公开(公告)号：WO2016027280A2

公开(公告)日：2016-02-25

申请号：PCT/IN2015000322

申请日：2015-08-14

申请人： COUNCIL SCIENT IND RES

发明人： ALAMARU VENKATA RAMI REDDY ,  NATARAJ SANNA KOTRAPPANAVAR ,  PRASAD KAMALESH ,  MONDAL DIBYENDU ,  POLISETTI VEERA BABU ,  BHATT JITKUMAR ,  MAHTO ASHESH

IPC分类号： C02F1/44

CPC分类号： C02F1/445 ,  B01D61/005 ,  B01D71/56 ,  C02F1/22 ,  C02F2101/101 ,  C02F2101/12 ,  C02F2101/308 ,  C02F2103/08 ,  C02F2103/14 ,  C02F2103/24 ,  C02F2303/16 ,  Y02A20/131 ,  Y02A20/132 ,  Y02W10/37

摘要： The present invention relates to a novel forward osmosis (FO) process for dewatering of a variety of feed solution using low water activity and high osmotic pressure deep eutectic solvent with and without dispersed magnetic nanoparticles as draw solution. In particular, choline chloride-ethylene glycol, choline chloride- glycerol, Fe304 dispersed in former and latter were utilized as draw solution in FO for one step desalination of brackish and seawater, water recovery from effluent of leather and dye industries, protein and DNA concentration at room temperature. Owing to very low freezing point, the diluted draw solution after FO was recovered through phase separation by chilling at Ca. -10 °C with concomitant production of usable water. Although the present invention focused on specific DES and dispersion of Fe3O4 as magnetic nanoparticles but use of other DES having high osmotic pressure and low freezing point and other magnetic nanoparticles dispersion are logical extension of present invention.

摘要翻译： 本发明涉及一种使用低水分活性的多种进料溶液脱水的新型正渗（FO）方法和具有和不具有分散磁性纳米颗粒作为拉伸溶液的高渗透压深共晶溶剂。 特别是，分离在前者和后者中的氯化胆碱 - 乙二醇，氯化胆碱 - 甘油，Fe304用作FO溶液，用于淡水和海水的一步脱盐，皮革和染料工业废水的回收，蛋白质和DNA浓度 在室温下。 由于非常低的凝固点，通过在Ca下冷却通过相分离回收FO后的稀释的溶液。 -10℃，伴随生产可用水。 尽管本发明集中于Fe 3 O 4作为磁性纳米颗粒的具体DES和分散体，但是使用具有高渗透压和低凝固点的其它DES以及其它磁性纳米颗粒分散体是本发明的逻辑延伸。

公开(公告)号：WO2010109289A8

公开(公告)日：2011-03-03

申请号：PCT/IB2010000588

申请日：2010-03-19

申请人： COUNCIL SCIENT IND RES ,  MEENA RAMAVATAR ,  PRASAD KAMALESH ,  SIDDHANTA ARUP KUMAR ,  GHOSH PUSHPITO KUMAR ,  MEHTA GAURAVKUMAR KISHOR ,  RAMAVAT BHARATKUMAR KALIDAS ,  GANESAN MEENAKSHI SUNDARAM ,  JHA BHAVANATH ,  MISHRA AVINASH ,  GANDHI MAHESH RAMNIKLAL ,  AGARWAL PRADEEP KUMAR ,  ESWARAN KARUPPANAN

发明人： MEENA RAMAVATAR ,  PRASAD KAMALESH ,  SIDDHANTA ARUP KUMAR ,  GHOSH PUSHPITO KUMAR ,  MEHTA GAURAVKUMAR KISHOR ,  RAMAVAT BHARATKUMAR KALIDAS ,  GANESAN MEENAKSHI SUNDARAM ,  JHA BHAVANATH ,  MISHRA AVINASH ,  GANDHI MAHESH RAMNIKLAL ,  AGARWAL PRADEEP KUMAR ,  ESWARAN KARUPPANAN

IPC分类号： C08B37/00

CPC分类号： C08B37/0003 ,  C08B37/0039

摘要： The present invention relates to a more convenient and energy efficient process for the preparation of agarose from Gracilaria and Gelidiella spp., more particularly Gracilaria dura and Gelidella acerosa from Indian waters, said process comprising steps of prc- treating the dry seaweed with alkali, rinsing the pre-treated seaweed until the washing shows a pH ranging between 7 and 9, adding water, autoclaving to obtain extractive, centrifuging hot seaweed extractive, then treating the clear hot extractive with surface active chemicals to induce precipitation of agarose, centrifuging the mass to remove the adhering liquid, rinsing the centrifuged mass with water to remove the surface active chemical, preparing a hot sol of the agarose mass in minimum quantity of water, re- precipitating the agarose with iso-propanol to achieve a product having dispersibility while preparing gel, and demonstrating that the said gel in DNA gel electrophoresis studies shows performance equal to that of gel obtained through more conventional process of agarose preparation from the same seaweed extractives as also to gel prepared from commercial benchmark.

摘要翻译： 本发明涉及一种更方便和节能的方法，用于制备来自印度水稻的江ia（Gracilaria）和Gel ella属（Gelidiella spp。），更特别是江particularly草（Acacilaria dura）和醋酸and螨（Gelidella acerosa）的琼脂糖，所述方法包括用碱处理干海藻 预处理的海藻直到洗涤显示pH范围在7至9之间，加水，高压灭菌以获得提取物，离心热海藻提取物，然后用表面活性化学品处理透明热萃取物以诱导琼脂糖沉淀，将质量离心 去除粘附液体，用水冲洗离心的物料以除去表面活性化学物质，在最少量的水中制备琼脂糖块的热溶胶，用异丙醇重新沉淀琼脂糖，得到具有分散性的产物，同时制备凝胶 并证明DNA凝胶电泳研究中的所述凝胶显示出与凝胶相似的性能 通过相同海藻提取物的更常规的琼脂糖制备方法获得，以及从商业标准制备的凝胶。

公开(公告)号：WO2016027280A4

公开(公告)日：2016-06-23

申请号：PCT/IN2015000322

申请日：2015-08-14

申请人： COUNCIL SCIENT IND RES

发明人： ALAMARU VENKATA RAMI REDDY ,  NATARAJ SANNA KOTRAPPANAVAR ,  PRASAD KAMALESH ,  MONDAL DIBYENDU ,  POLISETTI VEERA BABU ,  BHATT JITKUMAR ,  MAHTO ASHESH

IPC分类号： C02F1/44 ,  B01D61/00 ,  C02F1/22

CPC分类号： C02F1/445 ,  B01D61/005 ,  B01D71/56 ,  C02F1/22 ,  C02F2101/101 ,  C02F2101/12 ,  C02F2101/308 ,  C02F2103/08 ,  C02F2103/14 ,  C02F2103/24 ,  C02F2303/16 ,  Y02A20/131 ,  Y02A20/132 ,  Y02W10/37

摘要： The present invention relates to a novel forward osmosis (FO) process for dewatering of a variety of feed solution using low water activity and high osmotic pressure deep eutectic solvent with and without dispersed magnetic nanoparticles as draw solution. In particular, choline chloride-ethylene glycol, choline chloride- glycerol, Fe304 dispersed in former and latter were utilized as draw solution in FO for one step desalination of brackish and seawater, water recovery from effluent of leather and dye industries, protein and DNA concentration at room temperature. Owing to very low freezing point, the diluted draw solution after FO was recovered through phase separation by chilling at Ca. -10 °C with concomitant production of usable water. Although the present invention focused on specific DES and dispersion of Fe3O4 as magnetic nanoparticles but use of other DES having high osmotic pressure and low freezing point and other magnetic nanoparticles dispersion are logical extension of present invention.

摘要翻译： 本发明涉及一种使用低水分活性的各种进料溶液脱水的新型正渗（FO）方法和具有和不具有分散磁性纳米颗粒作为拉伸溶液的高渗透压深层共晶溶剂。 特别是分离在前者和后者中的氯化胆碱 - 乙二醇，氯化胆碱 - 甘油，Fe304用作FO溶液，用于一步淡化淡水和海水，从皮革和染料工业废水中回收水，蛋白质和DNA浓度 在室温下。 由于非常低的凝固点，通过在Ca下冷却通过相分离回收FO后的稀释的溶液。 -10℃，伴随生产可用水。 尽管本发明集中于Fe 3 O 4作为磁性纳米颗粒的具体DES和分散体，但是使用具有高渗透压和低凝固点的其它DES的其它磁性纳米颗粒分散体是本发明的逻辑延伸。

公开(公告)号：WO2016027280A8

公开(公告)日：2016-05-06

申请号：PCT/IN2015000322

申请日：2015-08-14

申请人： COUNCIL SCIENT IND RES

发明人： ALAMARU VENKATA RAMI REDDY ,  NATARAJ SANNA KOTRAPPANAVAR ,  PRASAD KAMALESH ,  MONDAL DIBYENDU ,  POLISETTI VEERA BABU ,  BHATT JITKUMAR ,  MAHTO ASHESH

IPC分类号： C02F1/44 ,  B01D61/00 ,  C02F1/22

CPC分类号： C02F1/445 ,  B01D61/005 ,  B01D71/56 ,  C02F1/22 ,  C02F2101/101 ,  C02F2101/12 ,  C02F2101/308 ,  C02F2103/08 ,  C02F2103/14 ,  C02F2103/24 ,  C02F2303/16 ,  Y02A20/131 ,  Y02A20/132 ,  Y02W10/37

摘要： The present invention relates to a novel forward osmosis (FO) process for dewatering of a variety of feed solution using low water activity and high osmotic pressure deep eutectic solvent with and without dispersed magnetic nanoparticles as draw solution. In particular, choline chloride-ethylene glycol, choline chloride- glycerol, Fe304 dispersed in former and latter were utilized as draw solution in FO for one step desalination of brackish and seawater, water recovery from effluent of leather and dye industries, protein and DNA concentration at room temperature. Owing to very low freezing point, the diluted draw solution after FO was recovered through phase separation by chilling at Ca. -10 °C with concomitant production of usable water. Although the present invention focused on specific DES and dispersion of Fe3O4 as magnetic nanoparticles but use of other DES having high osmotic pressure and low freezing point and other magnetic nanoparticles dispersion are logical extension of present invention.

摘要翻译： 本发明涉及用于使用低水活度和高渗透压深共晶溶剂（具有和不具有分散的磁性纳米粒子作为汲取溶液）对各种进料溶液进行脱水的新型正向渗透（FO）方法。 特别是氯化胆碱 - 乙二醇，氯化胆碱 - 甘油，分散在前者和后者中的Fe304被用作FO的汲取溶液，用于半咸水和海水的一步脱盐，皮革和染料工业废水的回收，蛋白质和DNA浓度 在室温下。 由于非常低的凝固点，通过在Ca中冷却而通过相分离回收FO后的稀释汲取溶液。 -10°C，同时生产可用水。 尽管本发明集中于作为磁性纳米颗粒的特定DES和Fe 3 O 4的分散，但使用具有高渗透压和低凝固点的其他DES和其他磁性纳米颗粒分散体是本发明的逻辑延伸。

公开(公告)号：WO2014027368A3

公开(公告)日：2014-04-10

申请号：PCT/IN2013000493

申请日：2013-08-12

申请人： COUNCIL SCIENT IND RES

发明人： GHOSH PUSHPITO KUMAR ,  MONDAL DIBYENDU ,  MAITI PRATYUSH ,  PRASAD KAMALESH ,  MAITI SUBARNA ,  SHAH BHARTI GUNVANTRAY ,  SIDDHANTA ARUP KUMAR

IPC分类号： C10L1/02 ,  C02F1/04 ,  C05D1/02 ,  C08B37/12 ,  C10L1/188 ,  C10L1/24 ,  C10L5/44

CPC分类号： C07D307/46 ,  C02F1/04 ,  C02F1/283 ,  C02F2303/02 ,  C05D1/00 ,  C05D1/02 ,  C07C51/31 ,  C07H3/02 ,  C08B37/0042 ,  C10L1/02 ,  C10L1/1881 ,  C10L1/1885 ,  C10L1/2493 ,  C10L5/44 ,  C10L2290/02 ,  C10L2290/04 ,  C10L2290/10 ,  C10L2290/12 ,  C10L2290/24 ,  C10L2290/28 ,  C10L2290/38 ,  C10L2290/44 ,  C10L2290/543 ,  C10L2290/544 ,  C10L2290/547 ,  C10L2290/548 ,  Y02E50/10 ,  Y02E50/30 ,  Y02P20/125 ,  Y02P20/136 ,  Y02W10/37

摘要： The invention relates to an integrated process for the production of 5-hydroxymethyl furfural (HMF), K2SO4, levulinic acid and formic acid from &kgr;-carrageenan, the latter being obtained from fresh Kappaphycus alvarezii seaweed biomass after expelling the juice. Mg(HSO4)2 was used in HMF synthesis, with co-production of galactose. The aqueous stream after HMF extraction was treated with the seaweed juice which process facilitated recovery of K2SO4 in pure form. The galactose may be utilised for synthesis of levulinic acid and formic acid before or after K2SO4 recovery or, alternatively, utilised for other purposes. Catalysts required in the synthetic reactions are generated in the process itself while the process energy required is met out of additional supplies of the seaweed biomass which is subjected to combustion/gasification.

摘要翻译： 本发明涉及一种用于从角叉菜胶生产5-羟甲基糠醛（HMF），K 2 SO 4，乙酰丙酸和甲酸的综合方法，后者是在榨出果汁后从新鲜的卡帕伐菌藻类海藻生物量获得的。 Mg（HSO4）2用于HMF合成，共同生产半乳糖。 HMF萃取后的水流用海藻汁处理，该方法便于纯化形式回收K 2 SO 4。 K2SO4回收前后，半乳糖可用于合成乙酰丙酸和甲酸，或者用于其他目的。 在合成反应中需要的催化剂在工艺本身中产生，而所需的工艺能量通过进行燃烧/气化的海藻生物质的额外供应来满足。

公开(公告)号：WO2006059180A3

公开(公告)日：2008-01-17

申请号：PCT/IB2004003977

申请日：2004-12-03

申请人： COUNCIL SCIENT IND RES

发明人： GHOSH PUSHPITO KUMAR ,  SIDDHANTA ARUP KUMAR ,  PRASAD KAMALESH ,  MEENA RAMAVATAR ,  BHATTACHARYA AMIT

IPC分类号： C08B37/12 ,  A61K9/48 ,  C08B37/00 ,  C08L5/00 ,  C08L5/12

CPC分类号： C08B37/0042 ,  C08J5/18 ,  C08J2305/00 ,  C08L5/00 ,  C08L5/12 ,  C08L2666/02

摘要： The present invention relates to use of inexpensive semi-refined kappa carrageenan as a seaweed polysaccharide in preparation of tough, biodegradable films exhibiting improved performance over films obtained from refined kappa carrageenan. The formulation requires no gelling salt and the only other essential components of the film are glycerol and water, the former being used as plasticizer as reported in the prior art. The films can be recycled and reprocessed if required. The performance of the films can be further enhanced by incorporating polyvinyl alcohol that lends toughness and clarity as also natural rubber latex that imparts greater elasticity and barrier properties. Films of optimum composition can be pulse heat sealed immediately after casting and used for preparation of soft capsules and pouches. It is possible to store solvents and oils in the pouches. In view of the more eco­friendly processing of semi-refined kappa carrageenan compared to refined kappa carrageenan, films made with the former would also effectively be "greener".

摘要翻译： 本发明涉及廉价的半精制卡波卡拉胶作为海藻多糖的用途，用于制备韧性可生物降解的膜，其表现出从精制的卡拉卡拉胶获得的薄膜的性能改善。 制剂不需要胶凝盐，膜的唯一其它基本组分是甘油和水，前者被用作现有技术中报道的增塑剂。 如果需要，这些胶片可以回收再利用。 通过加入提供韧性和透明度的聚乙烯醇以及赋予更大弹性和阻隔性能的天然橡胶胶乳，可以进一步提高膜的性能。 最佳组成的膜可以在铸造后立即进行脉冲热封，并用于制备软胶囊和小袋。 可以将溶剂和油储存在袋中。 鉴于与精制卡波卡拉胶相比，半精制卡波卡拉胶更加环保的加工，与前者相比的电影也将更加“绿化”。