公开(公告)号：EP2210658B1

公开(公告)日：2015-08-26

申请号：EP08847962.1

申请日：2008-09-11

申请人： M Technique Co., Ltd.

发明人： ENOMURA, Masakazu

IPC分类号： B01F3/08 ,  B01J13/00 ,  B01F7/00

CPC分类号： B01F7/00758 ,  B01F3/0807 ,  B01F7/00775 ,  B01F7/00791 ,  Y10S516/924

公开(公告)号：EP2818265A1

公开(公告)日：2014-12-31

申请号：EP13751729.8

申请日：2013-02-20

申请人： M Technique Co., Ltd.

发明人： AOYAGI, Shiho ,  ENOMURA, Masakazu

IPC分类号： B22F9/24 ,  B01F13/00 ,  B01F15/02 ,  B01J19/00

CPC分类号： B22F9/24 ,  B01F7/00775 ,  B01F2215/0409 ,  B01F2215/0431 ,  B01F2215/0481 ,  B01J19/1887 ,  B01J2219/00051 ,  B01J2219/00186 ,  B01J2219/00189 ,  B22F2301/00 ,  C22C13/00 ,  C22C28/00

摘要： The present invention addresses the problem of providing a method for producing microparticles. Composite microparticles are separated by mixing at least two kinds of fluids to be processed in a thin film fluid that is formed between approachable and separable opposing processing surfaces that relatively rotate, wherein the fluids to be processed are a metal fluid comprising at least two kinds of metal elements that are dissolved in a solvent in the form of metal and/ or metal compound and a fluid for separation containing at least one kind of separating substance for separating a composite substance comprising the at least two kinds of metal elements. The molar ratio between the at least two kinds of metal elements contained in the resulting microparticles is controlled by controlling the circumferential speed of the rotation at a confluence where the metal fluid and the fluid for separation merge at this time.

摘要翻译： 本发明解决了提供生产微粒的方法的问题。 通过在相对旋转的可接近和可分离的相对处理表面之间形成的薄膜流体中混合至少两种待处理流体来分离复合微粒，其中待处理流体是包含至少两种 以金属和/或金属化合物的形式溶解在溶剂中的金属元素和用于分离包含至少两种金属元素的复合物质的至少一种分离物质的用于分离的流体。 通过控制此时金属流体和分离用流体汇合的汇合处的旋转的圆周速度来控制所得微粒中包含的至少两种金属元素之间的摩尔比。

公开(公告)号：EP2351796B1

公开(公告)日：2014-10-22

申请号：EP09816273.8

申请日：2009-09-29

申请人： M Technique Co., Ltd.

发明人： ENOMURA Masakazu

IPC分类号： C09B67/50 ,  C09B67/20 ,  B01F7/26 ,  C09B67/16

CPC分类号： C09B67/0026 ,  B01F7/00775 ,  B01F7/00791 ,  B01F7/00875 ,  C09B67/0019 ,  C09B67/0096 ,  C09D11/322 ,  C09D17/003 ,  Y10T428/2982

公开(公告)号：EP2732871A1

公开(公告)日：2014-05-21

申请号：EP12811710.8

申请日：2012-07-05

申请人： M Technique Co., Ltd.

发明人： AOYAGI Shiho ,  ARAKI Kaeko ,  MAEKAWA Masaki ,  KURAKI Jun ,  ENOMURA Masakazu

IPC分类号： B01J19/00 ,  B01D9/02

CPC分类号： B01D9/0063 ,  B01D9/0054 ,  B01J19/1887 ,  B01J2219/00085 ,  B01J2219/00164 ,  B01J2219/00177 ,  C04B35/626 ,  C22B15/0089

摘要： The present invention addresses the problem of providing a method for producing microparticles having a controlled crystallite diameter. At least two types of fluids to be processed; i.e., a raw material fluid containing a substance to be separated, and a separating fluid containing a substance for causing separation of the substance to be separated, are mixed in a thin film fluid formed between at least two processing surfaces which are approachably and separably disposed facing each other. At least one processing surface rotates relative to the other, and the substance to be separated giving a controlled crystallite diameter is caused to separate. At this time, specific conditions related to the fluid to be processed introduced between the processing surfaces are varied to control the crystallite diameter of the substance to be separated. The specific conditions are at least two conditions selected from the group consisting of: the type of substance to be separated included in the raw material fluid and/ or substance included in the separating fluid; the concentration of the substance to be separated included in the raw material fluid and/ or substance included in the separating fluid; the pH of the raw material fluid and / or separating material fluid; the introduction temperature of the raw material fluid and/ or separating fluid; and the introduction velocity of the raw material fluid and/ or separating fluid.

摘要翻译： 本发明涉及提供具有受控微晶直径的微粒的制造方法的问题。 至少两种待处理的流体; 即含有待分离物质的原料流体和含有分离物质的分离液体的分离液体混合在形成在至少两个可接近和可分离的处理表面之间的薄膜流体中 面对彼此 至少一个处理表面相对于另一个处理表面旋转，并且使被分离的物质得到受控的微晶直径。 此时，在处理用面之间引入的与待处理流体有关的特定条件变化，以控制待分离物质的微晶直径。 具体条件为选自以下的至少两种条件：待分离的物质的类型包括在原料流体中的物质和/或包含在分离流体中的物质; 要分离的物质的浓度包括在分离流体中包含的原料流体和/或物质中; 原料流体和/或分离材料流体的pH; 原料流体和/或分离流体的导入温度; 和原料流体和/或分离流体的引入速度。

公开(公告)号：EP2703075A1

公开(公告)日：2014-03-05

申请号：EP12776554.3

申请日：2012-04-13

申请人： M Technique Co., Ltd.

发明人： ENOMURA, Masakazu

IPC分类号： B01J19/00

CPC分类号： B29B9/16 ,  B01F7/00775 ,  B01J19/1887 ,  B01J2219/00094 ,  B01J2219/00103 ,  B01J2219/00135 ,  B01J2219/00159 ,  B01J2219/00162 ,  B01J2219/00198 ,  B01J2219/00213 ,  B01J2219/00238 ,  B01J2219/182 ,  B01J2219/185 ,  B01J2219/187 ,  B82Y40/00

摘要： The invention addresses the problem of providing a novel method for controlling the particle size of deposited fine particles in a fine particle production method that introduces a fluid to be processed between at least two processing surfaces, which are disposed facing each other, are advancible and retractable, and at least one rotates relative to the other, to deposit fine particles in the thin fluid film which forms between said processing surfaces. A fluid to be processed is introduced between processing surfaces (1, 2) that are disposed facing each other, are advancible and retractable, and at least one rotates relative to the other to deposit fine particles in the thin fluid film that forms between the processing surfaces (1, 2). The particle size of said fine particles is controlled by controlling the temperature of the fluid to be processed that contains the deposited fine particles. Said temperature control can be accomplished by providing a temperature adjusting apparatus (33) and a jacket (34) in the flow channel or receptacle for the fluid to be processed after outflow and controlling the temperature of the fluid to be processed that contains the deposited fine particles.

摘要翻译： 本发明解决了以下问题：提供一种用于在至少两个彼此面对设置的处理表面之间引入待处理流体的微粒生产方法中用于控制沉积微粒的粒度的新方法的问题是可自由伸缩 并且至少一个相对于另一个旋转，以便在形成在所述处理表面之间的薄流体膜中沉积精细颗粒。 待处理流体被引入在彼此面对设置的处理表面（1,2）之间，可自由伸缩，并且至少一个相对于另一个旋转，以将细颗粒沉积在形成于处理表面之间的薄流体膜中 表面（1,2）。 通过控制包含沉积的微粒的待处理流体的温度来控制所述微粒的粒径。 所述温度控制可以通过在流出通道或容器中设置温度调节装置（33）和护套（34），用于流出后的待处理流体并控制含有沉积的细粒的待处理流体的温度 粒子。

公开(公告)号：EP2690079A1

公开(公告)日：2014-01-29

申请号：EP11861829.7

申请日：2011-03-23

申请人： M Technique Co., Ltd.

发明人： KURAKI Jun ,  MAEKAWA Masaki ,  HONDA Daisuke ,  ENOMURA Masakazu

IPC分类号： C04B35/626 ,  B01F5/06 ,  B01J19/00 ,  C01B33/193 ,  C01F7/02 ,  C01G9/02 ,  C01G23/04

CPC分类号： C01B33/113 ,  B01F7/00775 ,  B01F7/00791 ,  B01J14/00 ,  B01J19/1887 ,  C01B9/00 ,  C01B13/14 ,  C01B13/16 ,  C01B13/36 ,  C01B19/00 ,  C01B21/00 ,  C01B32/00 ,  C01B33/00 ,  C01B33/193 ,  C01B35/00 ,  C01G9/02 ,  C01G23/003 ,  C01P2002/72 ,  C01P2004/04 ,  C04B35/62625 ,  C04B2235/3284 ,  C04B2235/3418 ,  C04B2235/5445 ,  C04B2235/5454 ,  C04B2235/76

摘要： Provided is a more suitable method for producing ceramic microparticles. The present invention uses at least two types of fluids to be processed; at least one of the fluids to be processed is a fluid containing a ceramic starting material liquid that mixes and/ or dissolves a ceramic starting material in a basic solvent; of the fluids aside from the ceramic starting material liquid, at least one of the fluids to be processed is a fluid containing a solvent for precipitating ceramic microparticles; and ceramic microparticles are precipitated by mixing the fluid containing the ceramic starting material liquid and the fluid containing the solvent for precipitating ceramic microparticles within a thin film fluid formed between at least two surfaces (1,2) for processing that are provided facing each other, are able to approach and separate each other, and of which one is able to rotate with respect to the other. Ceramic microparticles having as increased crystallinity are obtained by mixing the fluid containing the precipitated ceramic microparticles precipitate and a fluid containing an acidic substance.

摘要翻译： 提供了一种更合适的陶瓷微粒的制造方法。 本发明使用至少两种待处理的流体; 要处理的流体中的至少一种是含有在碱性溶剂中混合和/或溶解陶瓷原料的陶瓷原料液的流体; 的待处理流体中的至少一种是含有用于沉淀陶瓷微粒的溶剂的流体; 并且通过将包含陶瓷原料液的流体和含有溶剂的流体混合在一起形成在用于相互面对的处理的至少两个表面（1,2）之间的薄膜流体中而沉淀陶瓷微粒， 能够彼此接近和分离，并且能够相对于另一个旋转。 通过混合含有沉淀的陶瓷微粒沉淀物的液体和含有酸性物质的流体，获得结晶度增加的陶瓷微粒。

公开(公告)号：EP2556884A1

公开(公告)日：2013-02-13

申请号：EP11766024.1

申请日：2011-04-08

申请人： M. Technique Co., Ltd.

发明人： ENOMURA, Masakazu

IPC分类号： B01J19/00 ,  B01F7/26

CPC分类号： B01J19/1887 ,  B01F3/0807 ,  B01F7/00775 ,  B01F7/00791 ,  B01J2219/00094 ,  B01J2219/00132 ,  Y10T137/0318

摘要： In order to enable the more stable performance of uniform treatment such as reaction by reducing pulsation generated in a fluid introduced between treatment surfaces using a micropump effect, provided is a device for treating an object to be treated between treatment surfaces (1, 2) facing each other of treatment parts which can move close to and away from each other and at least one of which rotates relatively with respect to the other, and performing the treatment by introducing a fluid between the treatment surfaces using a micropump effect by a recessed section (13) formed in at least one of the treatment surfaces (1, 2) and mixing and stirring the fluid between the treatment surfaces. The micropump effect generates force in the direction in which the treatment surfaces (1, 2) move away from each other by the rotation of a treatment part (10) and the recessed section (13) formed in the treatment surface (1) to thereby produce the effect of introducing the fluid between the treatment surfaces (1, 2). The recessed section (13) is formed so as to extend in the circumferential direction and inward/outward direction of the treatment surface (1), and multiple recessed sections (13) are provided or an additional recessed section (α) different from the recessed sections (13) is formed in at least one of the treatment surfaces (1, 2).

摘要翻译： 为了能够通过减少使用微泵效应在处理表面之间引入的流体中产生的脉动来实现均匀处理（例如反应）的更稳定的性能，提供了一种用于在处理表面（1,2） 彼此相互接近并相互移动的处理部件，并且其中至少一个相对于另一个旋转相对旋转，并且通过使用由凹部来的微泵效应在处理表面之间引入流体来进行处理（ 13），其形成在处理表面（1,2）的至少一个中，并且在处理表面之间混合和搅拌流体。 微型泵效应通过处理部（10）和形成在处理面（1）中的凹部（13）的转动而使处理面（1,2）相互移动的方向产生力，从而 产生在处理表面（1,2）之间引入流体的效果。 凹部（13）形成为在处理面（1）的周向和内/外方向上延伸，并且设置有多个凹部（13），或者与凹部（13）不同的附加凹部（±） 在至少一个处理面（1,2）中形成有切片（13）。

公开(公告)号：EP2540390A1

公开(公告)日：2013-01-02

申请号：EP11747294.4

申请日：2011-02-21

申请人： M Technique Co., Ltd.

发明人： ENOMURA Masakazu

IPC分类号： B01J19/18 ,  B01F3/08 ,  B01F5/00 ,  B01J19/00

CPC分类号： B01F7/00775 ,  B01F3/0807 ,  B01F7/00791 ,  B01J19/1887 ,  Y10T137/598 ,  Y10T137/8593 ,  Y10T137/87652

摘要： A fluid processing apparatus for processing a material to be processed between processing surfaces (1, 2) of processing members capable of approaching to and separating from each other, so as to rotate relative to each other, introduces a first fluid between the processing surfaces (1, 2), introduces a second fluid between the processing surfaces (1, 2) from another flow path (d2) independent of the first fluid, and mixes and stirs the first and second fluids between the processing surfaces (1, 2) to undergo treatment. A processing member (20) of the apparatus is composed by assembling a plurality of divided components of the processing member (20a, 20b). An opening (d20) and a flow path (d2) are formed in the space between the plurality of components of the processing member (20a, 20b). This eliminates the need to create all ring-shaped disks which are the processing member (20) as one block, and also eliminates the need to substantially process the flow path (d2) leading to the opening (d20), thereby making it possible to easily undergo decomposition and cleaning.

摘要翻译： 本发明提供一种流体处理装置，该流体处理装置在能够相互接近分离的处理用部件的处理用面（1,2）之间相互相对旋转地处理被处理物，并在处理用面间导入第一流体 （1,2）中的第一流体从独立于第一流体的另一流动路径（d2）在处理表面（1,2）之间引入第二流体，并且在处理表面（1,2）与第一流体之间混合并搅拌第一流体和第二流体， 接受治疗。 该装置的处理部件（20）通过组装处理部件（20a，20b）的多个分割部件而构成。 在处理构件（20a，20b）的多个构件之间的空间中形成开口（d20）和流动路径（d2）。 由此，不需要将作为处理用构件20的全部的环状圆盘作为一个块体来形成，并且也不需要对通向开口部d20的流路d2进行实质性的处理， 容易分解和清洁。

公开(公告)号：EP2184110A1

公开(公告)日：2010-05-12

申请号：EP08790917.2

申请日：2008-07-04

申请人： M Technique Co., Ltd.

发明人： ENOMURA, Masakazu

IPC分类号： B02C7/14 ,  B01F7/26 ,  B01J19/00 ,  B41J2/01 ,  B41M5/00 ,  C09B67/02 ,  C09B67/10 ,  C09B67/20 ,  C09D11/00

CPC分类号： B01J19/0093 ,  B01F7/00758 ,  B01F7/00791 ,  B01J19/10 ,  B01J19/123 ,  B01J19/1887 ,  B01J2219/00094 ,  B01J2219/00137 ,  C09B67/0022 ,  C09B67/0091 ,  Y10T137/0396 ,  Y10T137/6416 ,  Y10T137/8593 ,  Y10T137/85978

摘要： A fluid is processed between processing surfaces capable of approaching to and separating from each other, at least one of which rotates relative to the other. A first fluid containing a material to be processed is introduced between processing surfaces 1 and 2, by using a micropump effect acting with a depression 13 arranged on the processing surfaces from the center of the rotating processing surfaces. A second fluid containing a material to be processed, independent of this introduced fluid, is introduced from another fluid path d2 that is provided with an opening d20 leading to the processing surfaces, whereby the processing is done by mixing and stirring between the processing members 1 and 2. In a plane along the processing surfaces, directionality accompanies the introducing direction from the opening of the second fluid into the processing surfaces. Regarding the introducing direction of the second fluid, it is an outward direction away from the center for the fluid in the radial direction on the processing surface, and it is a forward direction for the fluid in the rotation direction of the fluid between the rotating processing surfaces.

摘要翻译： 在能够接近和分离的处理表面之间处理流体，其中至少一个相对于另一个旋转。 通过使用与从旋转处理用面的中心配置在处理用面上的凹部13起作用的微型泵效果，在处理用面1,2之间引入含有被处理材料的第一流体。 含有与被引入的流体无关的待处理材料的第二流体从另一个流体路径d2引入，该流体通道d2设置有通向处理表面的开口d20，由此通过在处理构件1之间进行混合和搅拌来进行处理 在沿着处理表面的平面中，方向性伴随着从第二流体的开口进入处理表面的引入方向。 关于第二流体的引入方向，在处理用面上为径向的流体的中心的向外方向是流体在旋转处理之间的流体的旋转方向的向前方向 表面。

公开(公告)号：EP2184109A1

公开(公告)日：2010-05-12

申请号：EP08790916.4

申请日：2008-07-04

申请人： M Technique Co., Ltd.

发明人： ENOMURA, Masakazu

IPC分类号： B02C7/14 ,  B01J19/00 ,  B41J2/01 ,  B41M5/00 ,  C09B67/02 ,  C09B67/10 ,  C09B67/20

CPC分类号： B01F3/0807 ,  B01F3/1221 ,  B01F5/221 ,  B01F7/00758 ,  B01F7/00775 ,  B01F7/00791 ,  B01J19/1887 ,  B22F1/0018 ,  B22F9/24 ,  B22F2998/00 ,  B22F2999/00 ,  C09B67/0022 ,  B22F1/0022 ,  B22F3/003

摘要： The present invention provides a method for producing nanoparticles, which comprises maintaining a minute space of 1 mm or less between two processing surfaces capable of approaching to and separating from each other and being rotating relative to each other, allowing the minute space maintained between the two processing surfaces to serve as a flow path of a processed fluid thereby forming a forced thin film of the processed fluid and separating nanoparticles in the forced thin film.