-
公开(公告)号:WO2023086241A1
公开(公告)日:2023-05-19
申请号:PCT/US2022/048573
申请日:2022-11-01
摘要: A gas separator includes a first distillation chamber and an evaporation chamber. A first liquid valve comprises an inlet in fluid communication with the first distillation chamber and an outlet in fluid communication with the evaporation chamber. A chiller is configured to chill the first distillation chamber to a first temperature and the evaporation chamber to a second temperature that is different than the first temperature. The gas separator operates a first mode during which distillation a gas mixture is received by the first distillation chamber, the gas mixture is separated into a first condensed liquid and a first separated gas mixture, and the separated gas is output by the first distillation chamber. During a second mode, the first liquid valve transfers the first condensed liquid to the evaporation chamber and the first distillation does not receive the gas mixture and does not supply the first separated gas mixture.
-
公开(公告)号:WO2022131737A1
公开(公告)日:2022-06-23
申请号:PCT/KR2021/018945
申请日:2021-12-14
申请人: 한화솔루션 주식회사
摘要: 본 발명은 염소화 반응의 HCl 제거방법에 관한 것으로, 더 상세하게는 방향족 화합물의 염소화 반응 시 생성된 HCl을 효율적으로 제거할 수 있는 방법에 관한 것이다. 본 발명은 컬럼형 반응기가 상호 직렬 연결되어, 말단이 염소로 치환된 최종 생성물을 제조하는 염소화 반응에 있어서, 상기 최후단에 위치하는 반응기와 연결된 스트립핑컬럼에서 상기 염소화 반응에서 발생된 염화수소를 가열시켜 제거하는 단계를 포함한다.
-
公开(公告)号:WO2022073853A1
公开(公告)日:2022-04-14
申请号:PCT/EP2021/077012
申请日:2021-09-30
发明人: BRACE, James William
摘要: The present disclosure relates generally to processes and systems for distillation of acetic acid products. In one aspect, the disclosure provides a process for separating a feed stream comprising acetic acid and propionic acid in a distillation column. The process includes introducing a feed stream into the column through a feed inlet; withdrawing a first product stream comprising acetic acid and propionic acid from a first draw outlet disposed at a level above the level of the feed inlet; and withdrawing a second product stream comprising acetic acid and propionic acid from a second draw outlet disposed at a level between the level of the feed inlet and the level of the first draw outlet. The volume ratio of the first product stream to the second product stream is in the range of 1:9 to 19:1; and the amount of propionic acid present in the second product stream is at least 50 ppmw greater than the amount of propionic acid present in the first product stream.
-
公开(公告)号:WO2020169934A1
公开(公告)日:2020-08-27
申请号:PCT/FR2020/050322
申请日:2020-02-20
申请人: GRIMS , INSTITUT NATIONAL POLYTECHNIQUE DE TOULOUSE , CENTRE NATIONAL DE LA RECHERCHE SCIENTIFIQUE - CNRS -
摘要: L'invention concerne un procédé de transfert thermique entre un premier et un deuxième fluide dans lequel le premier et le deuxième fluide circulent respectivement de part et d'autre d'une paroi thermiquement conductrice (3) d'un ensemble monobloc (1) formé d'un seul tenant agencé à l'intérieur d'un dispositif (10), l'ensemble monobloc (1) comportant: - une première structure tridimensionnelle alvéolaire thermiquement conductrice (2) apte à être traversée par le premier fluide, - au moins ladite paroi (3), et - une deuxième structure tridimensionnelle alvéolaire thermiquement conductrice (4) apte à être traversée par le deuxième fluide, la première structure tridimensionnelle alvéolaire (2) et la deuxième structure tridimensionnelle alvéolaire (4) étant situées de part et d'autre de ladite paroi (3) et solidaires de ladite paroi (3), de sorte que le transfert thermique est réalisé du premier fluide vers le deuxième fluide à travers ladite paroi (3) et que chacun des premier et deuxième fluides est à la fois sous phase liquide et sous phase gazeuse, la phase liquide du premier fluide circulant dans un sens opposé à la phase gazeuse du premier fluide et la phase liquide du deuxième fluide circulant dans un sens opposé à la phase gazeuse du deuxième fluide.
-
公开(公告)号:WO2020104472A1
公开(公告)日:2020-05-28
申请号:PCT/EP2019/081830
申请日:2019-11-19
发明人: RICHTER, Michael
摘要: Der Erfindung, die ein Verfahren und eine Vorrichtung zur Reinigung von verschmutzten Altöl betrifft, bei dem Ausgangsmaterial bis zur Gasphase erwärmt und der dabei entstehende Dampf rektifiziert wird, wobei gereinigtes Öl als Kondensat aus einem Abzug in einer Rektifikationskolonne entnommen wird, liegt die Aufgabe zugrunde, ein Verfahren und Vorrichtung zur Reinigung von verschmutztem Altöl anzugeben, welches auch in Kleinstanlagen eine effiziente Arbeit ermöglicht, so dass eine kompakte Anlagenkonfiguration und damit insbesondere ein mobiler Einsatz durch einen Containeraufbau ermöglicht wird. Der Erfindung liegt auch die Aufgabe zugrunde, den Aufwand für die Wartung zu verringern. Die erfindungsgemäße Aufgabenstellung wird dadurch gelöst, dass Altöl einer Verdampfung durch eine zumindest mittelbare Kontaktierung des Ausgangsmaterials mit einem Schmelzbad, dessen Schmelztemperatur über der Verdampfungstemperatur jedoch unter der Zündtemperatur des Altöls liegt, unterzogen wird und der Dampf in der Rektifikationskolonne rektifiziert wird.
-
公开(公告)号:WO2020023296A1
公开(公告)日:2020-01-30
申请号:PCT/US2019/042536
申请日:2019-07-19
申请人: UOP LLC
发明人: GOYAL, Amit , GHOSH, Sudipta , HAAS, Joe R.
摘要: An apparatus for separating a feed stream into product streams. The apparatus includes an upper section, a middle section, and a lower section. The middle section has a dividing wall separating it into two portions. A liquid barrier blocks the flow of liquid from the upper section into the middle section and allows vapor to flow from the middle section to the upper section. A vapor and liquid barrier blocks both the flow of both vapor from the lower section to the middle section and the flow of liquid from the middle section to the lower section. Vapor conduits allow vapor to flow from the lower section to each of the middle portions in varying amounts. Also processes for separating a feed stream.
-
公开(公告)号:WO2019191375A1
公开(公告)日:2019-10-03
申请号:PCT/US2019/024498
申请日:2019-03-28
申请人: NORELL, INC. , NORELL, Gregory B.
发明人: NORELL, Gregory B.
摘要: Described herein is a column packing for a distillation apparatus, the column packing having an upper end opposite a lower end, the column packing comprising: a body extending along a central axis, the body comprising: a central channel extending parallel to the central axis, the central channel comprising a first open end opposite a second open end; and a plurality of perimeter channels circumscribing the central channel, each of the perimeter channels comprising a first open end opposite a second open end wherein the multi-channel body is formed of fluoropolymer.
-
公开(公告)号:WO2019176188A1
公开(公告)日:2019-09-19
申请号:PCT/JP2018/044164
申请日:2018-11-30
申请人: 東洋エンジニアリング株式会社
IPC分类号: B01D3/32
摘要: 非断熱型蒸留塔1は、循環する作動流体により濃縮部2内の流体を間接的に冷却する第1および第2の冷却装置11,12と、循環する作動流体により回収部3内の流体を間接的に加熱する第1および第2の加熱装置21,22と、第1の冷却装置11と第1の加熱装置21との間の第1の循環経路P11~P14上で第1の冷却装置11からの作動流体を圧縮する第1の圧縮機31と、第2の冷却装置12と第2の加熱装置22との間の第2の循環経路P21~P24上で第2の冷却装置12からの作動流体を圧縮する第2の圧縮機32と、第1の循環経路P11~P14上で第1の加熱装置21からの作動流体を膨張させる第1の膨張装置41と、第2の循環経路P21~P24上で第2の加熱装置22からの作動流体を膨張させる第2の膨張装置42とを有している。
-
公开(公告)号:WO2019152980A1
公开(公告)日:2019-08-08
申请号:PCT/US2019/016631
申请日:2019-02-05
发明人: ROSS-MEDGAARDEN, Elizabeth I. , LEYSHON, David W. , RUFENER, Karl P. , KONGKITISUPCHAI, Sunti , WOLFF, Richard J. , PETRY, Kimberly A.
IPC分类号: C07D301/32 , B01D3/32
CPC分类号: C07D301/32 , B01D3/008 , B01D3/143 , B01D3/40 , B01D3/4227
摘要: A propylene oxide separation system comprising a heavies distillation column configured to receive a crude propylene oxide stream and discharge a heavies purge bottoms comprising at least one impurity selected from acetone, methanol, aldehydes, aldehyde derivatives, water, heavy hydrocarbons comprising C 5+ , or combinations thereof, and discharge a heavies distillation column overhead stream comprising a majority of the propylene oxide entering with the crude propylene oxide stream, and a first extractive distillation column configured to receive the heavies distillation column overhead stream and a first extraction solvent stream comprising a hydrocarbon solvent, and discharge a lights purge overhead comprising at least one impurity selected from aldehydes (e.g., acetaldehyde, formaldehyde, etc.) methyl formate, methanol, water, C 3 hydrocarbons, C 4 hydrocarbons, or combinations thereof, and discharge a rich solvent bottoms stream comprising a majority of the propylene oxide entering via the heavies distillation column overhead stream. A propylene oxide purification method is also provided.
-
10.
公开(公告)号:WO2019040252A1
公开(公告)日:2019-02-28
申请号:PCT/US2018/044913
申请日:2018-08-02
发明人: SABODA, Kevin J. , BELANGER, Paul W. , LENZ, Richard D. , LARSON, Kirk F. , BROWN, Steven C. , RICOTTA, John P. , CHEN, Guang X. , FAUST, Jeremy D.
摘要: An annular divided wall column for the cryogenic rectification of air or constituents of air is provided. The annular divided wall column includes a first annular column wall and a second annular column wall disposed within the first annular column wall to define an annulus column region and an interior core column region. The present annular divided wall column further includes structured packing elements disposed within at least the annulus column region as well as a ring-shaped cantilevered collector; and a ring-shaped distributor disposed in the annulus column region above or below the plurality of structured packing elements. The thermal expansion and contraction of the second annular column wall in a radial direction and in an axial direction is independent of the thermal expansion and contraction of the first annular column wall in the radial and axial directions.
-
-
-
-
-
-
-
-
-