摘要:
A chloroalkene production method comprising the steps of: carrying out the dehydrochlorination reaction of a chloroalkane in the presence of a Lewis acid catalyst containing a metal chloride to produce a chloroalkene; removing a metal component derived from the catalyst from the obtained reaction solution; and distilling the reaction solution to obtain the purified chloroalkene.
摘要:
The invention intends to provide a method for preventing deterioration in quality of the primer layer resulting from spinning-off and reattachment of a primer liquid on forming a polyurethane primer layer on a substrate for an eyeglass lens or the like using a coating composition containing a moisture-curing polyurethane resin. The method for producing a laminate according to the present invention comprises performing spin-coating while a spin-coating apparatus is forcefully evacuated through the side wall and/or the bottom thereof, on producing a laminate by spin-coating the surface of a substrate with a coating composition containing a moisture-curing polyurethane resin. More preferably, the spin-coating apparatus comprises a top cover, a lower chamber, and a rotatable substrate supporting device installed in the lower chamber; exhaust ports are provided in the top cover and at the bottom of the lower chamber; and the substrate supporting device is housed in a cylinder member wherein the aperture of at the lower end is larger than the aperture at the upper end.
摘要:
[Problem] To provide a production device whereby, after crushing polycrystalline silicon blocks, contaminating fine powders, such as a fine metal powder and fine silicon powder, can be efficiently removed by blowing a gas stream thereto. [Solution] A device for producing a cleaned crushed product of polycrystalline silicon blocks, said device being provided with: a) a conveying belt conveyer for a crushed product of polycrystalline silicon blocks, said conveying belt preferably being mesh-like; b) a gas stream-injector for blowing away fine powders mixed in the crushed product of polycrystalline silicon blocks, said injector being placed above a travel surface of the conveying belt of the conveying belt conveyer; and c) a mesh for preventing scattering of the crushed product of polycrystalline silicon blocks, said mesh being placed between the travel surface of the mesh-like conveying belt and the gas stream-injector for blowing away fine powders that is provided above the travel surface.
摘要:
To provide a photopolymerization device which can prevent sealability deterioration of a workpiece accomodation chamber, accomodating the workpiece, due to repeated operations. Provided is a photopolymerization device including: base 16 to which shaft insertion hole 16a is formed; workpiece retaining and rotating shaft section 20 which passes through the shaft insertion hole, relatively moves in an axial direction to the base, is rotatable about the axis, and holds workpiece W at an end part of the section; cover member 30 which has an opening 35 closable by the base and forms workpiece accomodation chamber R, accomodating the workpiece, by contacting the base with a peripheral part 36 of the opening; light irradiation device 40, which irradiates light to the workpiece placed in the workpiece accomodation chamber; and controller 60 which controls relative movement of the base and the cover member, relative movement of the base and the workpiece retaining and rotating shaft section in the axial direction, rotation of the workpiece retaining and rotating shaft section, and light irradiation of the light irradiation device, wherein the controller controls formation of the workpiece accomodation chamber by contacting the base with the peripheral part and rotation of the workpiece in a first region (R1) of the workpiece accomodation chamber, subsequently, the workpiece placement in a second region (R2), closer to the light irradiation device than the first region, by relative movement of the workpiece retaining and rotating shaft section to the base, and light irradiation toward the workpiece placed in the second region by the light irradiation device.