公开(公告)号：EP2690079B1

公开(公告)日：2016-03-09

申请号：EP11861829.7

申请日：2011-03-23

申请人： M Technique Co., Ltd.

发明人： KURAKI Jun ,  MAEKAWA Masaki ,  HONDA Daisuke ,  ENOMURA Masakazu

IPC分类号： B01F5/06 ,  B01J19/00 ,  C01B33/193 ,  C01F7/02 ,  C01G9/02 ,  C01G23/04

CPC分类号： C01B33/113 ,  B01F7/00775 ,  B01F7/00791 ,  B01J14/00 ,  B01J19/1887 ,  C01B9/00 ,  C01B13/14 ,  C01B13/16 ,  C01B13/36 ,  C01B19/00 ,  C01B21/00 ,  C01B32/00 ,  C01B33/00 ,  C01B33/193 ,  C01B35/00 ,  C01G9/02 ,  C01G23/003 ,  C01P2002/72 ,  C01P2004/04 ,  C04B35/62625 ,  C04B2235/3284 ,  C04B2235/3418 ,  C04B2235/5445 ,  C04B2235/5454 ,  C04B2235/76

公开(公告)号：EP2418015B1

公开(公告)日：2016-01-06

申请号：EP08878387.3

申请日：2008-11-25

申请人： M. Technique Co., Ltd.

发明人： ENOMURA, Masakazu

IPC分类号： B01J19/00 ,  B01F3/08 ,  B01F7/26

CPC分类号： B01J19/1887 ,  B01F7/00775 ,  B01F7/00791 ,  B01J19/0093 ,  B01J2219/00788 ,  B01J2219/00873 ,  B01J2219/00889

公开(公告)号：EP2781610A1

公开(公告)日：2014-09-24

申请号：EP12849152.9

申请日：2012-08-16

申请人： M Technique Co., Ltd.

发明人： MAEKAWA Masaki ,  HONDA Daisuke ,  ENOMURA Masakazu

IPC分类号： C22C5/08 ,  B22F1/00 ,  B22F9/24 ,  C22C9/00

CPC分类号： C22C9/00 ,  B22F1/0018 ,  B22F9/24 ,  B82Y30/00

摘要： The present invention addresses the problem of providing a novel, solid silver-copper alloy. Provided is a solid silver-copper alloy in which the concentration of copper contained in the silver-copper alloy is 0.1 - 99.94 wt%, and which has, as the principal constituent thereof, a non-eutectic structure which does not contain a eutectic when the solid silver-copper alloy is at room temperature. This silver-copper alloy can be produced by mixing a fluid containing silver ions and copper ions with a fluid containing a reducing agent, and separating silver-copper alloy particles therefrom. It is preferable to mix the fluid containing the silver ions and copper ions with the fluid containing the reducing agent in a thin-film fluid formed between processing surfaces arranged so as to face one another, capable of approaching toward and separating from one another, and capable of having at least one surface rotate relative to the other. The diameter of the particles of the silver-copper alloy is preferably 50nm or less. This solid silver-metal alloy may also be a solid alloy comprising one or more types of other metals in addition to silver and copper.

公开(公告)号：EP2687306A1

公开(公告)日：2014-01-22

申请号：EP11861223.3

申请日：2011-03-14

申请人： M Technique Co., Ltd.

发明人： ENOMURA Masakazu

IPC分类号： B22F9/24

CPC分类号： B22F9/24 ,  B22F2301/15 ,  B22F2301/255 ,  B22F2301/30

摘要： Provided is a producing method for metal microparticles for which the particle diameter is controlled. At least two types of fluids to be processed are used, and at least one of those fluids to be processed is a metallic solution characterized in that a metal and/ or metallic compound is dissolved in a solvent. Of the fluids to be processed other than the above, at least one is a reducing agent fluid that includes a reducing agent. The fluids to be processed are mixed in a thin film fluid created between at least two processing surfaces (1, 2) which are disposed to face each other and can be brought closer or separated, at least one face rotating relative to the other, and metal microparticles for which the particle diameter is controlled are precipitated out. At that time, the particle diameter of the metal microparticles is controlled by varying particular conditions for at least one of the metallic solution and the reducing agent fluid introduced between the processing surfaces (1, 2) . The particular conditions are at least one type selected from a set comprising the introduction rate for the metallic solution and/ or reducing agent fluid and the pH of the metallic solution and/ or the reducing agent fluid.

公开(公告)号：EP2644659A1

公开(公告)日：2013-10-02

申请号：EP11843349.9

申请日：2011-11-22

申请人： M Technique Co., Ltd.

发明人： MAEKAWA Masaki ,  HONDA Daisuke ,  ENOMURA Masakazu

IPC分类号： C09B67/02 ,  B82Y30/00 ,  C09B67/12 ,  C09B67/20 ,  C09B67/22 ,  C09B67/42

CPC分类号： C07F3/06 ,  B01D11/0269 ,  B01F3/0861 ,  B82Y30/00 ,  C01P2004/64 ,  C01P2004/82 ,  C07F1/08 ,  C09B67/0017 ,  C09B67/0019 ,  C09B67/0026 ,  C09B67/0035 ,  C09B67/0092 ,  C09C1/0081 ,  C09C1/04 ,  C09C1/627

摘要： The problem addressed by the present invention is to provide a high heat-resistant phthalocyanine. The phthalocyanine is separated by mixing a phthalocyanine separation solvent and a phthalocyanine solution characterized in that a phthalocyanine starting material is dissolved in a solvent. The phthalocyanine is characterized by having high heat resistance, the decomposition temperature of the separated phthalocyanine being at least 10°C higher than the decomposition temperature of the phthalocyanine starting material. Also, the phthalocyanine solution may be the result of dissolving at least two types of phthalocyanine starting material in the solvent, the separated phthalocyanine being characterized by containing a solid solvent of the at least two types of phthalocyanine starting material and by the decomposition temperature of the separated phthalocyanine being at least 10°C higher than the decomposition temperature of a mixture of at least two types of phthalocyanine separated by mixing the phthalocyanine separation solvent and each of at least two types of phthalocyanine solution resulting from dissolving each of the at least two types of phthalocyanine starting material in a solvent.

公开(公告)号：EP2644658A1

公开(公告)日：2013-10-02

申请号：EP11843150.1

申请日：2011-05-20

申请人： M Technique Co., Ltd.

发明人： MAEKAWA Masaki ,  ARAKI Kaeko ,  OKA Hideyuki ,  HONDA Daisuke ,  ENOMURA Masakazu

IPC分类号： C09B67/02 ,  B82B3/00 ,  C09B67/12 ,  C09B67/22 ,  C09B67/42

CPC分类号： C07F3/06 ,  B01D11/0269 ,  B01F3/0861 ,  B82Y30/00 ,  C01P2004/64 ,  C01P2004/82 ,  C07F1/08 ,  C09B67/0017 ,  C09B67/0019 ,  C09B67/0026 ,  C09B67/0035 ,  C09B67/0092 ,  C09C1/0081 ,  C09C1/04 ,  C09C1/627

摘要： The problem addressed by the present invention is to provide; solid solution pigment nanoparticles having a homogeneous solid solution ratio; a method for producing solid solution pigment nanoparticles having a homogeneous solid solution ratio in each primary particle; and a method for controlling the solid solution ratio of solid solution pigment nanoparticles. The solid solution pigment nanoparticles are prepared by precipitating at least two types of pigment by mixing a pigment precipitation solvent and; at least one type of pigment solution characterized in that at least two types of pigment are dissolved in a solvent: or at least two types of pigment solution characterized in that at least one type of pigment is dissolved in a solvent. The solid solution pigment nanoparticles are characterized in that the solid solution ratio of the at least two types of pigment in the primary particles of the precipitated solid solution pigment nanoparticles with respect to the ratio of the at least two types of pigment in the pigment solution mixed with the pigment precipitation solvent having a precision within 25%.

摘要翻译： 由本发明所解决的问题是提供; 具有均匀固溶体比固溶体颜料纳米粒子; 用于生产具有在各初级粒子的均匀固溶体比固溶体颜料纳米粒子的方法; 以及用于控制固体溶液颜料纳米粒子的固溶体比率的方法。 固溶体颜料纳米粒子通过通过混合颜料沉淀和溶剂沉淀至少两种类型的颜料的制备 其特征在于至少一种类型的颜料溶液做了至少两种类型的颜料在溶剂中溶解：或至少两种类型的颜料溶液中为特征的那样至少一种类型的颜料在溶剂中溶解。 将固体溶液颜料纳米粒子的特征在于的确在沉淀的固体溶液颜料纳米粒子的一次粒子的至少两种类型的颜料的固体溶液比相对于所述至少两种类型的颜料中的在色素溶液混合比率 用具有25％之内的精确度的色素沉淀的溶剂。

公开(公告)号：EP2428536A1

公开(公告)日：2012-03-14

申请号：EP09841154.9

申请日：2009-11-10

申请人： M. Technique Co., Ltd.

发明人： ENOMURA, Masakazu

IPC分类号： C09B67/02 ,  C09B67/46

CPC分类号： C09B67/0091 ,  B01F7/00791 ,  C09B67/0019 ,  C09B67/0022 ,  C09B67/0096 ,  C09B68/4253

摘要： The surface of fine pigment particles is efficiently treated using low energy without causing a cost increase. Provided is a method of treating the surface of fine pigment particles, characterized by maintaining a small gap of 1 mm or narrower between two treating surfaces which are able to get close to and apart from each other and relatively rotate and using the gap between the two treating surfaces which is kept so narrow, as a passage for a fluid to be treated, thereby forming a thin film of the fluid to be treated (forced thin film) . Fine pigment particles are formed in this thin-film fluid (forced thin film) . The method is further characterized by modifying the surface of the formed fine pigment particles within the thin-film fluid (forced thin film).

摘要翻译： 使用低能量有效地处理细颜料颗粒的表面而不会导致成本增加。 提供了一种处理细颜料颗粒表面的方法，其特征在于在两个处理表面之间保持1mm或更窄的小间隙，这两个处理表面之间能够彼此接近和分离并相对旋转，并且使用两者之间的间隙 处理保持如此窄的表面作为待处理流体的通道，由此形成待处理流体的薄膜（强制薄膜）。 在这种薄膜流体（强制薄膜）中形成细颜料颗粒。 该方法的特征还在于通过改变薄膜流体（强制薄膜）内形成的细颜料颗粒的表面。

公开(公告)号：EP2204351A1

公开(公告)日：2010-07-07

申请号：EP08831235.0

申请日：2008-09-11

申请人： M Technique Co., Ltd.

发明人： ENOMURA, Masakazu

IPC分类号： C01G23/053 ,  B01D9/02 ,  B01F3/08 ,  B01F17/52 ,  B01J19/00 ,  C09C1/36 ,  C09C3/04 ,  C09C3/06 ,  C09C3/08 ,  C09C3/10 ,  C09D17/00

CPC分类号： B01F5/221 ,  B01F3/12 ,  B01F7/00775 ,  B01F7/00791 ,  B01J19/10 ,  B01J19/123 ,  B01J19/1887 ,  B01J2219/00094 ,  B01J2219/00137 ,  B82Y30/00 ,  C01G23/053 ,  C01G23/0532 ,  C01G23/0536 ,  C01P2004/64 ,  C08K3/22 ,  C09C1/3676 ,  C09D5/00 ,  C09D7/61 ,  C09D7/67 ,  C09D7/68 ,  C09D17/008

摘要： It is an object to provide a method for producing titanium dioxide superfine particles, which produces monodispersed titanium dioxide superfine particles depending on its purpose, causes no clogging with a product due to self-dischargeability, requires no great pressure, and is excellent in productivity. In the method for producing titanium dioxide superfine particles in a fluid containing a titanium compound by separation, the fluid is formed into a thin film fluid between two processing surfaces arranged so as to be able to approach to and separate from each other, at least one of which rotates relative to the other, and the titanium dioxide superfine particles are separated in the thin film fluid.

摘要翻译： 本发明的目的是提供一种二氧化钛超细颗粒的制造方法，其根据其目的产生单分散的二氧化钛超细颗粒，不会由于自放电性而导致产品堵塞，不需要大的压力，生产率优异。 在通过分离含钛化合物的流体中生产二氧化钛超细颗粒的方法中，流体在两个处理表面之间形成为薄膜流体，这两个处理表面被布置成能够彼此接近和分离，至少一个 其相对于另一个旋转，并且二氧化钛超细颗粒在薄膜流体中分离。

公开(公告)号：EP2196194A1

公开(公告)日：2010-06-16

申请号：EP08830200.5

申请日：2008-09-10

申请人： M Technique Co., Ltd.

发明人： ENOMURA, Masakazu

IPC分类号： A61K9/127 ,  A61K9/107 ,  A61K9/50 ,  A61K47/08 ,  A61K47/10 ,  A61K47/12 ,  A61K47/20 ,  A61K47/24 ,  A61K47/26 ,  A61K47/28 ,  A61K47/42 ,  B01F3/08 ,  B01J13/00 ,  B01J13/04

CPC分类号： B01F3/0807 ,  A61K9/107 ,  A61K9/127 ,  A61K9/50 ,  A61K47/08 ,  A61K47/28 ,  A61K47/42 ,  B01F5/221 ,  B01F7/00775 ,  B01F7/00791 ,  B01J13/02

摘要： The present invention provides a production method for obtaining a biologically ingestible material having an intended diameter with low energy as compared with conventional methods, the method includes mixing a fluid to be processed in a dispersed phase containing a pharmacologically active substance and a fluid to be processed in a continuous phase including at least a disperse solvent, while each of the fluids are retained in an independent state, in a thin film fluid formed between two processing surfaces arranged to be opposite to each other to be able to approach to and separate from each other, at least one of which rotates relative to the other, through independent pathways corresponding to the respective phases, whereby the components contained in the fluid to be processed in a dispersed phase are formed into microparticles having a desired diameter.

摘要翻译： 本发明提供了与常规方法相比，获得具有低能量的生物摄取物质的生产方法，该方法包括将待处理流体混合在含有药理活性物质的分散相和待处理流体中 在包括至少一种分散溶剂的连续相中，当每种流体保持独立状态时，在彼此相对布置成能够接近和分离的两个处理表面之间形成的薄膜流体中 另一个，其中至少一个通过对应于各个相的独立通路相对于另一个旋转，由此包含在待分散相中待处理流体中的组分形成具有所需直径的微粒。

公开(公告)号：EP2194087A1

公开(公告)日：2010-06-09

申请号：EP08834495.7

申请日：2008-09-11

申请人： M Technique Co., Ltd.

发明人： ENOMURA,Masakazu

IPC分类号： C08J3/03 ,  C08J3/12

CPC分类号： C08J3/05

摘要： The object of the present invention is to provide a method for producing a resin microparticle aqueous dispersion, which can produce monodisperse resin microparticles, does not cause clogging by a product, does not require a high pressure, and hasahighproductivity. Thus, provided is a method for producing a resin microparticle aqueous dispersion, wherein a fluid having at least one kind of resin dissolved in a solvent with which a resin is soluble and compatible and a fluid of an aqueous solvent join together in a thin film fluid formed between processing surfaces arranged opposite so as to be able to approach to and separate from each other, at least one of which rotates relative to the other, whereby resin microparticles are obtained in the thin film fluid by way of separation/emulsification.

摘要翻译： 本发明的目的是提供一种用于制造树脂微粒分散液wässrige，能产生单分散的树脂微粒，不会引起由产品堵塞的方法，并不需要很高的压力，和hasahighproductivity。 因此，提供了一种生产树脂微粒wässrige分散体，worin具有至少一种在溶剂中溶解的树脂与树脂为溶解性及相容的和含水的流体溶剂中，在薄膜流体合流流体的方法 相反，如以能够接近和从海誓山盟分开，其中至少一个的旋转相对于另一个，由此树脂微粒在该薄膜流体中通过分离/乳化的方式获得排列处理用面之间形成的。