公开(公告)号：WO2002028822A3

公开(公告)日：2002-04-11

申请号：PCT/JP2001/008718

申请日：2001-10-03

Applicant: SHOWA DENKO K.K. ,  SASAKI, Toru ,  FURUKAWA, Tetsuhiro ,  SATO, Yoshinori ,  YAMAMOTO, Takuji ,  YONEYAMA, Takashi

Inventor： SASAKI, Toru ,  FURUKAWA, Tetsuhiro ,  SATO, Yoshinori ,  YAMAMOTO, Takuji ,  YONEYAMA, Takashi

IPC: C07C253/30

Abstract: Abstract An object of the invention is to provide a process for industrially producing fluorinated dicyanobenzenes using tetrachlorodicyanobenzene as a raw material. According to the present invention, fluorinated dicyanobenzene can be produced in a high yield by allowing tetrachlorodicyanobenzenes to react with a fluorinating agent in the presence of a non-protonic polar solvent in an amount of 0.1 to 3 times by mass based on the tetrachlorodicyanobenzene. Further, the above production can be conducted more efficiently by reacting while disintegrating or removing bulk solid matters.

公开(公告)号：WO1996004591A1

公开(公告)日：1996-02-15

申请号：PCT/US1995009798

申请日：1995-08-01

Applicant: E.I. DU PONT DE NEMOURS AND COMPANY ,  SHINOHARA, Kenichi ,  KASSAL, Robert, J. ,  SUZUKI, Osamu ,  YONEYAMA, Takashi

Inventor： E.I. DU PONT DE NEMOURS AND COMPANY

IPC: G03C03/00

CPC classification number: G03C3/00 ,  C08K5/13 ,  C08K5/34 ,  C08L59/00

Abstract: Resin compositions used to make parts for photographic sensitive materials, which are polyacetal resin compositions and are characterized by the concentration of formaldehyde generated from a formed object of the said composition in a closed environment being less than 20 ppm and by not compromizing with their photographic properties.

Abstract translation: 用于制备用于感光材料的部件的树脂组合物，其为聚缩醛树脂组合物，其特征在于在封闭环境中由所述组合物的形成物质产生的甲醛浓度小于20ppm，并且不影响其照相性能 。

公开(公告)号：WO0228822A2

公开(公告)日：2002-04-11

申请号：PCT/JP0108718

申请日：2001-10-03

Applicant: SHOWA DENKO KK ,  SASAKI TORU ,  FURUKAWA TETSUHIRO ,  SATO YOSHINORI ,  YAMAMOTO TAKUJI ,  YONEYAMA TAKASHI

Inventor： SASAKI TORU ,  FURUKAWA TETSUHIRO ,  SATO YOSHINORI ,  YAMAMOTO TAKUJI ,  YONEYAMA TAKASHI

IPC: C07C253/30 ,  C07C255/51

CPC classification number: C07C253/30 ,  C07C255/51

Abstract: Abstract An object of the invention is to provide a process for industrially producing fluorinated dicyanobenzenes using tetrachlorodicyanobenzene as a raw material. According to the present invention, fluorinated dicyanobenzene can be produced in a high yield by allowing tetrachlorodicyanobenzenes to react with a fluorinating agent in the presence of a non-protonic polar solvent in an amount of 0.1 to 3 times by mass based on the tetrachlorodicyanobenzene. Further, the above production can be conducted more efficiently by reacting while disintegrating or removing bulk solid matters.

Abstract translation: 发明内容本发明的目的是提供一种使用四氯二氰基苯作为原料工业生产氟化二氰基苯的方法。 根据本发明，通过使四氯二氰基苯在非质子极性溶剂的存在下，相对于四氯二氰基苯为0.1〜3质量％，与氟化剂反应，可以高收率地制备氟化二氰基苯。 此外，通过在分解或除去大量固体物质的同时进行反应，能够更有效地进行上述的制造。