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78 条记录 (耗时 0.042 秒)

    Process for the preparation of N,N-dimethyl-N-(2-bromo-4-methylphenyl)-triazene
    1.
    发明授权
    Process for the preparation of N,N-dimethyl-N-(2-bromo-4-methylphenyl)-triazene 失效
    制备N，N-二甲基-N-（2-溴-4-甲基苯基） - 三氮烯的方法

    公开(公告)号：US4394309A

    公开(公告)日：1983-07-19

    申请号：US249247

    申请日：1981-03-30

    申请人： Claus Stolzer

    发明人： Claus Stolzer

    IPC分类号： C07C245/24 ,  C07C17/093 ,  C07C41/22 ,  C07C67/00 ,  C07C241/00 ,  C07C113/00 ,  C07C87/60 ,  C07C113/04

    CPC分类号： C07C17/093 ,  C07C231/12 ,  C07C241/00

    摘要： A process for the preparation of N,N-dimethyl-N'-(2-bromo-4-methyl-phenyl)-triazene of the formula ##STR1## comprising (a) reacting N-acetyl-p-toluidine of the formula ##STR2## with bromine at a temperature between about 0.degree. and 100.degree. C., to give the intermediate product of the formula ##STR3## (b) reacting the intermediate product with hydrochloric acid by either (i) adding a dilute solution of aqueous hydrochloric acid to the intermediate product in its reaction solution and heating the mixture to a temperature between about 50.degree. and 120.degree. C., or(ii) precipitating the intermediate product from its reaction solution by mixing with water and filtering off, and without purification or drying heating the precipitate with dilute aqueous hydrochloric acid to a temperature between about 50.degree. and 120.degree. C., thereby to form a solution of 2-bromo-4-methylaniline hydrochloride, (c) reacting the resulting aqueous solution with an alkali metal nitrite at a temperature between about -20.degree. and +30.degree. C., and (d) reacting the product with dimethylamine at a temperature between about 0.degree. and 50.degree. C.

    摘要翻译： 制备下式的N，N-二甲基-N' - （2-溴-4-甲基 - 苯基） - 三烯的方法，包括：（a）使下式的N-乙酰基 - 对甲苯胺， 在约0℃至100℃的温度下加入溴，得到中间产物，其结构式如下：（b）使中间产物与盐酸反应，方法是（i）加入稀盐酸水溶液 在其反应溶液中向中间产物加酸，并将混合物加热至约50至120℃的温度，或（ii）通过与水混合并过滤从而将其从反应溶液中沉淀出来，并且不经纯化或 干燥，用稀盐酸水溶液将沉淀物加热至约50〜120℃，由此形成2-溴-4-甲基苯胺盐酸盐溶液，（c）使所得水溶液与碱金属亚硝酸盐 在约-20℃的温度下 EG和+ 30℃，和（d）在约0℃至50℃的温度下使产物与二甲基胺反应。

    P-(Alkenylamino) phenylamines
    3.
    发明授权
    P-(Alkenylamino) phenylamines 失效
    P-（烯基氨基）苯胺

    公开(公告)号：US4310694A

    公开(公告)日：1982-01-12

    申请号：US224982

    申请日：1981-01-14

    申请人： Josef Ehrenfreund

    发明人： Josef Ehrenfreund

    IPC分类号： A01N47/34 ,  C07C275/54 ,  C07C87/60 ,  C07C127/22

    CPC分类号： C07C275/54 ,  A01N47/34

    摘要： Novel substituted N-(p-aminophenyl)-N'-benzoyl ureas of the formula ##STR1## wherein each of R.sub.1 and R.sub.2 independently is C.sub.1 -C.sub.4 alkyl or C.sub.3 -C.sub.5 alkenyl, each of R.sub.3 and R.sub.4 independently is chlorine or bromine, and each of R.sub.5 and R.sub.6 independently is hydrogen, fluorine or chlorine, with the proviso that R.sub.5 and R.sub.6 are not both simultaneously hydrogen, processes for the manufacture of these compounds and compositions containing them for use in pest control, especially for controlling insects harmful to plants and animals. The novel compounds inhibit feeding damage and have in particular a pronounced ovolarvicidal and ovicidal action against plant-destructive insects.

    摘要翻译： 新颖的取代的N-（对氨基苯基）-N'-苯甲酰基脲，其中R 1和R 2各自独立地是C 1 -C 4烷基或C 3 -C 5烯基，R 3和R 4各自独立地是氯或溴， R5和R6独立地是氢，氟或氯，条件是R5和R6不同时为氢，制备这些化合物的方法和含有它们的组合物用于病虫害防治，特别是用于防治对植物有害的昆虫， 动物。 新型化合物抑制饲料损伤，特别是对植物破坏性昆虫具有明显的杀卵和杀卵作用。

    Novel 2-sulphonyl- (or -sulphinyl)-2'-aminoacetophenones
    4.
    发明授权
    Novel 2-sulphonyl- (or -sulphinyl)-2'-aminoacetophenones 失效
    新的2-磺酰基 - （或 - 亚磺酰基）-2'-氨基苯乙酮

    公开(公告)号：US4263455A

    公开(公告)日：1981-04-21

    申请号：US79605

    申请日：1979-09-27

    申请人： Pier G. Ferrini ,  Richard Goschke ,  Alfred Sallmann ,  Alberto Rossi

    发明人： Pier G. Ferrini ,  Richard Goschke ,  Alfred Sallmann ,  Alberto Rossi

    IPC分类号： A61K31/135 ,  A61K31/18 ,  A61K31/255 ,  A61K31/44 ,  A61P7/02 ,  A61P29/00 ,  C07C67/00 ,  C07C313/00 ,  C07C315/04 ,  C07C317/28 ,  C07D213/70 ,  C07D213/71 ,  C07C87/60 ,  C07C97/10

    CPC分类号： A61K31/255

    摘要： The invention relates to novel ortho-aminoacetophenones of the formula I ##STR1## and their tautomers, in which Z is hydrogen, halogen, lower alkyl, cycloalkyl, lower alkoxy, trifluoromethyl, nitro or substituted or unsubstituted sulphamoyl, m is 1 or 2, R is hydrogen, aryl or lower alkyl, R.sub.1 is hydrogen or lower alkyl, R.sub.2 is lower alkyl, cycloalkyl, aryl, cycloalkyl-lower alkyl, aryl-lower alkyl or substituted or unsubstituted pyridyl, R.sub.3 is hydrogen or lower alkyl and n is 1 or 2, with the exception of 2'-[N-(p-methoxyphenyl)-amino]-2-(methyl-sulphinyl)-acetophenone, 2'-amino-2-(methylsulphinyl)-acetophenone, 2'-amino-5'-chloro-2-(methylsulphinyl)-acetophenone, 2'-methylamino-2-(methylsulphinyl)-acetophenone, 2'-amino-5'-methyl-2-(methylsulphinyl)-acetophenone, 2'-amino-4'-chloro-2-(methylsulphinyl)-acetophenone, 2'-amino-6'-chloro-2-(methylsulphinyl)-acetophenone, 2'-amino-5',6'-dimethoxy-2-(methylsulphinyl)-acetophenone and 2'-amino-4',5'-dimethoxy-2-(methylsulphinyl)-acetophenone, and also to their salts.These compounds have a fibrinolytic and an antiinflammatory action.

    摘要翻译： 本发明涉及式I（I）的新型邻氨基苯乙酮及其互变异构体，其中Z为氢，卤素，低级烷基，环烷基，低级烷氧基，三氟甲基，硝基或取代或未取代的氨磺酰基，m为1 或2，R是氢，芳基或低级烷基，R1是氢或低级烷基，R2是低级烷基，环烷基，芳基，环烷基 - 低级烷基，芳基 - 低级烷基或取代或未取代的吡啶基，R3是氢或低级烷基， n为1或2，2' - [N-（对甲氧基苯基） - 氨基] -2-（甲基 - 亚磺酰基） - 苯乙酮，2'-氨基-2-（甲基亚磺酰基） - 苯乙酮，2' - 氨基-5'-氯-2-（甲基亚磺酰基） - 苯乙酮，2'-甲基氨基-2-（甲基亚磺酰基） - 苯乙酮，2'-氨基-5'-甲基-2-（甲基亚磺酰基） - 苯乙酮， 氨基-4'-氯-2-（甲基亚磺酰基） - 苯乙酮，2'-氨基-6'-氯-2-（甲基亚磺酰基） - 苯乙酮，2'-氨基-5'，6'-二甲氧基-2-（甲基亚磺酰基 ） - 苯乙酮和2'-氨基-4'，5'-二甲氧基-2-（甲基亚磺酰基） - 苯乙酮 ne，以及它们的盐。 这些化合物具有纤维蛋白溶解和抗炎作用。

    Process for preparing 3-chloro- and 3,5-dichloro-anilines
    5.
    发明授权
    Process for preparing 3-chloro- and 3,5-dichloro-anilines 失效
    制备3-氯代和3,5-二氯苯胺的方法

    公开(公告)号：US4193937A

    公开(公告)日：1980-03-18

    申请号：US942711

    申请日：1978-09-15

    申请人： Karlfried Wedemeyer ,  Wolfgang Kiel ,  Werner Evertz

    发明人： Karlfried Wedemeyer ,  Wolfgang Kiel ,  Werner Evertz

    IPC分类号： B01J23/40 ,  B01J37/03 ,  C07C87/52 ,  C07C87/60 ,  C07C93/00 ,  C07C93/08

    CPC分类号： B01J23/40 ,  B01J37/031

    摘要： Analines, meta-substituted by chlorine are prepared by reacting chloro-anilines having the formula ##STR1## wherein X.sup.1 and X.sup.2 are the same or different and represent chlorine, hydrogen or optionally substituted alkyl, aryl, aralkyl, alkoxy or aralkoxy, with one of the radicals X.sup.1 or X.sup.2 representing chlorine when 3-chloroanilines are being prepared andX.sup.1 and X.sup.2 representing chlorine when 3,5-dichloroanilines are being prepared andR.sup.1, R.sup.2 and R.sup.3 are the same or different and represent chlorine, hydrogen or optionally substituted alkyl, aryl, aralkyl, alkoxy or aralkoxy, with at least one of the radicals R.sup.1, R.sup.2 or R.sup.3 representing chlorinewith hydrogen in solution in a neutral or acid medium in the presence of noble metals which are in the elementary form or in the form of compounds and are optionally applied to supports, and in the presence of sulfur or sulfur compounds at elevated temperatures and under pressure.

    摘要翻译： 通过氯取代的分析物通过使具有式“IMAGE”的氯苯胺反应制备，其中X1和X2相同或不同，代表氯，氢或任选取代的烷基，芳基，芳烷基，烷氧基或芳烷氧基， 当制备3-氯苯胺时，X 1或X 2表示氯，X1和X2表示氯，当制备3,5-二氯苯胺时，R 1，R 2和R 3相同或不同，表示氯，氢或任选取代的烷基， 芳基，芳烷基，烷氧基或芳烷氧基，其中R1，R2或R3中的至少一个表示氯，在中性或酸性介质中的溶液中含有氢，在贵金属存在下，其为基本形式或化合物形式 并且任选地在升高的温度和压力下施加到载体上，并在硫或硫化合物的存在下。

    Preparation of o-iodoaniline
    7.
    发明授权
    Preparation of o-iodoaniline 失效
    邻碘苯胺的制备

    公开(公告)号：US3975438A

    公开(公告)日：1976-08-17

    申请号：US468200

    申请日：1974-05-08

    申请人： Ulrich Klabunde

    发明人： Ulrich Klabunde

    IPC分类号： C07C87/60

    CPC分类号： C07C211/52

    摘要： Described is the process of interconverting p-iodoaniline and o-iodoaniline, particularly converting p-iodoaniline to o-iodoaniline overall, by heating the former in the presence of aniline and, optionally, a mineral or organic acid.

    摘要翻译： 描述了相互转化对碘苯胺和邻碘苯胺的方法，特别是通过在苯胺和任选的矿物或有机酸的存在下加热前者，特别是将对碘苯胺全部转化成邻碘苯胺。