摘要:
The present disclosure relates to various testing methods that can be applied to oils, such as pyrolysis oils. Different testing methods can be used to determine the oxidative stability of an oil. The testing methods may also be used to differentiate between various oils and to determine the effectiveness of various antioxidants on the oxidative stability of an oil.
摘要:
A method for characterizing refinery feedstocks according to their corrosivity is provided. The characterization is based on any of: dissociation of acids in the crude, breakup of naphthenic acid molecular associations, and/or dissociation of sulfur compounds in the feedstocks. In one embodiment, the characterization is done via vibrational spectroscopic measurements over a range of temperature, e.g., from ambient to 700° F. The method can be practiced in any of refinery, terminal, and laboratories. It can be used in conjunction with models and hardware to optimize the usage of refinery feedstocks in the blending and valuation of the feedstocks.
摘要:
A thermal oxidation tester is shown for determining thermal stability of a fluid, particularly hydrocarbons when subjected to elevated temperatures. The tendency of the heated fluid to oxidize and (1) form deposits on a surface of a heater tube and (2) form solids therein, are both measured at a given flow rate, temperature and time. The measured results are used to determine whether a fluid sample passes or fails the test. At the beginning of each test, the test sample is aerated with dry air until saturation. Simultaneously, the test equipment is primed to remove pockets of air there from. After each test, the test equipment is flushed to remove the test sample there from.
摘要:
An apparatus for characterizing parameters for the cracking, in-situ combustion, and upgrading of hydrocarbons includes a reactor defining a chamber, a temperature probe operably associated with the reactor, and a gas inlet in fluid communication with the chamber. The apparatus further comprises a gas outlet in fluid communication with the chamber and an electromagnetic radiation attenuating material configured to heat the reactor when the electromagnetic radiation attenuating material is irradiated by electromagnetic radiation.
摘要:
A process for placing a roller burnished finish on the central portion of an unfinished lathe-turned heater tube includes controlling the rotational speed of the burnishing rollers and the pressure of the burnishing rollers against the central portion of the heater tube so that tooling marks are no longer apparent under substantially 10× magnification and the length of the central portion of the heater tube increases by no more than 0.002 inches per inch of length of the central portion of the heater tube.
摘要:
A novel method for measuring a deposit point is provided, which makes it possible to quickly and accurately measure a cloud point. A test sample is irradiated at an angle of incidence .theta. with an incoming light beam which satisfies an expression .theta.
摘要:
Samples of a petroleum oil stream (e.g. crude oil feed stream to a refinery) are continually monitored to determine incompatible asphaltenes therein and the rate of antifoulant is adjusted in response to changes in the level of incompatible asphaltenes. The method of the present invention employs thin layer chromatographic films for separating incompatible asphaltenes and for measuring an optical property indicative of the incompatible asphaltenes, and for varying antifoulant addition in response to changes of the optical property measured.
摘要:
A method for determining the fouling tendency of an asphaltene containing petroleum stream such as crude oil by the use of thin layer chromatography. The chromatogram of a crude oil formed in the presence of an asphaltene antisolvent which exhibits a fouling tendency developed a distinct, dark ring or disk.
摘要:
An apparatus for testing engine oils and in particular oils to be used in compression ignition engines. The apparatus includes a receptacle in which a sample of the liquid oil to be tested is poured. The receptacle has a cover plate with an opening. A test plate is mounted in the opening of the cover plate and seals the receptacle. A shaft with radial projections is mounted in the receptacle and submerged in the liquid oil to be tested. When the shaft rotates the projections splash oil against the test plate. First temperature sensing means are mounted in the test plate and second temperature sensing means are submerged in the liquid oil. A heating element is mounted over the cover plate. The first temperature sensing means are operatively connected to the heating element via a thermal regulator to thereby maintain the test plate at a preselected temperature. The second temperature sensing means serve to maintain the liquid oil sample at a preselected temperature.