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    Process for the recovery of spent fluorinated sulphonic acid catalyst in an alkylation process
    52.
    发明公开
    Process for the recovery of spent fluorinated sulphonic acid catalyst in an alkylation process 失效
    Verfahren zurRückgewinnungverbrauchter fluorierterSulfansäure-Katalysatorenfürein Alkylierungsverfahren。

    公开(公告)号：EP0614699A1

    公开(公告)日：1994-09-14

    申请号：EP94103027.2

    申请日：1994-03-01

    申请人： Haldor Topsoe A/S

    发明人： Hommeltoft, Sven Ivar

    IPC分类号： B01J38/60 ,  B01J27/30 ,  C07C2/62

    CPC分类号： B01J31/4092 ,  B01J31/0227 ,  B01J31/0258 ,  B01J38/60 ,  B01J2231/4205 ,  C07C2/62 ,  C07C2531/025 ,  Y02P20/584

    摘要： Process for the recovery of fluorinated sulphonic acid catalyst from tar being formed during alkylation of hydrocarbons in the presence of the fluorinated sulphonic acid catalyst and containing spent fluorinated sulphonic acid catalyst in form of salts with basic components in the tar, which process comprises,
       treating the tar with a proton donating acid by mixing of the acid and the tar, thereby, converting the spent catalyst to the fluorinated sulphonic acid;
       separating the obtained fluorinated sulphonic acid from the tar-acid mixture by stripping off the acid from the mixture with an inert stripping agent at a temperature of 0-200 o C and pressure of 0.001-1 atm; and finally
       recovering the separated fluorinated sulphonic acid from the stripping agent.

    摘要翻译： 用于在氟化磺酸催化剂存在下烃的烷基化期间形成的焦油中回收氟化磺酸催化剂的方法，并含有与焦油中的碱性组分形成的盐形式的废氟化磺酸催化剂，该方法包括处理 通过混合酸和焦油，通过质子供体酸的焦油，从而将废催化剂转化为氟化磺酸; 通过用惰性汽提剂在0-200℃的温度和0.001-1atm的压力下从混合物中除去酸从所述焦油酸混合物中分离得到的氟化磺酸; 并最终从剥离剂中回收分离的氟化磺酸。

    Process for preparing alkylbenzene
    55.
    发明公开
    Process for preparing alkylbenzene 失效
    Verfahren zur Herstellung von烷基苯。

    公开(公告)号：EP0520975A2

    公开(公告)日：1992-12-30

    申请号：EP92870094.7

    申请日：1992-06-26

    申请人： HUNTSMAN SPECIALTY CHEMICALS CORPORATION

    发明人： Dyroff, David Ray ,  Anantaneni, Prakasa Rao

    IPC分类号： C07C2/62 ,  C07C7/148 ,  C07C2/70 ,  C07C7/12

    CPC分类号： C07C15/107 ,  C07C7/148 ,  Y02P20/582

    摘要： There is disclosed an improved process for the production of linear alkylbenzene wherein monoolefins are reacted with benzene in a hydrogen fluoride catalyzed reaction followed by recovery of the alkylbenzene. An alumina treatment step is included which removes organic fluoride impurities in order to prevent release of hydrofluoric acid in downstream equipment. It has been discovered that the SO₃ sulfonation color of the alkylbenzene is surprisingly improved by the use of a high selectivity basic alumina for this treatment.

    摘要翻译： 公开了一种生产线性烷基苯的改进方法，其中单烯烃在氟化氢催化反应中与苯反应，然后回收烷基苯。 包括氧化铝处理步骤，其除去有机氟化物杂质以防止下游设备中氢氟酸的释放。 已经发现，通过在该处理中使用高选择性碱性氧化铝，烷基苯的SO 3磺化颜色出人意料地得到改善。

    ACID CATALYZED PROCESS.
    58.
    发明公开
    ACID CATALYZED PROCESS. 失效
    酸催化法。

    公开(公告)号：EP0324787A4

    公开(公告)日：1989-08-30

    申请号：EP87906886

    申请日：1987-09-28

    申请人： NELSON RES & DEV COMPANY

    发明人： MINASKANIAN GEVORK ,  PECK JAMES V

    IPC分类号： B01J31/02 ,  C07B61/00 ,  C07C1/24 ,  C07C2/62 ,  C07C2/86 ,  C07C5/27 ,  C07C5/29 ,  C07C9/00 ,  C07C11/09 ,  C07C27/12 ,  C07C43/04 ,  C07C45/45 ,  C07C49/20 ,  C07C49/76 ,  C07C67/04 ,  C07C67/08 ,  C07C69/14

    CPC分类号： C07C5/2791 ,  C07C1/24 ,  C07C67/04 ,  C07C2531/02 ,  C07C9/00 ,  C07C69/14

    摘要： Improved process for the acid-catalyzed conversion of a reactant into a reaction product wherein the improvement comprises contacting said reactant with an acid catalyst represented by general formula (I), wherein X is selected from the group consisting of oxygen, sulfur or represents 2 hydrogen atoms; Z is selected from the group consisting of the anions of strong acids, e.g. chloride, bromide, bisulfate, nitrate or dihydrogen phosphate; R1 is hydrogen or a lower alkyl having one to four carbon atoms; R is hydrogen or a methyl radical; m is an integer of from 2 to 6; n is 0 or 1; and o is 0 or an integer of from 1 to 17, at reaction conditions, and recovering a reaction product. Reactants which may be converted into reaction products in the process of this invention include hydrocarbons and heteroatom-substituted hydrocarbons, wherein said heteroatoms may be selected from the group consisting of nitrogen, oxygen, sulfur, phosphorus and halogen atoms. For example, in the present inventive process, olefins may be reacted with tertiary alkanes to provide alkylated products; olefins may be reacted with carboxylic acids to obtain esters; alcohols may be dehydrated to obtain olefins or ethers or reacted with carboxylic acid to obtain an alkylated product or an ester, respectively; anhydrides may be reacted with an aromatic or an olefinic compound to obtain acetylated derivatives thereof; epoxides may be reacted to the corresponding glycols, etc.

    Apparatus and method for controlling an alkylation reactor
    59.
    发明公开
    Apparatus and method for controlling an alkylation reactor 失效
    装置和用于控制烷基化反应器的方法。

    公开(公告)号：EP0088427A1

    公开(公告)日：1983-09-14

    申请号：EP83102262.9

    申请日：1983-03-08

    申请人： PHILLIPS PETROLEUM COMPANY

    发明人： Funk, Gary Lloyd ,  Feldman, James Arthur

    IPC分类号： C07C2/62 ,  G05D11/02

    CPC分类号： C07C2/62 ,  B01J19/0006

    摘要： An acid alkylation process is controlled so as to maintain a desired ratio of isobutane to olefins in a fluid stream flowing to the alkylation reactor and to maintain a desired acid to hydrocarbon ratio in the alkylation reactor. Also, if parallel alkylation reactors are utilized, the flow rate of the olefin stream to one of the alkylation reactors is manipulated so as to maintain a balanced loading on the parallel alkylation reactors. Such control results in improved quality of the alkylate produced and also improves the amount of alkylate produced from a particular amount of fluid to the alkylation reactor.