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    PROBE AND PRIMER FOR TUBERCLE BACILLUS DETECTION, AND METHOD OF DETECTING HUMAN TUBERCLE BACILLUS THEREWITH
    45.
    发明公开
    PROBE AND PRIMER FOR TUBERCLE BACILLUS DETECTION, AND METHOD OF DETECTING HUMAN TUBERCLE BACILLUS THEREWITH 有权
    探针和引物FOR结核杆菌用于检测人，这样检测和方法

    公开(公告)号：EP1746156A4

    公开(公告)日：2008-08-20

    申请号：EP05734679

    申请日：2005-04-22

    申请人： WAKO PURE CHEM IND LTD

    发明人： ISHIKAWA TOMOKAZU

    IPC分类号： C12Q1/68 ,  C12N15/09 ,  G01N33/53 ,  G01N33/569

    CPC分类号： C12Q1/689 ,  C12Q2600/16 ,  Y10S435/975

    摘要： Novel probe and primer for tubercle bacillus detection capable of avoiding diagnostic false positive; and a simple and easy, rapid, high-precision method of detecting human tubercle bacillus with the use thereof. There is provided an oligonucleotide comprising a part or the entirety of a nucleic acid sequence of SEQ ID NO: 1, SEQ ID NO: 2, SEQ ID NO: 3, SEQ ID NO: 4, SEQ ID NO: 5, SEQ ID NO: 6, SEQ ID NO: 7 or SEQ ID NO: 8 or comprising a part or the entirety of a sequence complementary thereto, which oligonucleotide is capable of hybridization with the nucleic acid sequence of IS6110 gene of human tubercle bacillus. Further, there are provided a probe and primer for tubercle bacillus detection, comprising the oligonucleotide. Still further, there is provided a method of detecting human tubercle bacillus, characterized in that use is made of the above probe and primer.

    METHOD FOR DEUTERATING HALOACRYLIC ACID OR ITS SALT
    46.
    发明公开
    METHOD FOR DEUTERATING HALOACRYLIC ACID OR ITS SALT 审中-公开
    卤素氘化丙烯酸或盐的方法

    公开(公告)号：EP1760064A4

    公开(公告)日：2008-03-05

    申请号：EP05750962

    申请日：2005-06-20

    申请人： WAKO PURE CHEM IND LTD

    发明人： MAESAWA TSUNEAKI ,  ITO NOBUHIRO ,  HIROTA KOSAKU ,  SAJIKI HIRONAO

    IPC分类号： C07C51/347 ,  C07B59/00 ,  C07B61/00 ,  C07C57/54

    CPC分类号： C07B59/001 ,  C07B2200/05 ,  C07C51/347 ,  C07C57/54

    摘要： This invention provides a method for deuterating a haloacrylic acid or its salt with high efficiency on a commercial scale. The method is characterized in that a compound represented by general formula [1] wherein R1 and R2 each independently represent a light hydrogen atom or a heavy hydrogen atom, and at least one of R1 and R2 represents a light hydrogen atom; R3 represents a light hydrogen atom, a heavy hydrogen atom, an alkali metal atom, or an alkaline earth metal atom; X represents a halogen atom; and n represents 1 or 2, is reacted with a heavy hydrogen source in the co-presence of a catalyst selected from palladium catalysts, platinum catalysts, rhodium catalysts, ruthenium catalysts, nickel catalysts, and cobalt catalysts not subjected to activation treatment. The deuterated compound is represented by general formula [2] wherein R4 and R5 each independently represent a light hydrogen atom or a heavy hydrogen atom, and at least one of R4 and R5 represents a heavy hydrogen atom; R3 represents a light hydrogen atom, a heavy hydrogen atom, an alkali metal atom, or an alkaline earth metal atom; X represents a halogen atom; and n represents 1 or 2.

    PROCESS FOR PRODUCING TRIARYLSULFONIUM SALT
    47.
    发明公开
    PROCESS FOR PRODUCING TRIARYLSULFONIUM SALT 有权
    用于生产三芳基

    公开(公告)号：EP1676835A4

    公开(公告)日：2007-01-17

    申请号：EP04792015

    申请日：2004-10-04

    申请人： WAKO PURE CHEM IND LTD

    发明人： SUMINO MOTOSHIGE ,  FUKASAWA KAZUHITO ,  IMAZEKI SHIGEAKI ,  WATANABE TETSUYA

    IPC分类号： C07C381/12

    CPC分类号： C07C381/12

    摘要： A process by which a triarylsulfonium salt in which only one aromatic ring differs from the others can be efficiently produced. The process, which is for producing a triarylsulfonium salt represented by the general formula [4]: (wherein R represents aryl optionally having a substituent different from R ; and A1 represents a strong-acid residue), is characterized by reacting a diaryl sulfoxide represented by the general formula [1]: with an aryl-Grignard reagent represented by the general formula [2]: RMgX (wherein X represents halogeno) in the presence of an activator having a high affinity for oxygen, the activator being used in an amount of 3 to 7.5 equivalents to the diaryl sulfoxide, and then reacting the reaction product with either a strong acid represented by the general formula [3]: HA1 or a salt of the acid.

    SULFONIUM SALT COMPOUND
    48.
    发明公开
    SULFONIUM SALT COMPOUND 有权
    SULPHONIUMSALZ-VERBINDUNG

    公开(公告)号：EP1314725A4

    公开(公告)日：2005-06-29

    申请号：EP01945637

    申请日：2001-06-27

    申请人： WAKO PURE CHEM IND LTD

    发明人： ISHIHARA MASAMI ,  SUMINO MOTOSHIGE ,  FUKASAWA KAZUHITO ,  KATANO NAOKI ,  IMAZEKI SHIGEAKI

    IPC分类号： C07C53/21 ,  C07C381/12 ,  G03F7/004 ,  G03F7/038 ,  G03F7/039 ,  C07C321/30 ,  C07C53/15 ,  C07C67/30 ,  C08K5/36 ,  C08K5/41 ,  C08L25/18 ,  G03F7/029

    CPC分类号： C07C53/21 ,  C07C381/12 ,  G03F7/0045 ,  G03F7/0382 ,  G03F7/0392

    摘要： A compound represented by the general formula [1] [1] (wherein R , R , and R each independently represents a residue of an aromatic hydrocarbon; Y represents an anion derived from a fluorinated carboxylic acid having three or more carbon atoms; and n is 1 or 2, provided that R , R , and R each is not a phenyl group having a substituent in an ortho and/or a meta position); and a composition comprising the compound and a diazodisulfone compound. Use of the compound or the composition as an acid generator for resists produces the effect of improving the profiles of ultrafine patterns or diminishing side wall irregularities in ultrafine patterns. The compound is also useful as a cationic photopolymerization initiator.

    摘要翻译： 由通式[1] [1]表示的化合物（其中R 1，R 2和R 3各自独立地表示芳族烃的残基; Y表示由氟化羧酸衍生的阴离子 具有三个或更多个碳原子;并且n是1或2，条件是R 1，R 2和R 3各自不是在邻位和/或间位具有取代基的苯基） ; 以及包含该化合物和重氮二砜化合物的组合物。 使用该化合物或该组合物作为抗酸剂的酸产生剂产生改善超细图案的轮廓或减小超细图案中的侧壁不规则的效果。 该化合物也可用作阳离子光聚合引发剂。