor type organic compound having both of donor atoms, i.e., an oxygen atom and a nitrogen atom.
摘要:
Disclosed is a process for the resolution of a mixture into at least one first fraction and one second fraction, the respective compositions of said fractions differing by at least one element. The process further comprises at least one elementary stage of fractionation, in which at least two inflows are placed in contact, these two flows being a first inflow (10) with low first fraction content, notably in counter-current, and a second inflow (11) with low second fraction content. Two outflows are obtained, said flows being a first outflow (12) enriched in first fraction with respect to the first inflow (10), and a second outflow (13) enriched in second fraction with respect to the second inflow (11). According to the invention, the elementary fractionation stage, which is non-static, is implemented in an elementary fractionation run, at which point at least one mass exchange buffer supply (15) is accumulated, and the elementary stage of fractionation is periodically initiated and repeated.
摘要:
The present invention relates to a method for the chlorination of a sucrose-6-acylate to produce a 4,1′,6′-trichloro-4,1′,6′-trideoxy-galactosucrose-6-acylate wherein said method includes steps of: (i) combining the sucrose-6-acylate with a chlorinating agent in a reaction vehicle comprising a tertiary amide to afford a mixture; (ii) heating said mixture for a heating period in order to provide chlorination of sucrose-6-acylate at the 4, 1′ and 6′ positions thereof; and (iii) quenching the product stream of (ii) to produce a 4,1′,6′-trichloro-4,1′,6′-trideoxy-galactosucrose-6-acylate; wherein before said quenching, a portion of said tertiary amide is removed by extraction into a solvent in which said tertiary amide is at least partially soluble.
摘要:
The particle components may be collected by using a phenomenon that the particle components in the aqueous phase aggregate at the liquid-to-liquid interface. Both of the particle components and the dissolved components in the aqueous phase may be simultaneously collected if combined with liquid-liquid extraction phenomenon that the dissolved components in the aqueous phase are collected into the solvent phase through the liquid-to-liquid interface. The aggregation phenomenon of the particle components at the liquid-to-liquid interface may be promoted by using an emulsion flow method, a method of applying mechanical external forces (such as stirring and vibrating) or another method combining both the above-mentioned methods.
摘要:
An elastic bar member is coupled to an orbiting mass oscillator and the entire assembly is suspended from a cable or the like such that the bar member has freedom of lateral motion and is nakedly immersed in a slurry having particulate material contained therein such as a mineral ore reject from which metal has been extracted. The rotor of the orbiting mass oscillator is driven at a speed such as to generate cycloidal sonic energy in the bar preferably at a frequency such as to set up resonant standing wave vibration of the bar in a cycloidal quadrature pattern. The cycloidal vibrational energy tends to set the surrounding fluid material into a whirling rotation or rotary traveling wave which facilitates the agglomeration or coagulation of the particles in the material and enhances the settling operation to make for more complete separation of the particles from the liquid.
摘要:
The apparatus consists of an upright vertical column for bringing fluid phases into mutual contact, comprising a set of perforated trays and means for bringing said trays and the fluid phases into relative movement. Each tray is provided with both small and large apertures of which the former designed for passing a dispersed phase of phases are positioned opposite the large apertures in the adjacent trays, and vice versa, the lastmentioned large apertures being designed for passing a continuous phase or phases. Relations between areas of the two apertures sized, between the number of large apertures and the sum of all apertures, and between total perforated and solid areas of the tray are specified. The large apertures are provided with slanted, or tangential extensions as to control a helical phase flow course respective to the column axis. The apparatus operates upon counterflow principle, a lighter phase ascending to the column top and a heavier phase falling down to the bottom thereof. The group of small and large apertures are regularly staggered in the trays in such a way that the path of the crossflow of the continuous phase between large apertures of adjacent trays is sufficiently long to secure the desired efficiency of the extraction but simultaneously sufficiently short to avoid too long pressure gradients.