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    PROCESS FOR PRODUCING N-METHYL SUCCINIMIDE
    2.
    发明申请
    PROCESS FOR PRODUCING N-METHYL SUCCINIMIDE 审中-公开
    生产N-甲基磺酰胺的方法

    公开(公告)号：WO2004058708A1

    公开(公告)日：2004-07-15

    申请号：PCT/US2003/040106

    申请日：2003-12-16

    Applicant: BATTELLE MEMORIAL INSTITUTE ,  WERPY, Todd, A. ,  FRYE, John, G., Jr. ,  WHITE, James, F. ,  HOLLADAY, Johnathan, E. ,  ZACHER, Alan, H.

    Inventor： WERPY, Todd, A. ,  FRYE, John, G., Jr. ,  WHITE, James, F. ,  HOLLADAY, Johnathan, E. ,  ZACHER, Alan, H.

    IPC: C07D207/40

    CPC classification number: C07D207/404 ,  C07D207/267

    Abstract: The invention includes methods of processing an initial di-carbonyl compound by conversion to a cyclic compound. The cyclic compound is reacted with an alkyating agent to form a derivative having an alkylated ring nitrogen. The invention encompasses a method of producing an N-alkyl product. Amonia content of a solution is adjusted to produce a ratio of ammonia to di-carboxylate compound of from about 1:1 to about 1.5:1. An alkylating agent is added and the initial compound is alkylated and cyclized. The invention includes methods of making N-methyl pyrrolidinone (NMP). Aqueous ammonia and succinate is introduced into a vessel and ammonia is adjusted to provide a ratio of ammonia to succinate of less than 2:1. A methylating agent is reacted with succinate at a temperature of from greater than 100 °C to about 400 °C to produce N-methyl succinimide which is purified and hydrogenated to form NMP.

    Abstract translation: 本发明包括通过转化为环状化合物来处理初始二羰基化合物的方法。 环状化合物与烷基化剂反应形成具有烷基化环氮的衍生物。 本发明包括生产N-烷基产物的方法。 调节溶液的阿莫尼亚含量以产生约1：1至约1.5：1的氨与二羧酸酯化合物的比例。 加入烷基化剂并将该初始化合物烷基化并环化。 本发明包括制备N-甲基吡咯烷酮（NMP）的方法。 将氨水和琥珀酸钠引入容器中，并调节氨以提供小于2:1的氨与琥珀酸的比例。 甲基化剂与琥珀酸盐在大于100℃至约400℃的温度下反应，生成N-甲基琥珀酰亚胺，将其纯化并氢化形成NMP。

    METHOD OF FORMING A DIANHYDROSUGAR ALCOHOL
    5.
    发明申请
    METHOD OF FORMING A DIANHYDROSUGAR ALCOHOL 审中-公开
    形成二醛醇的方法

    公开(公告)号：WO2007089527B1

    公开(公告)日：2008-03-06

    申请号：PCT/US2007001996

    申请日：2007-01-25

    Applicant: BATTELLE MEMORIAL INSTITUTE ,  HOLLADAY JOHNATHAN ,  WERPY TODD A ,  HU JIANLI ,  WANG YONG ,  ZHANG XINJIE

    Inventor： HOLLADAY JOHNATHAN ,  WERPY TODD A ,  HU JIANLI ,  WANG YONG ,  ZHANG XINJIE

    IPC: C07D493/04

    CPC classification number: C07D307/20 ,  C07D493/04 ,  Y02P20/127

    Abstract: The invention includes methods of producing dianhydrosugars. A polyol is reacted in the presence of a first catalyst to form a monocyclic sugar. The monocyclic sugar is transferred to a second reactor where it is converted to a dianhydrosugar alcohol in the presence of a second catalyst. The invention includes a process of forming isosorbide. An initial reaction is conducted at a first temperature in the presence of a solid acid catalyst. The initial reaction involves reacting sorbitol to produce 1,4-sorbitan, 3,6-sorbitan, 2,5-mannitan and 2,5-iditan. Utilizing a second temperature, the 1,4-sorbitan and 3,6-sorbitan are converted to isosorbide. The invention includes a method of purifying isosorbide from a mixture containing isosorbide and at least one additional component. A first distillation removes a first portion of the isosorbide from the mixture. A second distillation is then conducted at a higher temperature to remove a second portion of isosorbide from the mixture.

    Abstract translation: 本发明包括生产二脱水糖的方法。 多元醇在第一催化剂存在下反应形成单环糖。 将单环糖转移到第二反应器中，在第二反应器中在第二催化剂的存在下将其转化成二水糖醇。 本发明包括形成异山梨醇的方法。 初始反应在固体酸催化剂存在下的第一温度下进行。 最初的反应包括使山梨糖醇反应生成1,4-脱水山梨糖醇，3,6-脱水山梨糖醇，2,5-甘露糖醇和2,5-戊二酸。 利用第二温度，1,4-脱水山梨糖醇和3,6-脱水山梨糖醇转化为异山梨醇。 本发明包括从含有异山梨醇和至少一种附加组分的混合物中纯化异山梨醇的方法。 第一次蒸馏从混合物中除去第一部分异山梨醇。 然后在较高温度下进行第二次蒸馏以从混合物中除去第二部分异山梨醇。

    METHOD OF FORMING A DIANHYDROSUGAR ALCOHOL
    6.
    发明申请
    METHOD OF FORMING A DIANHYDROSUGAR ALCOHOL 审中-公开
    形成二氢化AR醇的方法

    公开(公告)号：WO2007089527A2

    公开(公告)日：2007-08-09

    申请号：PCT/US2007/001996

    申请日：2007-01-25

    Applicant: BATTELLE MEMORIAL INSTITUTE ,  HOLLADAY, Johnathan ,  WERPY, Todd, A. ,  HU, Jianli ,  WANG, Yong ,  ZHANG, Xinjie

    Inventor： HOLLADAY, Johnathan ,  WERPY, Todd, A. ,  HU, Jianli ,  WANG, Yong ,  ZHANG, Xinjie

    IPC: C07D493/04

    CPC classification number: C07D307/20 ,  C07D493/04 ,  Y02P20/127

    Abstract: The invention includes methods of producing dianhydrosugars. A polyol is reacted in the presence of a first catalyst to form a monocyclic sugar. The monocyclic sugar is transferred to a second reactor where it is converted to a dianhydrosugar alcohol in the presence of a second catalyst. The invention includes a process of forming isosorbide. An initial reaction is conducted at a first temperature in the presence of a solid acid catalyst. The initial reaction involves reacting sorbitol to produce 1 ,4-sorbitan, 3,6-sorbitan, 2,5-mannitan and 2,5-iditan. Utilizing a second temperature, the 1 ,4-sorbitan and 3,6-sorbitan are converted to isosorbide. The invention includes a method of purifying isosorbide from a mixture containing isosorbide and at least one additional component. A first distillation removes a first portion of the isosorbide from the mixture. A second distillation is then conducted at a higher temperature to remove a second portion of isosorbide from the mixture.

    Abstract translation: 本发明包括生产二脱水甘油糖的方法。 多元醇在第一催化剂存在下反应形成单环糖。 将单环糖转移到第二反应器中，在第二反应器中，在第二催化剂的存在下将其转化为二脱水甘油醇。 本发明包括形成异山梨醇的方法。 在固体酸催化剂存在下，在第一温度下进行初始反应。 初始反应包括使山梨糖醇反应生成1,4-脱水山梨糖醇，3,6-脱水山梨糖醇，2,5-甘露聚糖和2,5-己烷。 使用第二温度，将1,4-脱水山梨醇和3,6-脱水山梨醇转化为异山梨醇。 本发明包括从含有异山梨醇和至少一种另外的组分的混合物中纯化异山梨醇的方法。 第一蒸馏从混合物中除去第一部分的异山梨醇。 然后在较高温度下进行第二次蒸馏以从混合物中除去第二部分的异山梨醇。

    DEICING/ANTI-ICING FLUIDS
    7.
    发明申请
    DEICING/ANTI-ICING FLUIDS 审中-公开
    检测/防止流体

    公开(公告)号：WO2005105945A3

    公开(公告)日：2005-12-15

    申请号：PCT/US2005014520

    申请日：2005-04-28

    Applicant: BATTELLE MEMORIAL INSTITUTE ,  SAMUELS WILLIAM D ,  CONKLE NICHOLAS H ,  MONZYK BRUCE F ,  SIMMONS KEVIN L ,  FRYE JOHN G ,  WERPY TODD A ,  KUCZEK SARA F ,  CHAUHAN SATYA P

    Inventor： SAMUELS WILLIAM D ,  CONKLE NICHOLAS H ,  MONZYK BRUCE F ,  SIMMONS KEVIN L ,  FRYE JOHN G ,  WERPY TODD A ,  KUCZEK SARA F ,  CHAUHAN SATYA P

    IPC: C09K3/18

    CPC classification number: C09K3/18 ,  C09K3/185

    Abstract: A nontoxic deicing/anti-icing fluid includes a freezing point depressant selected from short chain polyols having 3 to 5 carbons atoms, and mixtures thereof, a wetting agent, an antioxidant/preservative, and water. The fluid has an LD50 greater than about 10,000 mg/L. Another deicing/anti-icing fluid includes the freezing point depressant, a vinylpyrrolidone polymer having a molecular weight between about 10,000 and about 700,000, and water. A runway deicing fluid includes glycerol, a buffer, an antioxidant/preservative, and water. Another deicing/anti-icing fluid includes a freezing point depressant having hydrophobic character, a wetting agent comprising an organophosphorus compound capable of producing an organic wettable surface, and water.

    Abstract translation: 无毒除冰/防冰液体包括选自具有3至5个碳原子的短链多元醇及其混合物，润湿剂，抗氧化剂/防腐剂和水的凝固点抑制剂。 流体的LD50大于约10,000 mg / L。 另一种除冰/防冰液体包括冰点抑制剂，分子量介于约10,000至约700,000之间的乙烯基吡咯烷酮聚合物和水。 跑道除冰液包括甘油，缓冲剂，抗氧化剂/防腐剂和水。 另一种除冰/防冰流体包括具有疏水性的凝固点抑制剂，包含能够产生有机可湿性表面的有机磷化合物的润湿剂和水。

    CHEMICAL PRODUCTION PROCESSES, SYSTEMS, AND CATALYST COMPOSITIONS
    8.
    发明申请
    CHEMICAL PRODUCTION PROCESSES, SYSTEMS, AND CATALYST COMPOSITIONS 审中-公开
    化学生产过程，体系和催化剂组合物

    公开(公告)号：WO2009029540A3

    公开(公告)日：2009-09-17

    申请号：PCT/US2008074090

    申请日：2008-08-22

    Applicant: BATTELLE MEMORIAL INSTITUTE ,  PETERSON THOMAS H ,  HOLLADAY JOHNATHAN E ,  ZACHER ALAN H ,  GRAY MICHEL J ,  WERPY TODD A ,  WHITE JAMES F

    Inventor： PETERSON THOMAS H ,  HOLLADAY JOHNATHAN E ,  ZACHER ALAN H ,  GRAY MICHEL J ,  WERPY TODD A ,  WHITE JAMES F

    IPC: C07C45/52 ,  B01J27/16 ,  C07C47/22

    CPC classification number: C07C45/52 ,  C07C49/17 ,  C07C47/22

    Abstract: Chemical production processes are provided that include exposing a reactant composition to a catalyst composition to form a product composition, with the reactant composition including a multihydric alcohol compound and the catalyst composition being effective to dehydrate at least a portion of the multihydric alcohol compound. Embodiments of the process provide that the reactant composition is exposed to the catalyst composition for less than about 0.25 seconds and/or that the catalyst is maintained at a temperature of from about 2800C to about 3200C. Processes utilizing a reactant composition including a multihydric alcohol compound and an inert compound are also provided.

    Abstract translation: 提供化学生产方法，其包括将反应物组合物暴露于催化剂组合物以形成产物组合物，其中反应物组合物包含多元醇化合物并且催化剂组合物有效使至少一部分多元醇化合物脱水。 该方法的实施方案规定反应物组合物暴露于催化剂组合物小于约0.25秒和/或催化剂保持在约280℃至约320℃的温度。 还提供了利用包含多元醇化合物和惰性化合物的反应物组合物的方法。

    METHOD OF FORMING A DIANHYDROSUGAR ALCOHOL
    9.
    发明申请
    METHOD OF FORMING A DIANHYDROSUGAR ALCOHOL 审中-公开
    形成二氢化AR醇的方法

    公开(公告)号：WO2007089527A3

    公开(公告)日：2008-01-17

    申请号：PCT/US2007001996

    申请日：2007-01-25

    Applicant: BATTELLE MEMORIAL INSTITUTE ,  HOLLADAY JOHNATHAN ,  WERPY TODD A ,  HU JIANLI ,  WANG YONG ,  ZHANG XINJIE

    Inventor： HOLLADAY JOHNATHAN ,  WERPY TODD A ,  HU JIANLI ,  WANG YONG ,  ZHANG XINJIE

    IPC: C07D493/04

    CPC classification number: C07D307/20 ,  C07D493/04 ,  Y02P20/127

    Abstract: The invention includes methods of producing dianhydrosugars. A polyol is reacted in the presence of a first catalyst to form a monocyclic sugar. The monocyclic sugar is transferred to a second reactor where it is converted to a dianhydrosugar alcohol in the presence of a second catalyst. The invention includes a process of forming isosorbide. An initial reaction is conducted at a first temperature in the presence of a solid acid catalyst. The initial reaction involves reacting sorbitol to produce 1,4-sorbitan, 3,6-sorbitan, 2,5-mannitan and 2,5-iditan. Utilizing a second temperature, the 1,4-sorbitan and 3,6-sorbitan are converted to isosorbide. The invention includes a method of purifying isosorbide from a mixture containing isosorbide and at least one additional component. A first distillation removes a first portion of the isosorbide from the mixture. A second distillation is then conducted at a higher temperature to remove a second portion of isosorbide from the mixture.

    Abstract translation: 本发明包括生产二脱水甘油糖的方法。 多元醇在第一催化剂存在下反应形成单环糖。 将单环糖转移到第二反应器中，在第二反应器中，在第二催化剂的存在下将其转化为二脱水甘油醇。 本发明包括形成异山梨醇的方法。 在固体酸催化剂存在下，在第一温度下进行初始反应。 初始反应包括使山梨醇反应生成1,4-脱水山梨糖醇，3,6-脱水山梨糖醇，2,5-甘露聚糖和2,5-己烷。 利用第二温度，将1,4-脱水山梨醇和3,6-脱水山梨醇转化为异山梨醇。 本发明包括从含有异山梨醇和至少一种另外的组分的混合物中纯化异山梨醇的方法。 第一蒸馏从混合物中除去第一部分的异山梨醇。 然后在较高温度下进行第二次蒸馏以从混合物中除去第二部分的异山梨醇。

    HYDROXYMETHYLFURFURAL REDUCTION METHODS AND METHODS OF PRODUCING FURANDIMETHANOL
    10.
    发明申请
    HYDROXYMETHYLFURFURAL REDUCTION METHODS AND METHODS OF PRODUCING FURANDIMETHANOL 审中-公开
    羟丙基纤维素还原方法及其制备方法

    公开(公告)号：WO2007146836A1

    公开(公告)日：2007-12-21

    申请号：PCT/US2007/070802

    申请日：2007-06-08

    Applicant: BATTELLE MEMORIAL INSTITUTE ,  LILGA, Michael, A. ,  HALLEN, Richard, T. ,  WERPY, Todd, A. ,  WHITE, James, F. ,  HOLLADAY, Johnathan, E. ,  FRYE, John, G. ,  ZACHER, Alan, H.

    Inventor： LILGA, Michael, A. ,  HALLEN, Richard, T. ,  WERPY, Todd, A. ,  WHITE, James, F. ,  HOLLADAY, Johnathan, E. ,  FRYE, John, G. ,  ZACHER, Alan, H.

    IPC: C07D307/12 ,  C07D307/40

    CPC classification number: C07D307/12 ,  C07D307/40

    Abstract: A method of reducing hydroxymethylfurfural (HMF) where a starting material containing HMF in a solvent comprising water is provided. H 2 is provided into the reactor and the starting material is contacted with a catalyst containing at least one metal selected from Ni, Co, Cu, Pd, Pt, Ru, Ir, Re and Rh, at a temperature of less than or equal to 250°C. A method of hydrogenating HMF includes providing an aqueous solution containing HMF and fructose. H 2 and a hydrogenation catalyst are provided. The HMF is selectively hydrogenated relative to the fructose at a temperature at or above 30°C. A method of producing tetrahydofuran dimethanol (THFDM) includes providing a continuous flow reactor having first and second catalysts and providing a feed comprising HMF into the reactor. The feed is contacted with the first catalyst to produce furan dimethanol (FDM) which is contacted with the second catalyst to produce THFDM.

    Abstract translation: 提供一种还原羟甲基糠醛（HMF）的方法，其中含有HMF的原料在包含水的溶剂中。 H 2被提供到反应器中，起始材料与含有选自Ni，Co，Cu，Pd，Pt，Ru，Ir，Re和Rh中的至少一种金属的催化剂接触， 温度小于或等于250℃。 氢化HMF的方法包括提供含有HMF和果糖的水溶液。 H 2 H 2和氢化催化剂。 在30℃或更高的温度下，HMF相对于果糖选择性氢化。 制备四氢呋喃二甲醇（THFDM）的方法包括提供具有第一和第二催化剂的连续流动反应器，并向反应器中提供包含HMF的进料。 进料与第一催化剂接触以产生与第二催化剂接触以产生THFDM的呋喃二甲醇（FDM）。

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