- 专利标题: Method for preparing phase-separated lead telluride-lead sulfide nanopowder using solution synthesis and phase-separated lead telluride-lead sulfide nanopowder prepared thereby
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申请号: US15739536申请日: 2016-06-24
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公开(公告)号: US10399148B2公开(公告)日: 2019-09-03
- 发明人: Yun-Mo Sung , Ki-Hyun Cho
- 申请人: Korea University Research and Business Foundation
- 申请人地址: KR Seoul
- 专利权人: Korea University Research and Business Foundation
- 当前专利权人: Korea University Research and Business Foundation
- 当前专利权人地址: KR Seoul
- 代理机构: Fox Rothschild LLP
- 优先权: KR10-2015-0090885 20150626
- 国际申请: PCT/KR2016/006741 WO 20160624
- 国际公布: WO2016/209018 WO 20161229
- 主分类号: C01G21/00
- IPC分类号: C01G21/00 ; C01G21/21 ; B22F9/24 ; B22F1/00 ; C01B17/20 ; C01B19/00 ; C04B35/626 ; C04B35/628
摘要:
The present invention relates to a method for preparing a phase-separated lead telluride-lead sulfide nanopowder using solution synthesis and a phase-separated lead telluride-lead sulfide nanopowder prepared by the method. The method includes: (a) mixing tellurium and a first solvent, followed by ultrasonic irradiation to prepare a tellurium precursor solution; (b) mixing an organosulfur compound and a second solvent, followed by ultrasonic irradiation to prepare a sulfur precursor solution; (c) mixing lead oxide, a third solvent, and a fourth solvent and heating the mixture to prepare a lead precursor solution; (d) adding the tellurium precursor solution to the lead precursor solution and allowing the mixture to react; (e) adding the sulfur precursor solution to the reaction mixture of step (d) and allowing the resulting mixture to react; and (f) cooling the reaction mixture of step (e) to room temperature to prepare a phase-separated lead telluride-lead sulfide nanopowder.
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