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    PROCESS FOR THE PRODUCTION OF METAL FLUORIDE MATERIALS
    35.
    发明申请
    PROCESS FOR THE PRODUCTION OF METAL FLUORIDE MATERIALS 审中-公开
    生产金属氟化物材料的方法

    公开(公告)号：WO2004039732A2

    公开(公告)日：2004-05-13

    申请号：PCT/US2003/034069

    申请日：2003-10-27

    Applicant: PLATINUM RESEARCH ORGANIZATION LLC

    Inventor： GREER, F., Conrad ,  ELSENBAUMER, Ronald, L. ,  OWEN, David, P.

    IPC: C01G49/10

    CPC classification number: B01J35/0013 ,  B01J27/12 ,  C01B7/035 ,  C01B9/08 ,  C01G1/06 ,  C01G49/10

    Abstract: A process for the production of metal fluorides comprising introducing a predetermined weight of anhydrous hydrofluoric acid into a reaction vessel and initiate a mixing action, preheating a predetermined weight of anhydrous metal to a predetermined reaction temperature, introducing aliquots of the anhydrous metal into the reaction vessel at intervals until the entire predetermined weight of the anhydrous metal has been added, removing excess anhydrous hydrofluoric acid from the reaction vessel, and remove a metal fluoride resultant product from the reaction vessel.

    Abstract translation: 一种生产金属氟化物的方法，包括将预定重量的无水氢氟酸引入反应容器中并引发混合作用，将预定重量的无水金属预热至预定的反应温度，将无水金属的等分试样引入反应容器 间隔直到加入了无水金属的整个预定重量，从反应容器中除去过量的无水氢氟酸，并从反应容器中除去金属氟化物。

    PREPARATION OF PURE FERRIC CHLORIDE FROM HYDROCHLORIC ACID SOLUTIONS BY SOLVENT EXTRACTION
    36.
    发明申请
    PREPARATION OF PURE FERRIC CHLORIDE FROM HYDROCHLORIC ACID SOLUTIONS BY SOLVENT EXTRACTION 审中-公开
    溶剂萃取法从氢氯酸溶液中制备纯氯化铁

    公开(公告)号：WO0202833B1

    公开(公告)日：2002-09-26

    申请号：PCT/RU0100231

    申请日：2001-06-18

    Applicant: SKLOKIN LEONID IRINEEVICH ,  KALINNIKOV VLADIMIR TROFIMOVIC ,  SIECKMAN WALTER ,  WADHAWAN SATISH

    Inventor： SKLOKIN LEONID IRINEEVICH ,  KALINNIKOV VLADIMIR TROFIMOVIC ,  SIECKMAN WALTER ,  WADHAWAN SATISH

    IPC: C01G49/00 ,  C22B3/26 ,  C22B7/00 ,  C01G49/10

    CPC classification number: C01G49/0009 ,  C22B3/0009 ,  C22B7/006 ,  Y02P10/234

    Abstract: The present invention relates to a field of preparing high-purity ferric chloride from hydrochloric solutions containing impurities. More specifically the invention concerns a ferric iron extraction from water solutions as a result of concentrated hydrochloric acid interaction with iron-containing concentrates, as a result of multi-stage extraction of ferric chloride from solutions of complicated composition and due to processing of industrial wastes, including spent etching solutions of metallurgical plants after chlorination. The essence of the invention is that the proposed method includes two stages of concentration, extraction, and stripping steps. As an extracting agent use is made of aliphatic alcohol, predominantly octanol-1, octanol-2, 2-ethylgexanol, and decanol-1 or their mixtures. The alcohol content in organic phase is up to 100 %. Attained technical result consists in obtaining high-purity ferric chloride solution with not less than 300 kg/m3 FeCl3 concentration. Ferric chloride recovery is 96-98 % irrespective of the nature of impurities present in a feed hydrochloric solution concurrently with the limitation of waste solutions and optimization of material flows and equipment used. The resulting ferric chloride solutions are feasible for further processing in high performance installations of spray roasting which permit combine in one process receiving of high-purity ferric oxide and regenerated hydrochloric acid of high concentration.

    Abstract translation: 本发明涉及由含有杂质的盐酸溶液制备高纯度氯化铁的领域。 更具体地说，本发明涉及由于浓盐酸与含铁浓缩物相互作用而从水溶液中提取三价铁，这是由于复杂组合物溶液中的多阶段萃取氯化铁和由于工业废物处理而导致的， 包括氯化后的冶金厂废蚀刻溶液。 本发明的实质在于所提出的方法包括两个浓缩步骤，提取步骤和剥离步骤。 作为萃取剂，使用脂肪醇，主要是辛醇-1，辛醇-2,2-乙基己醇和癸醇-1或它们的混合物。 有机相中的酒精含量高达100％。 获得的技术成果是获得含有不低于300 kg / m3 FeCl3浓度的高纯度三氯化铁溶液。 无论在进料盐酸溶液中存在的杂质的性质与废液的限制以及所用材料流和设备的优化同时进行，氯化铁的回收率为96-98％。 所得到的氯化铁溶液可用于喷雾焙烧的高性能装置中的进一步处理，其允许在一个工艺中接收高纯度的氧化铁和高浓度的再生盐酸。

    PREPARATION OF PURE FERRIC CHLORIDE FROM HYDROCHLORIC ACID SOLUTIONS BY SOLVENT EXTRACTION
    37.
    发明申请
    PREPARATION OF PURE FERRIC CHLORIDE FROM HYDROCHLORIC ACID SOLUTIONS BY SOLVENT EXTRACTION 审中-公开
    通过溶剂萃取从氢氯酸溶液中制备纯氯化铜

    公开(公告)号：WO0202833A3

    公开(公告)日：2002-06-27

    申请号：PCT/RU0100231

    申请日：2001-06-18

    Applicant: SKLOKIN LEONID IRINEEVICH ,  KALINNIKOV VLADIMIR TROFIMOVIC ,  SIECKMAN WALTER ,  WADHAWAN SATISH

    Inventor： SKLOKIN LEONID IRINEEVICH ,  KALINNIKOV VLADIMIR TROFIMOVIC ,  SIECKMAN WALTER ,  WADHAWAN SATISH

    IPC: C01G49/00 ,  C22B3/26 ,  C22B7/00 ,  C01G49/10

    CPC classification number: C01G49/0009 ,  C22B3/0009 ,  C22B7/006 ,  Y02P10/234

    Abstract: The present invention relates to a field of preparing high-purity ferric chloride from hydrochloric solutions containing impurities. More specifically the invention concerns a ferric iron extraction from water solutions as a result of concentrated hydrochloric acid interaction with iron-containing concentrates, as a result of multi-stage extraction of ferric chloride from solutions of complicated composition and due to processing of industrial wastes, including spent etching solutions of metallurgical plants after chlorination. The essence of the invention is that the proposed method includes two stages of concentration, extraction, and stripping steps. As an extracting agent use is made of aliphatic alcohol, predominantly octanol-1, octanol-2, 2-ethylgexanol, and decanol-1 or their mixtures. The alcohol content in organic phase is up to 100 %. Attained technical result consists in obtaining high-purity ferric chloride solution with not less than 300 kg/m3 FeCl3 concentration. Ferric chloride recovery is 96-98 % irrespective of the nature of impurities present in a feed hydrochloric solution concurrently with the limitation of waste solutions and optimization of material flows and equipment used. The resulting ferric chloride solutions are feasible for further processing in high performance installations of spray roasting which permit combine in one process receiving of high-purity ferric oxide and regenerated hydrochloric acid of high concentration.

    Abstract translation: 本发明涉及从含有杂质的盐酸溶液制备高纯度氯化铁的领域。 更具体地，本发明涉及由于与含铁浓缩物的浓盐酸相互作用而从水溶液中提取的铁铁，其结果是从复杂组成的溶液和工业废物的处理中多次提取氯化铁， 包括氯化后冶金厂的废蚀刻溶液。 本发明的实质是所提出的方法包括浓缩，萃取和汽提步骤的两个阶段。 作为提取剂，使用脂肪醇，主要是辛醇-1，辛醇-2,2-乙基庚醇和癸醇-1或它们的混合物。 有机相中的醇含量高达100％。 获得的技术成果在于获得不低于300 kg / m3 FeCl3浓度的高纯度氯化铁溶液。 氯化铁回收率为96-98％，与进料盐酸溶液中存在的杂质的性质同时伴随着废液的限制以及所使用的材料流和设备的优化。 所得到的氯化铁溶液在喷射焙烧的高性能装置中进一步加工是可行的，其允许在接收高纯度三氧化二铁和高浓度再生盐酸的一个工艺中结合。

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