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    Sulfur recovery unit
    5.
    发明授权
    Sulfur recovery unit 有权
    硫回收装置

    公开(公告)号：US09556030B2

    公开(公告)日：2017-01-31

    申请号：US14535428

    申请日：2014-11-07

    申请人： Saudi Arabian Oil Company

    发明人： John P. O'Connell

    IPC分类号： B01J12/00 ,  C01B17/04 ,  B01J19/24 ,  B01D53/52

    CPC分类号： C01B17/0456 ,  B01D53/52 ,  B01D2257/304 ,  B01J19/245 ,  B01J2219/24 ,  C01B17/04 ,  Y02P20/129

    摘要： A sulfur recovery unit for processing an acid gas feed to recover elemental sulfur, the sulfur recovery unit comprising a reaction furnace configured to burn the acid gas feed, an oxygen source, and a fuel gas to create a furnace outlet stream, the acid gas feed comprises hydrogen sulfide which is converted to elemental sulfur, a waste heat boiler configured to capture heat from the furnace outlet stream to create a cooled stream, a condenser configured to condense the cooled stream to produce a waste gas stream and a condensed stream comprising elemental sulfur, a thermal oxidizer configured to burn the waste gas stream to create a sulfur dioxide rich stream, and a sulfur dioxide scrubbing unit configured to remove the amount of sulfur dioxide from the sulfur dioxide rich stream to create an effluent stream and a recycle stream recycled to the reaction furnace.

    摘要翻译： 用于处理酸性气体原料以回收元素硫的硫回收单元，所述硫回收单元包括构造成燃烧所述酸性气体进料，氧源和燃料气体以产生炉出口流的反应炉，所述酸性气体进料 包括转化为元素硫的硫化氢，被配置为从炉出口流捕获热量以产生冷却的流的废热锅炉，被配置为冷凝冷却的流以产生废气流的冷凝器和包含元素硫的冷凝流 ，热氧化器，其被配置为燃烧废气流以产生富二氧化物流;以及二氧化硫洗涤单元，其被配置为从富二氧化物流中除去二氧化硫的量以产生流出物流和循环流 反应炉。

    PROCESS FOR DEGASSING CONDENSED SULFUR FROM A CLAUS SULFUR RECOVERY SYSTEM
    6.
    发明申请
    PROCESS FOR DEGASSING CONDENSED SULFUR FROM A CLAUS SULFUR RECOVERY SYSTEM 有权
    从酸性硫回收系统中分解浓缩的硫磺的方法

    公开(公告)号：US20150376007A1

    公开(公告)日：2015-12-31

    申请号：US14845744

    申请日：2015-09-04

    申请人： PHILLIPS 66 COMPANY

    发明人： Alfred E. Keller

    IPC分类号： C01B17/04

    CPC分类号： C01B17/0456 ,  B01D5/0012 ,  B01D5/0051 ,  B01D5/0093 ,  B01D19/0052 ,  C01B17/0232 ,  C01B17/0447

    摘要： A process of producing degassed liquid sulfur using process gas containing H2S to agitate the liquid sulfur being degassed while in contact with a degassing catalyst. Process gas is less costly and less complicated and quickly accomplishes substantial degassing rendering the liquid sulfur much safer in storage and transportation.

    摘要翻译： 使用含有H 2 S的工艺气体来生产脱气液体硫的方法，以搅拌与脱气催化剂接触的脱硫液体硫。 工艺气体成本较低且复杂度较低，并且迅速完成了大量的脱气，使得液体硫在储存和运输中更加安全。

    PROCESS FOR IN-SITU PRODUCTION OF LOW DISSOLVED HYDROGEN SULFIDE, DEGASSED, SULFUR FROM CLAUS SULFUR RECOVERY
    7.
    发明申请
    PROCESS FOR IN-SITU PRODUCTION OF LOW DISSOLVED HYDROGEN SULFIDE, DEGASSED, SULFUR FROM CLAUS SULFUR RECOVERY 有权
    低硫磺硫化氢生产工艺，酸洗，硫酸从硫酸盐还原

    公开(公告)号：US20140377155A1

    公开(公告)日：2014-12-25

    申请号：US14303946

    申请日：2014-06-13

    申请人： PHILLIPS 66 COMPANY

    发明人： Alfred E. Keller

    IPC分类号： C01B17/04 ,  B01D5/00

    CPC分类号： B01D53/002 ,  B01D5/00 ,  B01D5/0009 ,  B01D5/0012 ,  B01D5/0051 ,  B01D5/0069 ,  B01D5/0093 ,  B01J8/02 ,  C01B17/0232 ,  C01B17/0439 ,  C01B17/0447 ,  C01B17/0456 ,  C01B17/0469 ,  C01B17/05 ,  F25J1/00 ,  F25J1/0002

    摘要： A process of producing degassed liquid sulfur within a vertical sulfur condenser may include providing a plurality of condenser tubes within an external casing; submerging exit ends of the plurality of condenser tubes within a liquid reservoir resulting in submerged exit ends of the plurality of condenser tubes; passing the Claus process gas into an inlet end of the plurality of condenser tubes; condensing the Claus process gas within the condenser tubes to produce condensed Claus process gas within the plurality of condenser tubes; and collecting the condensed Claus process gas in the liquid reservoir upon exiting of the condensed Claus process gas at an exit end of the plurality of condenser tubes. The process may further include converting hydrogen sulfide by the Claus reaction 2H2S+SO23/xSx+2H2O, and decomposing polysulfanes to hydrogen sulfide and sulfur, wherein elemental sulfur is freed from hydrogen sulfide.

    摘要翻译： 在垂直硫冷凝器内产生脱气液硫的过程可包括在外壳内提供多个冷凝器管; 将多个冷凝器管的出口端浸没在液体储存器内，导致多个冷凝器管的浸没出口端; 将Claus工艺气体送入多个冷凝器管的入口端; 在所述冷凝器管内冷凝所述Claus工艺气体以在所述多个冷凝器管内产生冷凝的Claus工艺气体; 以及在所述多个冷凝器管的出口端离开所述冷凝的Claus工艺气体之后，在所述液体储存器中收集所述冷凝的Claus工艺气体。 该方法可以进一步包括通过克劳斯反应2H 2 S + SO 2 3 / xS x + 2H 2 O转化硫化氢，并将多硫烷分解成硫化氢和硫，其中元素硫不含硫化氢。

    APPARATUS FOR IN-SITU PRODUCTION OF LOW DISSOLVED HYDROGEN SULFIDE, DEGASSED, SULFUR FROM CLAUS SULFUR RECOVERY
    8.
    发明申请
    APPARATUS FOR IN-SITU PRODUCTION OF LOW DISSOLVED HYDROGEN SULFIDE, DEGASSED, SULFUR FROM CLAUS SULFUR RECOVERY 有权
    用于生产低硫酸氢硫化物的装置，从硫酸回收中回收的硫酸

    公开(公告)号：US20140374070A1

    公开(公告)日：2014-12-25

    申请号：US14303937

    申请日：2014-06-13

    申请人： PHILLIPS 66 COMPANY

    发明人： Alfred E. Keller

    IPC分类号： B01D53/00

    CPC分类号： B01D53/002 ,  B01D5/00 ,  B01D5/0009 ,  B01D5/0012 ,  B01D5/0051 ,  B01D5/0069 ,  B01D5/0093 ,  B01J8/02 ,  C01B17/0232 ,  C01B17/0439 ,  C01B17/0447 ,  C01B17/0456 ,  C01B17/0469 ,  C01B17/05 ,  F25J1/00 ,  F25J1/0002

    摘要： A horizontal sulfur condenser may include an exterior casing with a plurality of condenser tubes arranged longitudinally within the casing, a liquid sulfur reservoir at a longitudinal end within the exterior casing, and an internal baffle that protrudes into the liquid sulfur reservoir from the surface. The lowest of the plurality of condenser tubes is parallel to a wall of the exterior casing. A Claus process gas inlet is proximate a first end of the plurality of condenser tubes, which are arranged horizontally but are positioned vertically above the sulfur reservoir. A liquid sulfur outlet is located at the liquid sulfur surface. The baffle creates multiple chambers above the sulfur reservoir, such as a first chamber defined by the exterior casing and the baffle to receive condensed Claus sulfur in the liquid reservoir, and a second chamber defined by the exterior casing and the baffle to receive degassed liquid sulfur.

    摘要翻译： 水平硫冷凝器可以包括外壳，其具有在壳体内纵向布置的多个冷凝器管，在外壳内的纵向端部处的液体硫储存器，以及从表面突出到液体硫储存器中的内部挡板。 多个冷凝器管中的最下部平行于外壳的壁。 克劳斯工艺气体入口靠近多个冷凝器管的第一端，其水平布置，但位于硫储存器上方的垂直上方。 液体硫出口位于液硫表面。 挡板在硫储存器上方产生多个室，例如由外壳和挡板限定的第一室，以在液体储存器中容纳冷凝的克劳斯硫，以及由外壳和挡板限定的第二室，以接收脱气的液体硫 。

    Process for the production of sulfur from sulfur dioxide with tail gas recycle
    9.
    发明授权
    Process for the production of sulfur from sulfur dioxide with tail gas recycle 有权
    从尾气回收二氧化硫生产硫的方法

    公开(公告)号：US08425874B2

    公开(公告)日：2013-04-23

    申请号：US13153422

    申请日：2011-06-04

    申请人： Mahin Rameshni ,  Stephen L Santo

    发明人： Mahin Rameshni ,  Stephen L Santo

    IPC分类号： C01B17/04

    CPC分类号： C01B17/0404 ,  B01D2257/302 ,  C01B17/0456 ,  C01B17/0478 ,  C01B17/161

    摘要： The reduction of the gas stream containing sulfur dioxide to elemental sulfur is carried out by reacting a reducing gas, such as natural gas, methanol or a mixture of hydrogen and carbon monoxide, with recycled sulfur and recycled tail gas to produce a stream containing hydrogen sulfide that may be reacted with the gas stream that contains sulfur dioxide. Gas streams with a molar concentration of sulfur dioxide from 1 to 100% may be processed to achieve nearly 100% sulfur recovery efficiency.

    摘要翻译： 将含二氧化硫的气流还原成元素硫是通过还原性气体如天然气，甲醇或氢和一氧化碳的混合物与再循环的硫和循环的尾气反应生成含有硫化氢的物流 其可以与含有二氧化硫的气流反应。 可以加工摩尔浓度为1至100％的二氧化硫的气流，以达到接近100％的硫回收效率。