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    Hypofluorites and bis-hypofluorites, and process for preparing same
    1.
    发明公开
    Hypofluorites and bis-hypofluorites, and process for preparing same 失效
    次氟酸盐和双次氟酸盐及其制备方法

    公开(公告)号：EP0259817A3

    公开(公告)日：1988-05-04

    申请号：EP87113058

    申请日：1987-09-07

    申请人： AUSIMONT S.p.A.

    发明人： Marraccini, Antonio, Dr. ,  Guglielmo, Giorgio, Dr. ,  Malacrida, Alessandro, Dr. ,  Roberti, Lamberto

    IPC分类号： C07C71/00 ,  C07C143/70

    CPC分类号： C07C71/00 ,  C07C309/00

    摘要： Mono- and bis-hypofluorites respectively of formula: FO₂S-R f -CF₂OF and FOCF₂-Rʹ f -CF₂OF wherein R f is perfluoroalkylene or perfluorochloroalkylene and Rʹ f is perfluoroalkylene or perfluorooxyalkylene are prepared by a process which is conducted continuously, at a temperature from 0 to 60°C and comprises starting from the respective acyl fluorides
    by reaction of fluorine in the gas phase in the presence of a catalyst consisting of K, Rb, Cs or Ba fluorine, preferably supported on a metal material.

    摘要翻译： 分别为式FO 2 S-R f-CF 2 OF和FOCF 2 -R f-CF 2 OF的单 - 和双 - 次氟酸，其中R f为全氟亚烷基或全氟亚氯代亚烷基，R'f为全氟亚烷基或全氟氧亚烷基通过连续进行的方法制备， 包括从各自的酰基氟化物开始，通过氟在气相中在由K，Rb，Cs或Ba氟组成的催化剂存在下反应，所述催化剂优选负载在金属材料上。

    Process for preparing methacrylates of fluorinated alcohols
    5.
    发明公开
    Process for preparing methacrylates of fluorinated alcohols 失效
    Verfahren zur Herstellung der Methacrylate von fluorierten Alkoholen。

    公开(公告)号：EP0394927A2

    公开(公告)日：1990-10-31

    申请号：EP90107669.5

    申请日：1990-04-23

    申请人： AUSIMONT S.p.A.

    发明人： Gregorio, Guglielmo, Dr. ,  Roberti, Lamberto ,  Strepparola, Ezio, Dr.

    IPC分类号： C07C69/653 ,  C07C67/08

    CPC分类号： C07C67/08 ,  C07C69/653

    摘要： The present invention relates to a process for preparing methacrylates of fluorinated alcohols, which comprises reacting said alcohols with an excess of methacrylic acid in the presence of phosphoric anhydride which acts as catalyst and absorbs the water formed. The process may be applied to primary, secondary and tertiary fluorinated alcohols and to alcohols and diols with perfluoroether chains.

    摘要翻译： 本发明涉及一种制备氟化醇的甲基丙烯酸酯的方法，该方法包括在作为催化剂并吸收形成的水的磷酸酐存在下使所述醇与过量的甲基丙烯酸反应。 该方法可以应用于一级，二级和三级氟化醇和具有全氟醚链的醇和二醇。

    Process for preparing Hypofluorites and bis-hypofluorites
    6.
    发明公开
    Process for preparing Hypofluorites and bis-hypofluorites 失效
    制备次氟酸盐和双次氟酸盐的方法

    公开(公告)号：EP0259817A2

    公开(公告)日：1988-03-16

    申请号：EP87113058.9

    申请日：1987-09-07

    申请人： AUSIMONT S.p.A.

    发明人： Marraccini, Antonio, Dr. ,  Guglielmo, Giorgio, Dr. ,  Malacrida, Alessandro, Dr. ,  Roberti, Lamberto

    IPC分类号： C07C71/00 ,  C07C309/80 ,  B01J27/12

    CPC分类号： C07C71/00 ,  C07C309/00

    摘要： Mono- and bis-hypofluorites respectively of formula: FO₂S-R f -CF₂OF and FOCF₂-Rʹ f -CF₂OF wherein R f is perfluoroalkylene or perfluorochloroalkylene and Rʹ f is perfluoroalkylene or perfluorooxyalkylene are prepared by a process which is conducted continuously, at a temperature from 0 to 60°C and comprises starting from the respective acyl fluorides
    by reaction of fluorine in the gas phase in the presence of a catalyst consisting of K, Rb, Cs or Ba fluorine, preferably supported on a metal material.

    摘要翻译： 分别为式FO 2 S-R f-CF 2 OF和FOCF 2 -R f-CF 2 OF的单 - 和双 - 次氟酸，其中R f为全氟亚烷基或全氟亚氯代亚烷基，R'f为全氟亚烷基或全氟氧亚烷基通过连续进行的方法制备， 包括从各自的酰基氟化物开始，通过氟在气相中在由K，Rb，Cs或Ba氟组成的催化剂存在下反应，所述催化剂优选负载在金属材料上。