Method of decomposing thermosetting resin, apparatus and heat control program
    43.
    发明公开
    Method of decomposing thermosetting resin, apparatus and heat control program 有权
    韦尔法罕zur Zersetzung eineshitzehärtbarenHarzes,Vorrichtung undWärmesteuerprogramm

    公开(公告)号:EP1193286A1

    公开(公告)日:2002-04-03

    申请号:EP01307709.4

    申请日:2001-09-11

    IPC分类号: C08J11/24 C08J11/28

    摘要: Disclosed is a method of decomposing a thermosetting resin by a decomposer. This method comprising the steps of pre-heating the thermosetting resin up to a pre-heating temperature T0, kneading the pre-heated thermosetting resin together with a decomposer, and concurrently heating a mixture comprising the thermosetting resin and the decomposer up to a kneading temperature T1, thereby allowing a reaction to take place between the decomposer and the thermosetting resin to obtain a kneaded matter wherein the decomposer has been consumed, and heating the kneaded matter to a maximum temperature T2 to thereby decompose the thermosetting resin, wherein the pre-heating temperature T0 is not higher than the boiling temperature of the decomposer, the kneading temperature T1 is not lower than the pre-heating temperature T0 but is lower than the thermal decomposition temperature of the thermosetting resin, the maximum temperature T2 is lower than the decomposition temperature of the thermosetting resin, and the pre-heating of the thermosetting resin is performed under the following conditions of temperature T0 and time t: 100°C ≦ T0 0.5 min ≦ t ≦ 7 min.

    摘要翻译: 公开了通过分解器分解热固性树脂的方法。 该方法包括以下步骤:将热固性树脂预热至预热温度T0,将预热的热固性树脂与分解器一起捏合,同时将包含热固性树脂和分解剂的混合物加热至捏合温度 T1,从而使分解器和热固性树脂之间发生反应,得到分解器已被消耗的捏合物,并将捏合物加热到最高温度T2,从而分解热固性树脂,其中预热 温度T0不高于分解器的沸腾温度,捏合温度T1不低于预热温度T0但低于热固性树脂的热分解温度,最高温度T2低于分解温度 的热固性树脂,并且在该热固性树脂的预热下进行 温度T0和时间t的以下条件:<100℃ 0.5分钟

    Method of decomposing a polyurethane
    46.
    发明公开
    Method of decomposing a polyurethane 审中-公开
    Verfahren zur Zersetzung eines Polyurethans

    公开(公告)号:EP1142945A2

    公开(公告)日:2001-10-10

    申请号:EP01107988.6

    申请日:2001-03-29

    IPC分类号: C08J11/28

    摘要: A method of recovering a decomposition product from a polyurethane, the method comprising the steps of thermally decomposing a polyurethane into a liquid containing a polyol and a urea compound which is soluble in the polyol, and solids containing a urea compound which is insoluble in the liquid in the presence of a polyamine compound at a temperature of 120 to 250°C; removing the solids; hydrolyzing the residue with water retained at a high temperature of 200 to 320°C and a high pressure; and recovering the resulting polyamine and/or polyol.

    摘要翻译: 一种从聚氨酯中回收分解产物的方法,该方法包括以下步骤:将聚氨酯热分解成含有可溶于多元醇的多元醇和脲化合物的液体,以及含有不溶于液体的尿素化合物的固体 在多胺化合物存在下,在120〜250℃的温度下, 去除固体; 用保持在200〜320℃的高温和高压的水进行水解; 并回收得到的多胺和/或多元醇。

    Apparatus for decomposition and recovery of polyurethane resin
    50.
    发明公开
    Apparatus for decomposition and recovery of polyurethane resin 有权
    Vorrichtung zur Zersetzung undRückgewinnungvon Polyurethanharz

    公开(公告)号:EP1006143A1

    公开(公告)日:2000-06-07

    申请号:EP99119083.6

    申请日:1999-10-01

    IPC分类号: C08J11/28 C08J11/14

    摘要: Disclosed is an apparatus for decomposing a polyurethane resin and recovering the decomposed polyurethane resin as a polyamine compound and a polyol compound, said apparatus including: a fluidizer that fluidizes the polyurethane resin as a target compound of hydrolysis decomposition; a reactor that hydrolyzes the fluidized target compound of decomposition with either one of supercritical water and high-temperature high-pressure water to a decomposition product mixture; a water supplier that feeds either one of supercritical water and high-temperature high-pressure water to the reactor; and a post-processor that causes the decomposition product mixture discharged from the reactor to be subjected to a post treatment procedure, such as dehydration, addition, distillation, separation, and liquid separation to recover the polyamine compound and/or the polyol compound.
    According to the present invention, there can be provided an apparatus of decomposition and recovery that continuously decomposes and recovers polyurethane resin with high-temperature high-pressure water or supercritical water, which advantageously reduces the required energy cost, reduces the size of the whole apparatus, removes foreign substances from the shredder dust, and decreases the required quantities of substances for decomposition.

    摘要翻译: 公开了一种用于分解聚氨酯树脂并回收作为多胺化合物和多元醇化合物的分解的聚氨酯树脂的装置,所述装置包括:使作为水解分解的目标化合物的聚氨酯树脂流化的流化剂; 使用超临界水和高温高压水中的任一种水解分解产物混合物的流化目标化合物的反应器; 将超临界水和高温高压水中的一种供给反应堆的供水者; 以及将从反应器排出的分解产物混合物进行脱水,添加,蒸馏,分离和液体分离等后处理程序的后处理器,以回收多胺化合物和/或多元醇化合物。 根据本发明,可以提供一种分解和回收装置,其使用高温高压水或超临界水连续分解和回收聚氨酯树脂,这有利于降低所需的能量成本,减小整个装置的尺寸 从粉碎机中除去异物,减少分解物质所需的量。