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    POLYMERIC DYES
    2.
    发明申请
    POLYMERIC DYES 审中-公开
    聚合染料

    公开(公告)号：WO2008138726A2

    公开(公告)日：2008-11-20

    申请号：PCT/EP2008/055038

    申请日：2008-04-25

    Applicant: CIBA HOLDING INC. ,  CREMER, Christian ,  RIGGS, Richard Lewis ,  FRÖHLING, Beate ,  MÜLLER, Martin

    Inventor： CREMER, Christian ,  RIGGS, Richard Lewis ,  FRÖHLING, Beate ,  MÜLLER, Martin

    IPC: C08G77/22 ,  C09B69/10

    CPC classification number: C08G77/26 ,  A61K8/11 ,  A61K8/26 ,  A61K8/898 ,  A61K2800/413 ,  A61K2800/43 ,  A61K2800/434 ,  A61Q5/065 ,  B82Y5/00 ,  C07F7/1836 ,  C08G77/22 ,  C08L83/08 ,  C09B69/008 ,  C09B69/101 ,  C09B69/103 ,  C09B69/106 ,  C09B69/107 ,  C09B69/109 ,  D06P1/0052 ,  D06P3/145 ,  Y10T428/29

    Abstract: A highly crosslinked polysiloxane dye comprising at least 10 Si atoms, including at least one moiety of the formula (I) whose open Si-bonds each are linked to an oxygen atom and open O-bond is linked to a silicon atom in the rest of the polysiloxane, and wherein T is a direct bond or an organic spacer group such as C 1 -C 18 alkylene, C 2 -C 12 alkenylene, C 5 -C 10 cycloalkylene, C 5 -C 10 arylene, -C 5 -C 10 arylene-(C 1 -C 10 alkylene)-, each of which may be end-capped towards the linkage to Dye by CO, COO, NR 1 , CONR 1 , NR 1 CONR 1 , CS, CSS, CSNR 1 , NR 1 CSNR 1 , O, S, SO, SO 2 , C 5 -C 10 cycloalkylene, C 5 -C 10 arylene; or T is C 3 -C 18 alkylene interrupted, and optionally end- capped towards the linkage to Dye, by CO, COO, NR 1 , CONR 1 , NR 1 CONR 1 , CS, CSS, CSNR 1 , NR 1 CSNR 1 , O, S, SO, -SO 2 -, C 5 -C 10 cycloalkylene, C 5 -C 10 arylene; or is CO; (CH 2 CH 2 -O) 1-5 ; COO; N(R 1 ); CON(R 1 ); O; S; SO; SO 2 ; R 1 is hydrogen; unsubstituted or substituted, straight-chain or branched, monocyclic or polycyclic, interrupted or uninterrupted C 1 -C 14 alkyl; C 2 -C 14 alkenyl; C 6 -C 10 aryl; C 6 -C 10 aryl-C 1 - C 10 alkyl; or C 5 -C 10 alkyl(C 5 -C 10 aryl); and Dye is a residue of an organic dye, is useful for dyeing of organic materials, such as keratin-containing fibers, wool, leather, silk, cellulose or polyamides.

    Abstract translation: 包含至少10个Si原子的高度交联的聚硅氧烷染料，包括至少一个式（I）的部分，其开放的Si键各自连接到氧原子和开放的O形键，其余部分与硅原子连接 聚硅氧烷，其中T是直接键或有机间隔基团，例如C 1 -C 18亚烷基，C 2 -C 3烷基， 亚烷基亚烷基，C 5 -C 10亚环烷基，C 5 -C 10亚芳基 ，-C 5 -C 10亚芳基 - （C 1 -C 10亚烷基） - ，其各自为 可以通过CO，COO，NR 1，CONR 1，NR 1和CON 1连接到染料上， / SUP>，CS，CSS，CSNR ，NR 1，CSNR 1，O，S，SO，SO 2， C 1 -C 5亚烷基，C 5 -C 10亚芳基，C 5 -C 10亚环烷基，C 5 -C 10亚芳基， 或T是C 3 -C 18亚烷基中断，并且任选地通过CO，COO，NR 1至H 2连接到Dye的连接上。 ，CONR 1，NR 1，...，CS，CSS，CSNR 1，NR 1， O，S，SO，-SO 2 - ，C 5 -C 10 - ， - C 1 -C 6烷基， 亚环烷基，C 5 -C 10亚芳基; 或是CO; （CH 2 CH 2 -O） 1-5 ; COO; N（R 1 ）; CON（R 1 ）; O; S; 所以; SO 2 ; R 1是氢; 未取代或取代的直链或支链单环或多环，间断或不间断的C 1 -C 14烷基; ç 2 -C 14 烯基; ç 6 -C 10 芳基; C 6 -C 10芳基-C 1 -C 10烷基; C 1 -C 6烷基; 或C 5 -C 10烷基（C 5 -C 10芳基）; 染料是有机染料的残留物，可用于染色有机材料，如含角蛋白的纤维，羊毛，皮革，丝绸，纤维素或聚酰胺。

    PROCESS FOR THE PREPARATION OF FUROPYRROLES
    3.
    发明申请
    PROCESS FOR THE PREPARATION OF FUROPYRROLES 审中-公开
    制备氟化物的方法

    公开(公告)号：WO2005005430A3

    公开(公告)日：2005-06-16

    申请号：PCT/EP2004051259

    申请日：2004-06-28

    Applicant: CIBA SC HOLDING AG ,  RIGGS RICHARD LEWIS ,  WESTWOOD NICHOLAS JAMES ,  SMITH DAVID MACDONALD ,  MORTON COLIN

    Inventor： RIGGS RICHARD LEWIS ,  WESTWOOD NICHOLAS JAMES ,  SMITH DAVID MACDONALD ,  MORTON COLIN

    IPC: C07D487/04 ,  C07D491/04 ,  C07D491/048

    CPC classification number: C07D487/04 ,  C07D491/04

    Abstract: The present invention relates to a process for the preparation of furopyrroles of the general formula (I), comprising (a) heating a compound of the formula (II) under microwave irradiation optionally in the presence of an inert solvent, wherein A and A are Cl-C18alkyl, C2-Cl8alkenyl, C2-Cl8alkynyl, C5-C8cycloalkyl, C5- C8cycloalkenyl, aryl or heteroaryl, A is hydrogen, C1-C18alkyl, cyanomethyl, Ar ,-CR R -(CH2 )m -Ar or Y- R , wherein R and R independently of each other stand for hydrogen or C1-C4alkyl, or phenyl which can be substituted up to three times with C1-C4alkyl, Ar stands for aryl, C5-C8 cloalkyl, C5-C8 cycloalkenyl or heteroaryl, which can be substituted one to three times with C1-C8alkyl, C1-C8alkoxy, halogen or phenyl, which can be substituted with C1-C8alkyI or C1-C8alkoxy one to three times, and m stands for 0, 1, 2, 3 or 4, R is C1-C18alkyl, in particular C1-C4alkyl, aryl, in particular phenyl, or aralkyl, in particular benzyl, which can be substituted one to three times with C1-C8alkyl, C1-C8alkoxy, or halogen, Y is -C(O)-, -C(O)O-, -C(O)NH-, -SO2NH- or -SO2- and R is C1-Cl8alkyl, Ar , or aralkyl. The furopyrroles of the general formula (I) can be obtained in high yield and high purity by the process of the present invention.

    Abstract translation: 本发明涉及一种制备通式（I）的呋喃并吡咯的方法，其包括（a）在微波辐射下任选地在惰性溶剂存在下加热式（II）化合物，其中A 1， 和A 2是C 1 -C 18烷基，C 2 -C 18烯基，C 2 -C 18炔基，C 5 -C 8环烷基，C 5 -C 8环烯基，芳基或杂芳基，A 3是氢，C 1 -C 18烷基，氰甲基，Ar 3， R 31 - （CH 2）m -Ar 3或Y-R 32，其中R 30和R 31彼此独立地代表氢或C 1 -C 4烷基 或可以被C 1 -C 4烷基取代三次的苯基，Ar 3代表芳基，C 5 -C 8烷基，C 5 -C 8环烯基或杂芳基，其可以被C 1 -C 8烷基，C 1 -C 8烷基取代一至三次 C 1-8烷氧基，卤素或苯基，其可以被C 1 -C 8烷基或C 1 -C 8烷氧基取代一至三次，m代表0,1,2,3或4，R是C 1 -C 18烷基，特别是C 1 -C 4烷基， 芳基，特别是苯基或芳烷基，特别是苄基， 可以用C 1 -C 8烷基，C 1 -C 8烷氧基或卤素取代一至三次，Y是-C（O） - ， - C（O）O-，-C（O）NH-，-SO 2 NH-或 - SO 2 - 和R 32是C 1 -C 8烷基，Ar 3或芳烷基。 通过本发明的方法可以高产率和高纯度获得通式（I）的呋喃并吡咯。

    PROCESS FOR THE PREPARATION OF FUROPYRROLES
    4.
    发明申请
    PROCESS FOR THE PREPARATION OF FUROPYRROLES 审中-公开
    制备呋喃甲醇的方法

    公开(公告)号：WO2005005430A2

    公开(公告)日：2005-01-20

    申请号：PCT/EP2004/051259

    申请日：2004-06-28

    Applicant: CIBA SPECIALTY CHEMICALS HOLDING INC. ,  RIGGS, Richard Lewis ,  WESTWOOD, Nicholas James ,  SMITH, David Macdonald ,  MORTON, Colin

    Inventor： RIGGS, Richard Lewis ,  WESTWOOD, Nicholas James ,  SMITH, David Macdonald ,  MORTON, Colin

    IPC: C07D491/00

    CPC classification number: C07D487/04 ,  C07D491/04

    Abstract: The present invention relates to a process for the preparation of furopyrroles of the general formula (I), comprising (a) heating a compound of the formula (II) under microwave irradiation optionally in the presence of an inert solvent, wherein A 1 and A 2 are C l -C 18 alkyl, C 2 -C l8 alkenyl, C 2 -C l8 alkynyl, C 5 -C 8 cycloalkyl, C 5- C 8 cycloalkenyl, aryl or heteroaryl, A 3 is hydrogen, C 1 -C 18 alkyl, cyanomethyl, Ar 3 ,-CR 30 R 31 -(CH 2 ) m -Ar 3 or Y- R 32 , wherein R 30 and R 31 independently of each other stand for hydrogen or C 1 -C 4 alkyl, or phenyl which can be substituted up to three times with C 1 -C 4 alkyl, Ar 3 stands for aryl, C 5 -C 8 cloalkyl, C 5 -C 8 cycloalkenyl or heteroaryl, which can be substituted one to three times with C 1 -C 8 alkyl, C 1 -C 8 alkoxy, halogen or phenyl, which can be substituted with C 1 -C 8 alkyI or C 1 -C 8 alkoxy one to three times, and m stands for 0, 1, 2, 3 or 4, R is C 1 -C 18 alkyl, in particular C 1 -C 4 alkyl, aryl, in particular phenyl, or aralkyl, in particular benzyl, which can be substituted one to three times with C 1 -C 8 alkyl, C 1 -C 8 alkoxy, or halogen, Y is -C(O)-, -C(O)O-, -C(O)NH-, -SO 2 NH- or -SO 2 - and R 32 is C 1 -C l8 alkyl, Ar 3 , or aralkyl. The furopyrroles of the general formula (I) can be obtained in high yield and high purity by the process of the present invention.

    Abstract translation: 本发明涉及制备通式（I）呋喃并呋喃的方法，其包括（a）在微波辐射下任选地在存在下式（II）的情况下加热式 惰性溶剂，其中A 1和A 2是C 1 -C 18烷基，C≡2 -C≡C8烯基，C≡C12炔基，C≡C-sub C8-C8环烯基，芳基或杂芳基，A 3是氢，C 1 -C 8环烷基，C 5 -C 8环烯基，芳基或杂芳基，A 3是氢，C≡1 C18烷基，氰甲基，Ar 3，-CR 30 R 31 - （CH 3） - ， - CH 2），或者Y-R <32>，或者Y-R <32> 其中R 30和R 31彼此独立地代表氢或C 1 -C 4 - / - ，其中R 30和R 31彼此独立地代表氢或C 1 -C 4 - 烷基或可被C 1 -C 4烷基取代至多三次的苯基，Ar 3代表芳基，C 1 -C 4烷基， 低于5-C 8 cloa C 1 -C 8 - 环烯基或杂芳基，其可以被C 1 -C 8取代1-3次， C 1-8烷基，C 1 -C 8烷氧基，卤素或可被C 1 -C 8取代的苯基 烷基或C 1 -C 8烷氧基取代1-3次，m代表0,1,2,3或4，R是C

    APPARATUS FOR THERMOSETTING THERMOPLASTIC TUBES
    5.
    发明申请
    APPARATUS FOR THERMOSETTING THERMOPLASTIC TUBES 审中-公开
    热变形管热电偶装置

    公开(公告)号：WO2003028981A1

    公开(公告)日：2003-04-10

    申请号：PCT/US2002/030107

    申请日：2002-09-23

    Applicant: PILOT INDUSTRIES, INC. ,  RIGGS, Richard, H. ,  GABBEY, David, John ,  MARION, Patrick, L.

    Inventor： RIGGS, Richard, H. ,  GABBEY, David, John ,  MARION, Patrick, L.

    IPC: B29C53/08

    CPC classification number: B29C33/56 ,  B29C35/00 ,  B29C53/083 ,  B29C53/84 ,  B29K2101/12

    Abstract: An apparatus is disclosed for thermosetting thermoplastic tubes (20) in a predefined shape having at least one bend. The apparatus includes an oven (10) with an interior chamber (12) which is heated to a temperature approaching that at which the tube thermally deforms. An elongated former (22) has a channel (23) dimensioned to receive the tube, and this channel has the predefined shape. A thermally absorbent coating (30) is disposed only on a surface of the former adjacent to and extending across each bend (24) of the former. This thermally absorbent coating locally adds the thermal energy required to reset the memory of the tube at the bend location. A conveyor (21) extends through the oven chamber from an inlet end and to an outlet end of the oven, and the former is attached to the conveyor.

    Abstract translation: 公开了一种具有至少一个弯曲部的预定形状的热固性热塑性管（20）的装置。 该设备包括具有内部室（12）的烘箱（10），其被加热到接近管子热变形的温度。 细长的成形器（22）具有用于容纳管的尺寸的通道（23），并且该通道具有预定的形状。 吸热性涂层（30）仅在前者的表面上设置，邻近并延伸穿过前者的每个弯曲部（24）。 这种吸热涂层局部地增加了在弯曲位置复位管的存储器所需的热能。 输送机（21）从烘箱的入口端和出口端延伸穿过烘箱室，并且前者连接到输送机。

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