摘要:
According to the invention, the shaped bodies are comprised of at least one heavy metal, preferably Fe, Ni, Co, Sn, Mo or W, which can be reduced from a corresponding metal compound at a temperature of less than 1,500 DEG C. The shaped bodies have an outer diameter ranging from 0.05 to 0.5 mm and a diameter to wall thickness ratio ranging from 0.5 to 3 %. According to the method, starting materials are applied as a covering layer to supporting elements of any shape, and the green products produced in such a manner are subsequently heat-treated. During the heat-treatment, the supporting elements are pyrolyzed, the covering layers are, in essence, thermally decomposed, and the decomposition products are sintered. The outer dimensions of the supporting elements are selected such that they are larger than the shaped bodies to be produced. Metallic compounds, preferably metal oxides, metal hydroxides, metal carbonates, or organometallic compounds are selected as starting materials and can be reduced at a temperature of less than 1,200 DEG C. The heat treatment is carried out in a reductive atmosphere containing hydrogen and/or carbon in such a way that the starting materials are essentially reduced to the sintered metal which provides the foundation for the respectively used metal compound.
摘要:
The invention concerns a process permitting the preparation of a new powder, which as such or further processed is useful within a wide variety of different fields and which has magnetic and electric properties. The powder includes at least 0.5 % by weight of iron containing silicate and at least 10 % by weight of metallic iron and/or alloyed iron and is prepared by a process comprising the steps of mixing an iron containing powder and a silicon containing powder; and reducing the obtained mixture at a temperature above about 450 DEG C.
摘要:
The invention relates to a method for the production of power mixtures, or composite powders, from at least one first type of powder chosen from the group, high-melting metals, physically resistant materials, or ceramic powders and at least one second type of powder, chosen from the group of binding metals, binding metal mixed crystals and binding metal alloys. The second type of powder is produced, in an aqueous suspension of the first type of powder, from precursor compounds, which are in the form of water-soluble salts, by precipitation as the oxalate, separating the mother liquor and reduction to the metal.
摘要:
A method for producing a hydrogen storage alloy powder, characterized as comprising charging powders of raw materials and a plurality of balls into a pot of a ball mill, converting the atmosphere in the pot to a hydrogen atmosphere, and then subjecting the raw material powders to a mechanical alloying in the hydrogen atmosphere.
摘要:
A method for producing a porous metal powder comprising subjecting a starting metal to an oxidation treatment and then to a reduction treatment, characterized in that the starting metal is oxidized in the presence of chlorine and/or a chloride. Massive metal bodies formed after reduction comprise pillar-shaped particles being entangled in one another as are rootstocks, and thus, the metal powder has open pores.
摘要:
The invention relates to a method for producing wolfram carbides by gas-phase carburetion of wolfram powders and/or suitable wolfram precursor compounds in powder form at temperatures above 850 DEG C. According to the method a CO2/CO mixture with a CO2 content greater than the Boudouard equilibrium content corresponding to the carburetion temperature is used as carburetion gas phase.
摘要:
Methods for the manufacture of fine metal powders from metal-containing ammonium compounds such as ammonium oxalate metal salts. The method includes decomposing particulates of the ammonium oxalate metal salt by heating to a decomposition temperature in the presence of a dilute hydrogen gas to decompose the ammonium oxalate compound, and form a fine metal powder by heating to a higher refining temperature to remove contaminants from the fine metal powder. The method may include the conversion of a non-oxalate metal compound to a hydrated metal oxalate and the dehydration of the hydrated metal oxalate before decomposition to the metal. The method is applicable to the production of a wide variety of metals of high purity and fine particle size.
摘要:
The present disclosure generally relates to the field of fortification of food with iron. More particularly, the present disclosure relates to an irregular and porous elemental iron powder, which is suitable for fortifying food and pharmaceuticals with iron, and a composition comprising the same. The present disclosure also relates to a simple, economic, and efficient method for producing the said iron powder. The present disclosure further relates to an iron-fortified beverage or food product fortified with the elemental iron powder and a method of preparing the same. The elemental iron powder has metallic iron content of at least about 98% and surface area ranging from about 0.5 m2/g to about 1.0 m2/g. The elemental iron powder has high dissolution rate and relative bioavailability compared to the standard of care.