Monodisperse nanoparticles and method of making
    3.
    发明授权
    Monodisperse nanoparticles and method of making 失效
    单分散纳米颗粒和制备方法

    公开(公告)号:US07820124B1

    公开(公告)日:2010-10-26

    申请号:US11543608

    申请日:2006-10-05

    IPC分类号: C07C2/00

    摘要: A material comprising a plurality of nanoparticles. Each of the plurality of nanoparticles includes at least one of a metal phosphate, a metal silicate, a metal oxide, a metal borate, a metal aluminate, and combinations thereof. The plurality of nanoparticles is substantially monodisperse. Also disclosed is a method of making a plurality of substantially monodisperse nanoparticles. The method includes providing a slurry of at least one metal precursor, maintaining the pH of the slurry at a predetermined value, mechanically milling the slurry, drying the slurry to form a powder; and calcining the powder at a predetermined temperature to form the plurality of nanoparticles.

    摘要翻译: 包含多个纳米颗粒的材料。 多个纳米颗粒中的每一个包括金属磷酸盐,金属硅酸盐,金属氧化物,金属硼酸盐,金属铝酸盐及其组合中的至少一种。 多个纳米颗粒基本上是单分散的。 还公开了制备多个基本上单分散纳米颗粒的方法。 该方法包括提供至少一种金属前体的浆料,将浆料的pH保持在预定值,机械研磨浆料,干燥浆料以形成粉末; 并在预定温度下煅烧粉末以形成多个纳米颗粒。

    Borate crystals for optical frequency conversion
    4.
    发明申请
    Borate crystals for optical frequency conversion 有权
    硼酸盐晶体用于光学变频

    公开(公告)号:US20050247918A1

    公开(公告)日:2005-11-10

    申请号:US10520364

    申请日:2003-07-14

    摘要: Novel nonlinear optical materials are described having the general formula 5MxM′yScz(BO3)4 where M and M′ are metals, typically rare earth metals, and the sum of x, y, and z is about four. One example of such a material is La0.7Y0.3SC3(BO3)4. Exemplary crystalline materials according to the general formula exhibit useful optical characteristics and desirable physical properties for nonlinear optical applications. Novel compositions and devices using the nonlinear optical materials also are described.

    摘要翻译: 描述了具有以下通式的新型非线性光学材料:具有通式5 M x S(z 3) 其中M和M'是金属,通常是稀土金属,x,y和z之和约为4。 这种材料的一个例子是La 0.7 O 3(3/4)4(3) / SUB>。 根据通式的典型结晶材料对于非线性光学应用显示出有用的光学特性和期望的物理性质。 还描述了使用非线性光学材料的新型组合物和装置。

    Nonaborate compositions and their preparation
    6.
    发明申请
    Nonaborate compositions and their preparation 失效
    无硼组合物及其制备

    公开(公告)号:US20030109751A1

    公开(公告)日:2003-06-12

    申请号:US10181628

    申请日:2002-07-19

    发明人: David M Schubert

    IPC分类号: C07F005/02 C01B035/10

    摘要: A family of borate compounds containing an isolated (finite) nonaborate anion with the structural formula nullB9O12(OH)6null3null. Preferred amine nonaborate compounds have a resolved oxide formula of A2O.3B2O3.2H2O, where A is the monovalent cation of an amine salt, such as guanidinium and imidazolium. Also provided is a method for preparing these compounds by crystallization from an aqueous solution under mild conditions without the formation of significant amounts of by-products. These compounds have potential application as precursors for the production of advanced boron nitride ceramic materials, and as flame retardants, corrosion inhibitors, and biocides.

    摘要翻译: 含有结构式[B9O12(OH)6] 3-的分离(有限)非硼酸阴离子的硼酸盐化合物族。 优选的胺非硼酸盐化合物具有分解的氧化物配方为A 2 O 3 B 2 O 3·2H 2 O,其中A是胺盐的一价阳离子,例如胍和咪唑鎓。 还提供了一种通过在温和条件下从水溶液中结晶而制备这些化合物而不形成大量副产物的方法。 这些化合物可用作生产先进的氮化硼陶瓷材料以及作为阻燃剂,腐蚀抑制剂和杀生物剂的前体。

    Zinc borate, and production method and use thereof
    7.
    发明申请
    Zinc borate, and production method and use thereof 失效
    硼酸锌及其制备方法和用途

    公开(公告)号:US20030030042A1

    公开(公告)日:2003-02-13

    申请号:US09914789

    申请日:2001-09-05

    IPC分类号: C09K021/00 C08K003/38

    摘要: A zinc borate having a particular crystallite size and containing very little sodium components and a method of preparing the same. The zinc borate has a particular chemical composition, has a crystallite size of not smaller than 40 nm as found from diffraction peaks of indexes of planes of (020), (101) and (200) in the X-ray diffraction image (Cu-knull) and contains sodium components in amounts of not larger than 100 ppm as measured by the atomic absorptiometric method.

    摘要翻译: 具有特定微晶尺寸并且含有非常少的钠组分的硼酸锌及其制备方法。 硼酸锌具有特定的化学成分,其X射线衍射图像(Cu-Cu)中的(020),(101)和(200)的平面指数的衍射峰所得到的微晶尺寸不小于40nm, kalpha),并且通过原子吸收光度法测量的含有不大于100ppm的钠组分。

    Method for generating laser light and laser crystal
    8.
    发明授权
    Method for generating laser light and laser crystal 失效
    产生激光和激光晶体的方法

    公开(公告)号:US06510169B2

    公开(公告)日:2003-01-21

    申请号:US09782787

    申请日:2001-02-14

    IPC分类号: H01S316

    摘要: A crystalline material for optically pumped solid state lasers has the chemical composition of M3RE1-x Ybx(BO3)3, where M is selected from the group Mg, Ca, Sr, Ba, and Ra, optionally replaced at least partially with another element from this group, RE is selected from the group Sc, Y, Lu, and Y partially replaced with Lu, and x is greater than or equal to 0 and less than or equal to 1. The material is useful for preparing lasers having high average initial power and short pulse duration, and has flat amplification and fluorescence spectra, high thermal conductivity and a large emission cross-section.

    摘要翻译: 用于光泵浦固体激光器的结晶材料具有M3RE1-x Ybx(BO3)3的化学组成,其中M选自Mg,Ca,Sr,Ba和Ra组,任选地至少部分地与另一元素 该组RE选自Sc,Y,Lu和Y部分被Lu替代,x大于或等于0且小于或等于1.该材料可用于制备具有高平均初始值的激光 功率和短脉冲持续时间,具有平坦的放大和荧光光谱,高导热性和大的发射截面。

    Borate phosphor synthesis using boron nitride
    9.
    发明授权
    Borate phosphor synthesis using boron nitride 失效
    硼酸盐磷光体合成使用氮化硼

    公开(公告)号:US5776368A

    公开(公告)日:1998-07-07

    申请号:US916383

    申请日:1997-08-22

    申请人: Chung-Nin Chau

    发明人: Chung-Nin Chau

    摘要: An improved method for a single step firing synthesis of borate phosphors wherein at least about half the amount of a volatile, low melting point, boron source such as boric acid or boron oxide is replaced with an equivalent amount of boron nitride. The method having the advantages of a single step firing and providing better control over the stoichiometry of the phosphor.

    摘要翻译: 用于硼酸盐荧光体的单步烧成合成的改进方法,其中至少约一半的挥发性,低熔点硼源如硼酸或氧化硼的量被等量的氮化硼代替。 该方法具有单步烧制的优点,并且能够更好地控制荧光体的化学计量。