摘要:
POTASSIUM CHLORIDE AND WATER AND ADDED TO A FIRST AQUEOUS NITRATE-CHLORIDE MOTHER LIQUOR HAVING A
K+/(K++NH4+)
MOL RATIO OF NOT MORE THAN ABOUT 0.37 TO FORM A POTASSIUM NITRATE CRYSTALLIZATION MEDIUM. THE MEDIUM IS COOLED TO PRECIPITATE CRYSTALLINE POTASSIUM NITRATE AND FORM A SECOND NITRATE-CHLORIDE MOTHER LIQUOR. AFTER SEPARATION OF THE POTASSIUM NITRATE, AMMONIUM NITRATE IS ADDED TO THE SECOND MOTHER LIQUOR, ALL ADDED WATER IS EVAPORATED TO FORM AN AMMONIUM CHLORIDE CRYSTALLIZATION MEDIUM, AND AMMONIUM CHLORIDE IS CRYSTALLIZED AT A TEMPERATURE HIGHER THAN THE POTASSIUM NITRITE CRYSTALLIZATION. THE AMMONIUM CHLORIDE IS SEPARATED, AND THE RESIDUAL MOTHER LIQUOR IS RECYCLED TO RECEIVE ADDITIONAL POTASSIUM CHLORIDE AND WATER. THE MAINTENANCE OF A NET BALANCE OF COM-
PONENTS PERMITS CONTINUOUS OPERATION OF A CYCLIC METATHESIS OPERATION.
摘要:
1,099,318. Crystallizing. SOCIETA' EDISON. June 9, 1965 [June 10, 1964], No. 24466/ 65. Heading B1G. [Also in Division F4] Cooling and crystallization of a saturated solution is effected in a vessel by means of water-cooled heat exchange tubing 1 resiliently suspended from a frame 2 which is vibrated by a cam operated by a motor 18. The tubing is in the form of two bundles operating in parallel, each bundle comprising a plurality of tubes, each connected to the next alternately at the top and bottom. The solution is stirred by a propellor 19 between the bundles.