公开(公告)号：WO2010138440A1

公开(公告)日：2010-12-02

申请号：PCT/US2010/035924

申请日：2010-05-24

Applicant: 3M INNOVATIVE PROPERTIES COMPANY ,  NELSON, James M., ,  ARCHIBALD, Matthew N., ,  THOMPSON, Wendy L., ,  MILLER, Jeremy A., ,  LARSON, Randy A., ,  SPAWN, Terrance D.,

Inventor： NELSON, James M., ,  ARCHIBALD, Matthew N., ,  THOMPSON, Wendy L., ,  MILLER, Jeremy A., ,  LARSON, Randy A., ,  SPAWN, Terrance D.,

IPC: B01J19/18 ,  B01D1/22 ,  C08J3/215

CPC classification number: B01J19/1887 ,  B01D1/222 ,  B01J19/1862 ,  B01J19/2415 ,  B01J2219/0004 ,  B01J2219/00094 ,  B01J2219/00765 ,  C08J3/2053 ,  C08J3/215

Abstract: A method of making a filled resin includes the steps of: Providing a wiped film evaporator with an internal evaporator chamber maintained under vacuum and having an internal chamber wall maintained at an elevated temperature; introducing solvent-borne particles and organic matrix into the internal chamber; and compounding the solvent-borne particles and the organic matrix in the internal evaporator chamber by forming a thin film against the internal chamber wall, the thin film including organic matrix and particles, and the vacuum conditions and elevated temperature being sufficient to remove solvent from the particles and organic matrix to provide the filled resin. Less than about 10% of the particles in the resulting filled resin are agglomerated.

Abstract translation: 制备填充树脂的方法包括以下步骤：提供具有保持在真空下并具有保持在升高的温度下的内部室壁的内部蒸发器室的擦拭膜蒸发器; 将溶剂型颗粒和有机基质引入内室; 并通过在内部室壁上形成薄膜，将溶剂型颗粒和有机基质混合在内部蒸发器室中，该薄膜包括有机基质和颗粒，并且真空条件和升高的温度足以从 颗粒和有机基质提供填充树脂。 所得填充树脂中少于约10％的颗粒团聚。

公开(公告)号：WO2014062450A3

公开(公告)日：2014-06-26

申请号：PCT/US2013064109

申请日：2013-10-09

Applicant: 3M INNOVATIVE PROPERTIES CO ,  MARTIN STEVEN J ,  DRESSEL LUKE T ,  HUTT AARON E ,  SCHOTZ ERIC A ,  SPAWN TERENCE D ,  GUERRA MIGUEL A ,  FUKUSHI TATSUO ,  MILLER JEREMY A ,  GEISE CHRISTOPHER M ,  MCDONELL JAMES A

Inventor： MARTIN STEVEN J ,  DRESSEL LUKE T ,  HUTT AARON E ,  SCHOTZ ERIC A ,  SPAWN TERENCE D ,  GUERRA MIGUEL A ,  FUKUSHI TATSUO ,  MILLER JEREMY A ,  GEISE CHRISTOPHER M ,  MCDONELL JAMES A

IPC: C07C17/26 ,  C07C17/00 ,  C07C19/16

CPC classification number: C07C45/58 ,  C07C17/00 ,  C07C17/093 ,  C07C17/26 ,  C07C19/16

Abstract: A method of making α,ω-diiodoperfluoroalkanes includes combining: diatomic iodine, at least one perfluoroalkylene oxide represented by the formula wherein Rf represents a perfluoroalkyl group; and at least one of: a) a first metallic compound comprising nickel, and a second metallic compound comprising molybdenum that is compositionally different from the first metallic compound; or b) a metallic alloy comprising from 50 to 70 percent by weight of nickel and from 20 to 40 percent by weight of molybdenum, based on the total weight of the metallic alloy, thereby producing at least one product represented by the formula I(CF2)nI, wherein n independently represents an integer in the range of from 1 to 11. The total weight of the at least one product wherein n is 3 or greater exceeds the total weight of the at least one product wherein n is 1 or 2 by a factor of at least 4.

Abstract translation: 一种制造α，ω-二碘全氟烷烃的方法包括将二元碘，至少一种由下式表示的全氟环氧烷组合：其中Rf表示全氟烷基; 以及至少一种：a）包含镍的第一金属化合物和包含钼的第二金属化合物，所述钼与所述第一金属化合物在组成上不同; 或b）基于所述金属合金的总重量包含50至70重量％的镍和20至40重量％的钼的金属合金，由此产生至少一种由式I表示的产物（CF 2 ）nI，其中n独立地表示1至11的整数。其中n为3或更大的至少一种产物的总重量超过其中n为1或2的至少一种产物的总重量 至少是4的因素。

公开(公告)号：WO2014062450A2

公开(公告)日：2014-04-24

申请号：PCT/US2013/064109

申请日：2013-10-09

Applicant: 3M INNOVATIVE PROPERTIES COMPANY ,  MARTIN, Steven J. ,  DRESSEL, Luke T. ,  HUTT, Aaron E. ,  SCHOTZ, Eric A. ,  SPAWN, Terence D. ,  GUERRA, Miguel A. ,  FUKUSHI, Tatsuo ,  MILLER, Jeremy A. ,  GEISE, Christopher M. ,  MCDONELL, James A.

Inventor： MARTIN, Steven J. ,  DRESSEL, Luke T. ,  HUTT, Aaron E. ,  SCHOTZ, Eric A. ,  SPAWN, Terence D. ,  GUERRA, Miguel A. ,  FUKUSHI, Tatsuo ,  MILLER, Jeremy A. ,  GEISE, Christopher M. ,  MCDONELL, James A.

IPC: C07C17/00

CPC classification number: C07C45/58 ,  C07C17/00 ,  C07C17/093 ,  C07C17/26 ,  C07C19/16

Abstract: A method of making α,ω-diiodoperfluoroalkanes includes combining: diatomic iodine, at least one perfluoroalkylene oxide represented by the formula wherein R f represents a perfluoroalkyl group; and at least one of: a) a first metallic compound comprising nickel, and a second metallic compound comprising molybdenum that is compositionally different from the first metallic compound; or b) a metallic alloy comprising from 50 to 70 percent by weight of nickel and from 20 to 40 percent by weight of molybdenum, based on the total weight of the metallic alloy, thereby producing at least one product represented by the formula I(CF 2 ) n I, wherein n independently represents an integer in the range of from 1 to 11. The total weight of the at least one product wherein n is 3 or greater exceeds the total weight of the at least one product wherein n is 1 or 2 by a factor of at least 4.

Abstract translation: 制备α，ω-二碘全氟烷烃的方法包括组合：双原子碘，至少一种由下式表示的全氟代氧化烯其中Rf表示全氟烷基; 和至少一种：a）包含镍的第一金属化合物和包含与第一金属化合物成分不同的钼的第二金属化合物; 或b）金属合金，其包含基于金属合金的总重量的50-70重量％的镍和20至40重量％的钼，由此产生至少一种由式I表示的产物（CF 2 ）nI，其中n独立地表示1至11范围内的整数。其中n为3或更大的至少一种产物的总重量超过至少一种产物的总重量，其中n为1或2，其中n为1或2， 至少4的因素。