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1.发明公开IMPROVED METHOD OF ELECTROPHORETIC DEPOSITION OF FERROELECTRIC FILMS USING A TRI-FUNCTIONAL ADDITIVE AND COMPOSITIONS FOR EFFECTING SAME 审中-公开改进方法电泳沉积FERRO电动MOVIES使用TRI-功能性添加剂和组合物对于这种应用
公开(公告)号：EP1259660A2
公开(公告)日：2002-11-27
申请号：EP00971675.4
申请日：2000-10-25
发明人： GAL-OR, Leah , GOLDNER, Roni , SEZIN, Nina , PISMANY, Ala , BRANDON, David
IPC分类号： C25D13/02
CPC分类号： C25D13/02 , H01L41/317 , H01L41/43
摘要： An improved method for depositing ferroelectric particles on a surface of a substrate to form films or stand-alone bodies. The improvement is based on electrophoretic deposition (EPD) of ferroelectric films by using a tri-functional phosphate ester additive having a concentration less than 10 volume percent in the EPD suspension, without the need for addition of a binder. The method includes preparation of the suspension by washing and dispersing ferroelectric particles, for example, commercially available PZT powder, in a polar solvent such as ethanol, followed by addition of the phosphate ester additive to the suspension, and an ultrasound treatment. The suspension is used in EPD of the ferroelectric particles on a prepared substrate. Following EPD, the green film is dried and sintered at high temperature. Visual and physical examination of stand alone and patterned PZT deposited films show excellent quality obtained in manufacturing a diversity of piezoelectric products, featuring exceptionally high green film uniformity, thickness distribution, and reproducibility to within ± 2 microns for 20 micrometer film thickness. The phosphate ester additive functions by improving stabilization and control of suspension characteristics and properties during the electrophoretic migration process, and by improving desired dimensions, characteristics, and electrical properties of the deposited green film. Thin or thick ferroelectric films, either as stand alone products, or formed on geometrically demanding patterned or non-patterned substrates are produced by using the method. The improved method is applicable to different ferroelectric particulate materials and to different substrates used for manufacturing piezoelectric elements and devices, in a cost effective manner.
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2.发明授权METHOD OF ELECTROPHORETIC DEPOSITION OF CERAMIC BODIES FOR USE IN MANUFACTURING DENTAL APPLIANCES 有权电泳涂膜参与制造牙科产品陶瓷体的方法中使用
公开(公告)号：EP1073781B2
公开(公告)日：2008-11-05
申请号：EP99911422.6
申请日：1999-03-16
CPC分类号： A61C13/001 , A61C5/77 , A61C13/0022 , C25D1/14 , C25D13/02 , H05K1/0306 , H05K3/022
摘要： A method for electrophoretic deposition of ceramic particles as a green body shaped as a dental appliance, the method comprising the steps of (a) forming a suspension of the ceramic particles in a first polar solvent, the ceramic particles constituting at least about 5 % of the first suspension by weight; (b) passing a direct electrical current through the first suspension, using a deposition electrode (20) shaped as the dental appliance to form a green body; (c) coating the green body with glass particles; and (d) sintering the resultant coated body for obtaining a glass coated all-ceramic dental appliance.
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3.发明公开
公开(公告)号：EP1017886A1
公开(公告)日：2000-07-12
申请号：EP98914661.8
申请日：1998-04-13
发明人： GAL-OR, Leah , BRANDON, David , GOLDNER, Roni , CHERNIAK, Liudmilla , PERLIN, Leonid , SEZIN, Nina , LIUBOVICH, Sonia
IPC分类号： C25D13/02
CPC分类号： C25D1/14 , A61C13/001 , C25D13/02 , H05K1/0306 , H05K3/022
摘要： A method of electrophoretic deposition of a ceramic green body. A ceramic powder is optionally washed with a polar solvent such as deionized water, dried, and suspended in a polar organic solvent in a proportion of at least 20 % by weight. A positive surface charge is imposed on the suspended particles by conventional means such as ball milling or ultrasonic treatment. A green body is deposited on a cathode by passing a direct electric current of constant current density through the suspension. The density of the green body generally is at least 70 % of theoretical. The density of the fired body generally is at least 98 % of theoretical. A layered green body may be deposited by using several suspensions of differing global ceramic composition and depositing each microlayer in a different suspension.
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4.发明授权A METHOD FOR THE IMPLEMENTATION OF ELECTRONIC COMPONENTS IN VIA-HOLES OF A MULTI-LAYER MULTI-CHIP MODULE 有权用于电子部件的执行程序通过多层多芯片模块的贯通孔
公开(公告)号：EP1354503B1
公开(公告)日：2007-08-01
申请号：EP01980882.3
申请日：2001-10-25
发明人： SCHUSTER, Israel
CPC分类号： H05K3/4061 , H01L21/486 , H01L23/5383 , H01L23/5384 , H01L23/58 , H01L23/647 , H01L2224/32225 , H01L2924/09701 , H01L2924/12044 , H01L2924/15192 , H01L2924/19105 , H05K1/0306 , H05K1/16 , H05K1/162 , H05K1/165 , H05K1/167 , H05K3/4611 , H05K3/4629 , H05K2201/0209 , H05K2203/135 , Y10T29/49082 , Y10T29/49089 , Y10T29/49099 , Y10T29/49101
摘要： The substrate (2) containing the via-hole (3) is inserted into an electrophoretic cell (1) and an electrode (6) (the 'first electrode') is placed on top of a first orifice of the via-hole(s) (3), to be implemented with electrical component(s), so that the electrode (6) totally covers the first orifice. Electrically charged either conductive and/or non-conductive particles are provided by immersing the volume of the via-hole(s) (3) in a conductive medium (17) consisting of the electrically charged particles. An electric field is created between the first electrode (6) and a second electrode (4) through the via-hole(s) (3) and the conductive medium (17) and the electrically charged particles are precipitated on the inner surface of the first electrode (6) that is directed to the second orifice of the via-hole(s) (3), until a desired portion of the volume of the via-hole(s) (3) is filled with a first layer of the charged particles having a desired thickness. More layers may be created by repeating this process using additional electophoretic cell(s), until remaining portion of the volume of the via-hole(s) (3) is filled with the additional charged particles.
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5.发明授权WEAR AND THERMAL RESISTANT MATERIAL PRODUCED FROM SUPER HARD PARTICLES BOUND IN A MATRIX OF GLASSCERAMIC BY ELECTROPHORETIC DEPOSITION 有权磨损和耐热材料生产的FROM超硬颗粒通过电泳沉积作者陶瓷结合的矩阵
公开(公告)号：EP1305456B1
公开(公告)日：2004-09-15
申请号：EP01947768.6
申请日：2001-07-05
发明人： BRANDON, David , CHERNIAK, Liudmila
CPC分类号： C25D13/02 , C25D15/00 , Y10T428/31504
摘要： A substrate coated with a deposited composite comprising uniformly dispersed hard material particles in a glassceramic matrix. The deposited bulk composite may comprise uniformly dispersed hard material particles in a glassceramic matrix or hard material particles uniformly dispersed in a glassceramic matrix in a ratio of at least 20% by weight of glassceramic particles and at least 20% by weight of hard material; said mixture having a Vickers hardness of more than 2000 and up to 3000 kg/mm and demonstrates an extreme toughness, abrasive and wear resistance, high chemical inertness and a high cutting capability properties.
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6.发明公开METHOD OF ELECTROPHORETIC DEPOSITION OF CERAMIC BODIES FOR USE IN MANUFACTURING DENTAL APPLIANCES 有权电泳涂膜参与制造牙科产品陶瓷体的方法中使用
公开(公告)号：EP1073781A4
公开(公告)日：2003-01-08
申请号：EP99911422
申请日：1999-03-16
发明人： GAL-OR LEAH , GOLDNER RONI , CHERNIAK LIUDMILA , SEZIN NINA , LIUBOVICH SONIA
CPC分类号： A61C13/001 , A61C5/77 , A61C13/0022 , C25D1/14 , C25D13/02 , H05K1/0306 , H05K3/022
摘要： A method for electrophoretic deposition of ceramic particles as a green body shaped as a dental appliance, the method comprising the steps of (a) forming a suspension of the ceramic particles in a first polar solvent, the ceramic particles constituting at least about 5 % of the first suspension by weight; (b) passing a direct electrical current through the first suspension, using a deposition electrode (20) shaped as the dental appliance to form a green body; (c) coating the green body with glass particles; and (d) sintering the resultant coated body for obtaining a glass coated all-ceramic dental appliance.
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公开(公告)号：EP1818956A2
公开(公告)日：2007-08-15
申请号：EP06004253.8
申请日：2006-03-02
发明人： Thon, Assaf
IPC分类号： H01G9/052
CPC分类号： H01G9/052 , H01G9/0525
摘要： The invention is a high capacitance capacitor anode manufactured by creating a green anode body from particles of a dielectric oxide film-forming electrical conducting non-agglomerated powder, sintering the green anode body, and anodizing the sintered body. The non-agglomerated powder comprises fine particles having a small average particle size and a narrow size distribution, which gives the green anode body a morphology that allows it to be sintered at temperatures lower than 1200°C. The invention is also a method of manufacturing these anodes.
摘要翻译： 本发明是通过由电介质氧化膜形成导电非附聚粉末的颗粒形成绿色阳极体，烧结绿色阳极体并阳极氧化烧结体而制造的高容量电容器阳极。 非团聚粉末包含平均粒径小，分布狭窄的细小颗粒，使得阳极主体能够在低于1200℃的温度下烧结。 本发明也是制造这些阳极的方法。
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8.发明公开IMPROVED METHOD OF ELECTROPHORETIC DEPOSITION OF FERROELECTRIC FILMS USING A TRI-FUNCTIONAL ADDITIVE AND COMPOSITIONS FOR EFFECTING SAME 审中-公开改进方法电泳沉积FERRO电动MOVIES使用TRI-功能性添加剂和组合物对于这种应用
公开(公告)号：EP1259660A4
公开(公告)日：2006-09-13
申请号：EP00971675
申请日：2000-10-25
发明人： GAL-OR LEAH , GOLDNER RONI , SEZIN NINA , PISMANY ALA , BRANDON DAVID
CPC分类号： C25D13/02 , H01L41/317 , H01L41/43
摘要： An improved method for depositing ferroelectric particles on a surface of a substrate to form films or stand-alone bodies. The improvement is based on electrophoretic deposition (EPD) of ferroelectric films by using a tri-functional phosphate ester additive having a concentration less than 10 volume percent in the EPD suspension, without the need for addition of a binder. The method includes preparation of the suspension by washing and dispersing ferroelectric particles, for example, commercially available PZT powder, in a polar solvent such as ethanol, followed by addition of the phosphate ester additive to the suspension, and an ultrasound treatment. The suspension is used in EPD of the ferroelectric particles on a prepared substrate. Following EPD, the green film is dried and sintered at high temperature. Visual and physical examination of stand alone and patterned PZT deposited films show excellent quality obtained in manufacturing a diversity of piezoelectric products, featuring exceptionally high green film uniformity, thickness distribution, and reproducibility to within ± 2 microns for 20 micrometer film thickness. The phosphate ester additive functions by improving stabilization and control of suspension characteristics and properties during the electrophoretic migration process, and by improving desired dimensions, characteristics, and electrical properties of the deposited green film. Thin or thick ferroelectric films, either as stand alone products, or formed on geometrically demanding patterned or non-patterned substrates are produced by using the method. The improved method is applicable to different ferroelectric particulate materials and to different substrates used for manufacturing piezoelectric elements and devices, in a cost effective manner.
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9.发明授权METHOD OF ELECTROPHORETIC DEPOSITION OF CERAMIC BODIES FOR USE IN MANUFACTURING DENTAL APPLIANCES 有权电泳涂膜参与制造牙科产品陶瓷体的方法中使用
公开(公告)号：EP1073781B1
公开(公告)日：2005-06-08
申请号：EP99911422.6
申请日：1999-03-16
CPC分类号： A61C13/001 , A61C5/77 , A61C13/0022 , C25D1/14 , C25D13/02 , H05K1/0306 , H05K3/022
摘要： A method for electrophoretic deposition of ceramic particles as a green body shaped as a dental appliance, the method comprising the steps of (a) forming a suspension of the ceramic particles in a first polar solvent, the ceramic particles constituting at least about 5 % of the first suspension by weight; (b) passing a direct electrical current through the first suspension, using a deposition electrode (20) shaped as the dental appliance to form a green body; (c) coating the green body with glass particles; and (d) sintering the resultant coated body for obtaining a glass coated all-ceramic dental appliance.
摘要翻译： 一种用于陶瓷粒子的电泳沉积，成形为牙科器具生坯的方法，该方法包括以下步骤：（a）在第一极性溶剂中形成的悬浮液的陶瓷颗粒的，该陶瓷颗粒构成至少约5％的 第一悬浮液（重量）; （B）使直流电流通过所述第一悬浮液中，使用成形为牙科器具以形成生坯的沉积电极（20）; （C）涂覆生坯玻璃颗粒; 和（d）烧结所得涂装体，用于获得涂覆全瓷牙科器具的玻璃。
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公开(公告)号：EP1399937A1
公开(公告)日：2004-03-24
申请号：EP02738584.8
申请日：2002-06-13
IPC分类号： H01G9/052
CPC分类号： H01G9/052
摘要： AbstractThe present invention provides a process for manufacturing a porous metal electrode, wherein the porosity degree is in the range of 30 to 50% and the metal is capable of forming a stable, uniform, oxide layer having a dielectric constant equal to or greater than 20 (ε ≥ 20), preferably selected from the group consisting of tantalum and niobium, comprising a substantially uniform porous layer of deposited said metal particles thereon. The present invention further relates to a stable suspension for electrophoretically homogeneously deposition of said metal.
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