A method for producing a multilayer structure
    22.
    发明公开
    A method for producing a multilayer structure 审中-公开
    HerstellungsverfahrenfürMehrschichtstruktur

    公开(公告)号:EP2103719A1

    公开(公告)日:2009-09-23

    申请号:EP08005041.2

    申请日:2008-03-18

    摘要: Provided is method for producing a multilayer structure, one method comprising the steps of:
    - providing a suspension comprising first particles and second particles, wherein the first and second particles have opposite charges;
    - introducing an electrode and a counterelectrode into the suspension;
    - applying a current to said electrode and counterelectrode, whereby at least one layer comprising said first particles is deposited on said electrode and at least one layer comprising said second particles is deposited on the counterelectrode; and
    - changing the direction of the current applied to said electrode and said counterelectrode, whereby at least one layer comprising said second particles is deposited on the electrode and at least one layer comprising said first particles is deposited on the counterelectrode.
    In another embodiment, there is provided a method for producing a multilayer structure, comprising the steps of:
    - providing a suspension comprising first particles and particles having magnetic properties, wherein the first particles are charged;
    - introducing an electrode having electromagnetic properties and a counterelectrode into the suspension;
    - applying current to said electromagnetic electrode and counterelectrode, whereby at least one layer comprising said first particles is deposited on said electrode; and
    - applying an electromagnetic field to said electrode, whereby at least one layer comprising said particles having magnetic properties is deposited on said electrode.
    The present invention also provides multilayer structures obtainable by said processes.

    摘要翻译: 提供了一种制备多层结构的方法,一种方法包括以下步骤: - 提供包含第一颗粒和第二颗粒的​​悬浮液,其中第一和第二颗粒具有相反的电荷; - 将电极和反电极引入悬浮液中; - 向所述电极和反电极施加电流,由此在所述电极上沉积包含所述第一颗粒的至少一层,并且包含所述第二颗粒的​​至少一层沉积在所述反电极上; 以及 - 改变施加到所述电极和所述反电极的电流的方向,由此将包含所述第二颗粒的​​至少一个层沉积在所述电极上,并且包含所述第一颗粒的至少一个层沉积在所述反电极上。 在另一个实施方案中,提供了一种制备多层结构的方法,包括以下步骤: - 提供包含第一颗粒和具有磁性的颗粒的悬浮液,其中第一颗粒被带电; - 将具有电磁特性的电极和反电极引入所述悬浮液中; - 向所述电磁电极和对电极施加电流,由此在所述电极上沉积包含所述第一颗粒的至少一层; 以及 - 向所述电极施加电磁场,由此在所述电极上沉积包含具有磁特性的所述颗粒的至少一层。 本发明还提供了可通过所述方法获得的多层结构。

    Piezoelectric tubes
    23.
    发明公开
    Piezoelectric tubes 有权
    压电管

    公开(公告)号:EP1976039A3

    公开(公告)日:2009-01-14

    申请号:EP08104575.9

    申请日:2004-02-12

    摘要: A method and apparatus for forming piezoelectric tubes is provided. The method includes forming a suspension (1) of ceramic particles (2) in a fluid medium (3), positioning a rod (5) in the fluid medium (3), depositing particles (2) on the rod (5) by electrophoresis, and heat-treating the deposited particles to form a piezoelectric tube by heating the deposited particles to a first predetermined temperature to solidify the particles to a surface of the rod and burn the rod, thereby leaving a tube of solidified particles closed at one end, and heating the tube to a second predetermined temperature to thereby sinter the tube to form a dense ceramic tube. The apparatus is adapted for carrying out the method.

    Self-healing layer on non-ferrous metals using polyoxometalates
    24.
    发明公开
    Self-healing layer on non-ferrous metals using polyoxometalates 审中-公开
    Selbstheilende Beschichtungen auf Nicht-Eisen-Metallen unter Verwendung von Polyoxometallaten

    公开(公告)号:EP1820882A1

    公开(公告)日:2007-08-22

    申请号:EP06075365.4

    申请日:2006-02-21

    摘要: The invention relates to a method for applying a multifunctional layer on a substrate. Accordingly said layer is applied by means of a process by using an aqueous solution that comprises a POM and/or a crack-healing agent, which POM and/or a crack healing agent is/are incorporated in said layer during said process to obtain a self-healing layer. Generally, said substrate comprises a metallic substrate, preferably a non-ferrous metallic substrate, and most preferably Al, Mg, Ti and alloys thereof. Said POMs are heteropolyanions of the type (X n M m O y ) x- , in which X=Si, P, Ce, B, Mn and in which M=Mo, W or V and y>1, m>1 and n≤m and x indicates the valence of the polyanion. A Keggin-type POM is preferred. Said crack-healing agent is selected from particles of mixed oxides, clay particles, metallic oxide/epoxy resin microspheres, or a mixture thereof. Preferably said POMs are supported by media selected from insoluble micro- or nanoparticles (e.g. SiO 2 ) or polymer capsules. The application of said layer occurs by means of conventional anodising, hard anodising, plasma electrolytic oxidation, or electro(less) deposition. Further the invention relates to said POM and/or a crack-healing agent. Finally, the present invention relates to a coated substrate, obtained by the method according to the invention.

    摘要翻译: 本发明涉及一种在基板上施加多功能层的方法。 因此,所述层通过使用包含POM和/或裂纹愈合剂的水溶液的方法施加,在所述方法期间将POM和/或裂纹愈合剂掺入所述层中以获得 自愈层 通常,所述衬底包括金属基底,优选有色金属基底,最优选Al,Mg,Ti及其合金。 所述POM是类型(X n M m O y)x-的杂多阴离子,其中X = Si,P,Ce,B,Mn,其中M = Mo,W或V,y> 1,m> 1和 n‰,x表示聚阴离子的化合价。 优选Keggin型POM。 所述裂纹愈合剂选自混合氧化物,粘土颗粒,金属氧化物/环氧树脂微球体或其混合物的颗粒。 优选地,所述POM由选自不溶性微粒或纳米颗粒(例如SiO 2)或聚合物胶囊的介质支持。 所述层的应用通过常规阳极氧化,硬质阳极氧化,等离子体电解氧化或电沉积(较少)进行。 此外,本发明涉及所述POM和/或裂纹愈合剂。 最后,本发明涉及通过本发明的方法获得的涂覆基材。

    PIEZOELECTRIC TUBES
    27.
    发明公开
    PIEZOELECTRIC TUBES 有权
    PIEZOELEKTRISCHERÖHREN

    公开(公告)号:EP1639657A4

    公开(公告)日:2006-08-30

    申请号:EP04710575

    申请日:2004-02-12

    申请人: UNIV NANYANG

    摘要: The present invention relates to a method of forming piezoelectric tubes. The method includes forming a suspension of ceramic particles in a fluid medium,positioning a rod in the fluid and then depositing particles on the rod using electrophoresis. The deposited layer is then heat treated to form a piezoelectric tube.

    摘要翻译: 提供一种用于形成压电管的方法和装置。 该方法包括在流体介质(3)中形成陶瓷颗粒(2)的悬浮液(1),将棒(5)定位在流体介质(3)中,通过电泳将颗粒(2)沉积在杆(5)上 并且通过将沉积的颗粒加热到第一预定温度来将沉积的颗粒热处理以形成压电管,以将颗粒固化到杆的表面并燃烧杆,从而在一端留下凝固的颗粒管, 并将管加热到第二预定温度,从而烧结管以形成致密的陶瓷管。 该装置适用于执行该方法。

    VERFAHREN ZUM HERSTELLEN VON METALLISCHEN FORMKÖRPERN MIT EINER KERAMISCHEN SCHICHT, METALLISCHER FORMKÖRPER UND DESSEN VERWENDUNG
    29.
    发明公开
    VERFAHREN ZUM HERSTELLEN VON METALLISCHEN FORMKÖRPERN MIT EINER KERAMISCHEN SCHICHT, METALLISCHER FORMKÖRPER UND DESSEN VERWENDUNG 有权
    方法制备金属有形体的陶瓷层,模具成形及其用途

    公开(公告)号:EP1587969A2

    公开(公告)日:2005-10-26

    申请号:EP04704542.2

    申请日:2004-01-23

    IPC分类号: C25D13/02

    摘要: The invention relates to a method for producing metallic moulded bodies comprising a ceramic layer according to the membrane method, whereby a porous metallic membrane is used. The invention also relates to a metallic moulded body comprising a ceramic layer and to the use of one such metallic moulded body. The aim of the invention is to provide a cost-effective, rapid method which is as non-polluting as possible for producing metallic moulded bodies comprising a ceramic layer according to the membrane method using a porous metallic membrane, whereby the penetration depth, the green density and the deposition speed of the ceramic particles in the metallic membrane can be controlled. To this end, the porous metallic membrane is sealed by electrophoretic deposition of ceramic particles in the pores of the metallic membrane, the metallic membrane being arranged between two electrodes for the electrophoretic deposition, and the space between an electrode and the metallic membrane being filled with a dispersion containing the ceramic particles to be deposited in the pores and a dispersant.

    IMPROVED METHOD OF ELECTROPHORETIC DEPOSITION OF FERROELECTRIC FILMS USING A TRI-FUNCTIONAL ADDITIVE AND COMPOSITIONS FOR EFFECTING SAME
    30.
    发明公开
    IMPROVED METHOD OF ELECTROPHORETIC DEPOSITION OF FERROELECTRIC FILMS USING A TRI-FUNCTIONAL ADDITIVE AND COMPOSITIONS FOR EFFECTING SAME 审中-公开
    改进方法电泳沉积FERRO电动MOVIES使用TRI-功能性添加剂和组合物对于这种应用

    公开(公告)号:EP1259660A2

    公开(公告)日:2002-11-27

    申请号:EP00971675.4

    申请日:2000-10-25

    IPC分类号: C25D13/02

    摘要: An improved method for depositing ferroelectric particles on a surface of a substrate to form films or stand-alone bodies. The improvement is based on electrophoretic deposition (EPD) of ferroelectric films by using a tri-functional phosphate ester additive having a concentration less than 10 volume percent in the EPD suspension, without the need for addition of a binder. The method includes preparation of the suspension by washing and dispersing ferroelectric particles, for example, commercially available PZT powder, in a polar solvent such as ethanol, followed by addition of the phosphate ester additive to the suspension, and an ultrasound treatment. The suspension is used in EPD of the ferroelectric particles on a prepared substrate. Following EPD, the green film is dried and sintered at high temperature. Visual and physical examination of stand alone and patterned PZT deposited films show excellent quality obtained in manufacturing a diversity of piezoelectric products, featuring exceptionally high green film uniformity, thickness distribution, and reproducibility to within ± 2 microns for 20 micrometer film thickness. The phosphate ester additive functions by improving stabilization and control of suspension characteristics and properties during the electrophoretic migration process, and by improving desired dimensions, characteristics, and electrical properties of the deposited green film. Thin or thick ferroelectric films, either as stand alone products, or formed on geometrically demanding patterned or non-patterned substrates are produced by using the method. The improved method is applicable to different ferroelectric particulate materials and to different substrates used for manufacturing piezoelectric elements and devices, in a cost effective manner.