Process for producing particles
    1.
    发明授权

    公开(公告)号:US09796831B2

    公开(公告)日:2017-10-24

    申请号:US14114682

    申请日:2012-04-24

    IPC分类号: C08K3/34 C08K5/41 C07C381/02

    摘要: A process for producing particles, the process including pulverizing particles of a compound represented by formula (I) with a median diameter (50% D) of over 100 μm by using a pulverizer in the presence of at least one member selected from the group consisting of silica, talc and clay, to obtain particles of the compound represented by formula (I) with a median diameter (50% D) of 100 μm or less, in formula (I), R1 and R2 each independently represent a hydrogen atom or an alkyl group having 1 to 6 carbon atoms, or alternatively, R1 and R2 are inked to each other to form a ring together with the nitrogen atom to which they are bound, m represents an integer of 2 to 9, Mn+ represents H+ or an n-valent metal ion, and n represents an integer of 1 or 2.

    Preparation of thiosulphuric acid derivatives
    4.
    发明授权
    Preparation of thiosulphuric acid derivatives 有权
    硫代硫酸衍生物的制备

    公开(公告)号:US07217834B2

    公开(公告)日:2007-05-15

    申请号:US11105603

    申请日:2005-04-14

    申请人: Hartmuth Buding

    发明人: Hartmuth Buding

    IPC分类号: C07C381/02

    CPC分类号: C07C381/02

    摘要: The invention relates to a novel process for preparing salts of S-alkyl esters of thiosulphuric acid by reacting organic dihalides with thiosulphates in water.

    摘要翻译: 本发明涉及通过使有机二卤化物与硫代硫酸盐在水中反应来制备硫代硫酸的S-烷基酯的盐的新方法。

    Reactive formazan dyes and hydrazones
    8.
    发明授权
    Reactive formazan dyes and hydrazones 失效
    活性甲an染料和腙

    公开(公告)号:US5387674A

    公开(公告)日:1995-02-07

    申请号:US117686

    申请日:1993-09-08

    摘要: There are described formazan dyes of the formula ##STR1## where n is 1 or 2,Kat.sup..sym. is the equivalent of a cation,Me is copper or nickel,X is a radical of the formula CO--O or SO.sub.2 --O,Y is vinyl or a radical of the formula C.sub.2 H.sub.4 --Q, where Q is a group which is detachable under alkaline reaction conditions,the ring A may be substituted and benzofused, the ring B is substituted and may be benzofused, and the ring C may be substituted, the use thereof for dyeing or printing hydroxyl- or nitrogen-containing organic substrates, and novel hydrazones.

    摘要翻译: 描述了通式“IMAGE”的甲an染料,其中n是1或2,Kat(+)是阳离子的当量,Me是铜或镍,X是式CO-O或SO2-O的基团, Y是乙烯基或式C2H4-Q的基团,其中Q是在碱性反应条件下可分离的基团,环A可以被取代和苯并稠合,环B被取代并且可以是苯并稠合的,并且环C可以 被用于染色或印刷含羟基或含氮有机底物和新型腙的用途。

    4,4'-bis-(.beta.-hydroxyethylsulfonyl)-biphenyl and its esters
    10.
    发明授权
    4,4'-bis-(.beta.-hydroxyethylsulfonyl)-biphenyl and its esters 失效
    4,4'-双 - (β-羟乙基磺酰基) - 联苯及其酯

    公开(公告)号:US4659856A

    公开(公告)日:1987-04-21

    申请号:US775138

    申请日:1985-09-12

    摘要: Compounds of the general formula (1) ##STR1## in which the Zs, preferably identical to each other, each denote a hydroxy group or a sulfato, thiosulfato or phosphato group. They can be prepared by first converting biphenyl by sulfochlorination into biphenyl-4,4'-disulfochloride, then reducing the latter with an alkali metal or alkaline earth metal sulfite or hydrogensulfite to sulfinic acid, and in turn reacting the latter with ethylene oxide to give 4,4'-bis-(.beta.-hydroxyethylsulfonyl)-biphenyl, which can be esterified in conventional manner. They are used for modifying and improving the physical and coloristic properties of materials made of natural and/or synthetic polyamide fibers and/or polyurethane fibers and as auxiliaries in dyeing processes for such fiber materials.

    摘要翻译: 其中Z,优选彼此相同的通式(1)的化合物(1)各自表示羟基或硫酸根,硫代硫酸根或磷酸根。 它们可以通过首先通过磺基氯化将联苯转化为联苯-4,4'-二磺酰氯,然后用碱金属或碱土金属亚硫酸盐或亚硫酸氢盐将其还原成亚磺酸,然后将其与环氧乙烷反应,得到 4,4'-双 - (β-羟乙基磺酰基) - 联苯,其可以常规方式酯化。 它们用于改善和改善由天然和/或合成聚酰胺纤维和/或聚氨酯纤维制成的材料的物理和色彩特性,并用作这种纤维材料的染色工艺中的助剂。