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    Method to recover free fatty acids from fats and oils
    3.
    发明授权
    Method to recover free fatty acids from fats and oils 有权

    公开(公告)号：US10465144B2

    公开(公告)日：2019-11-05

    申请号：US16106570

    申请日：2018-08-21

    Applicant: Corn Oil One, LLC

    Inventor： Mohan Prasad A. Dasari ,  Hugh Tallant Warren ,  Kidron Joel Knox ,  Charles C. Gallop

    IPC: C11B3/06 ,  C11B3/00 ,  C11B7/00 ,  C11B3/16 ,  C11B13/02

    Abstract: Methods for producing oil from distillers corn oil having high free fatty acid content are provided. In the method, distiller's corn oil is treated with a mixture including an alcohol to result in a low-free fatty acid oily phase and an alcohol phase. The mixture may also include an alkali. The alcohol may be a monohydric alcohol and an aqueous alcohol, such as an aqueous alcohol having a concentration of at least about 15% alcohol-by-weight. The low-free fatty acid phase may include oil and at least one impurity. The low-free fatty acid phase may be cooled, and the oil may be separated from the at least one impurity using membrane filtration.

    METHOD TO DESTABILIZE EMULSION FEEDSTOCKS FOR THE RECOVERY OF VALUABLE PRODUCTS
    7.
    发明申请
    METHOD TO DESTABILIZE EMULSION FEEDSTOCKS FOR THE RECOVERY OF VALUABLE PRODUCTS 审中-公开

    公开(公告)号：US20170298293A1

    公开(公告)日：2017-10-19

    申请号：US15479734

    申请日：2017-04-05

    Applicant: RRIP, LLC

    Inventor： Mohan Prasad A. Dasari ,  Hugh Tallant Warren

    IPC: C11B13/00 ,  C11B13/02

    CPC classification number: C11B13/00 ,  A23J7/00 ,  A23K20/174 ,  C07C29/095 ,  C07C29/76 ,  C07C213/08 ,  C07C213/10 ,  C07C227/28 ,  C07C227/40 ,  C11B3/00 ,  C11B7/00 ,  C11B11/00 ,  C11B13/02 ,  Y02W30/74

    Abstract: Provided are methods to destabilize emulsion feedstocks. Benefits of the provided methods include a reducing or eliminating the amount of acid necessary to process the feedstocks, less processing time, cleaner separation of the resulting phases, and increased recovery of valuable products. In the methods, a moderate temperature is applied to the feedstock to create a first mixture. The moderate temperature may be between 120 and 220 degrees Celsius. The first mixture is mixed at the moderate temperature, such as by staged mixing in some embodiments. Moreover, the first mixture is retained at the moderate temperature for up to six hours. The first mixture is separated into an oil phase, convoluted phase, and a water phase. In some embodiments, the moderate temperature may be 125 to 150 degrees Celsius, such as between 125 and 130 degrees Celsius. Moreover, the first mixture may be retained at the moderate temperature for between forty-five minutes and four hours, such as from two to four hours. The separation may occur at the moderate temperature.

    Method and arrangement for the separation of tall oil products from black liquor
    8.
    发明授权
    Method and arrangement for the separation of tall oil products from black liquor 有权

    公开(公告)号：US09719048B2

    公开(公告)日：2017-08-01

    申请号：US14778384

    申请日：2014-03-20

    Applicant: Anders Goran Hofstedt

    Inventor： Anders Goran Hofstedt

    IPC: C11B13/00 ,  D21C11/00 ,  C11B13/02

    CPC classification number: C11B13/005 ,  C11B13/02 ,  D21C11/0007 ,  Y02W30/74

    Abstract: A method and arrangement for separating tall oil products from a black liquor-containing boiling liquid that has been drained off, was produced within a kraft mill chip digester, and includes a fibrous cellulose material in a mixture with the black liquor and tall oil products, and where the boiling liquid is separated in a separation unit arranged to mechanically separate the boiling liquid into a fibrous cellulose material and a mixture of mixed black liquor and tall oil products, where the mixture of boiling liquid and tall oil products is brought to a separation tank, the separation tank being a gravity separation tank, and adapted to be emptied in a discontinuous manner of the tall oil product collected and concentrated therein, the tall oil products being floated on top of and above a fraction of mixed black liquor, where the tall oil products is brought to a centrifugal separator.

    Process for the recovery of fatty acids from discarded solid soap materials
    9.
    发明授权
    Process for the recovery of fatty acids from discarded solid soap materials 失效
    废弃固体肥皂材料回收脂肪酸的方法

    公开(公告)号：US4464305A

    公开(公告)日：1984-08-07

    申请号：US421975

    申请日：1982-09-23

    Applicant: Charles H. Patrick, Jr.

    Inventor： Charles H. Patrick, Jr.

    IPC: C11B13/02 ,  C09F5/00 ,  C11B1/00

    CPC classification number: C11B13/02 ,  Y02W30/74

    Abstract: A process for the recovery of fatty acids from discarded solid soap material comprises the steps of:(a) stirring discarded solid soap material into a melt of one or more fatty acids at the melting temperature of the discarded soap which is usually from about 40.degree. C. to about 180.degree. C. until the soap material has dissolved in the fatty acid melt;(b) adding to the thus-produced solution of soap material in the fatty acid melt an amount of an undiluted acid sufficient to convert the soap material to free fatty acid and form one or more alkali metal salts, and heating and stirring at about 40.degree. C. to about 180.degree. C. to produce free fatty acid and one or more alkali metal salts;(c) separating the freed fatty acid in the fatty acid melt from the thus-produced salt of one or more alkali metals; and(d) refining freed fatty acids using filtration, distillation, decolorization, deodorization, etc.It is preferred that the lower melt temperatures be utilized to avoid discoloration, but time requirements dictated by the varying composition of the soap may make the use of the more elevated temperatures expedient.

    Abstract translation: 从废弃的固体肥皂材料中回收脂肪酸的方法包括以下步骤：（a）在废皂的熔融温度下将废弃的固体皂物质搅拌成一种或多种脂肪酸的熔体，通常为约40℃ C.至约180℃，直到皂材料溶解在脂肪酸熔体中; （b）将如此生产的肥皂材料在脂肪酸熔体中加入一定量的未稀释的酸，足以将肥皂材料转化成游离脂肪酸并形成一种或多种碱金属盐，并在约40℃下加热和搅拌 约180℃，以产生游离脂肪酸和一种或多种碱金属盐; （c）从如此生产的一种或多种碱金属盐中分离出脂肪酸熔体中释放的脂肪酸; 并且（d）使用过滤，蒸馏，脱色，除臭等来提炼释放出的脂肪酸。优选使用较低的熔融温度来避免变色，但由皂的不同组成决定的时间要求可以使用 更高的温度方便。

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