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    VERFAHREN ZUR HERSTELLUNG VON PYRROLIDIN
    2.
    发明公开
    VERFAHREN ZUR HERSTELLUNG VON PYRROLIDIN 有权
    用于生产甲基吡咯烷

    公开(公告)号：EP2872494A1

    公开(公告)日：2015-05-20

    申请号：EP13734413.1

    申请日：2013-07-05

    Applicant: BASF SE

    Inventor： BOU CHEDID, Roland ,  MELDER, Johann-Peter ,  DOSTALEK, Roman ,  PASTRE, Jörg ,  TAN, Aik Meam

    IPC: C07D295/023

    CPC classification number: C07D295/023

    Abstract: Disclosed is a method for producing pyrollidine of formula (I) by reacting 1.4-butandiol (BDO) of formula (II) with ammoniac in the presence of hydrogen and a supported, metal-containing catalyser, characterised in that, prior to its reduction with hydrogen, the catalytically active mass of the catalyser contains oxygen-containing compounds of aluminium, copper, nickel and cobalt and oxygen-containing compounds of tin in the wt.% range of 0.2 to 5.0%, calculated as SnO, and in that the reaction is performed in the liquid phase at an absolute pressure in the range of 160 to 220 bar, at a temperature in the range of 160 to 230
    o C, using ammoniac at a molar ratio to the used BDO of 5 to 50 and in the presence of 1.0 to 4.5 wt.% hydrogen relative to the quantity of BDO used.

    3,5-DIETHYL-2-PROPYL-TETRAHYDROPYRAN AND STEREOISOMERS THEREOF FOR USE AS AROMA CHEMICALS
    3.
    发明公开
    3,5-DIETHYL-2-PROPYL-TETRAHYDROPYRAN AND STEREOISOMERS THEREOF FOR USE AS AROMA CHEMICALS 审中-公开

    公开(公告)号：EP3466938A1

    公开(公告)日：2019-04-10

    申请号：EP17194908.4

    申请日：2017-10-05

    Applicant: BASF SE

    Inventor： MARION, Nicolas ,  PINKOS, Rolf ,  RUEDENAUER, Stefan ,  GARLICHS, Florian ,  PELZER, Ralf ,  DOSTALEK, Roman ,  PFEFFINGER, Joachim ,  VINCKIER, Anja

    IPC: C07D309/04

    Abstract: The present invention relates to 3,5-diethyl-2-propyl-tetrahydropyran of formula (I)

    and its stereoisomers and mixtures thereof, to a method for preparing 3,5-diethyl-2-propyl-tetrahydropyran or a stereoisomer thereof or a mixture of stereoisomers thereof, to the composition obtainable by this method, to the use of 3,5-diethyl-2-propyl-tetrahydropyran or of a stereoisomer or of a mixture of stereoisomers thereof or of said composition as an aroma chemical and to the use thereof for modifying the scent character of a fragranced composition, to an aroma chemical containing 3,5-diethyl-2-propyl-tetrahydropyran or a stereoisomer or a mixture of stereoisomers thereof or said composition, and to a method of preparing a fragranced composition or for modifying the scent character of a fragranced composition.

    VERFAHREN ZUR HERSTELLUNG EINES MONO-N-ALKYL-PIPERAZINS
    5.
    发明公开
    VERFAHREN ZUR HERSTELLUNG EINES MONO-N-ALKYL-PIPERAZINS 有权
    VERFAHREN ZUR HERSTELLUNG EINES单-N-烷基哌嗪

    公开(公告)号：EP2855443A1

    公开(公告)日：2015-04-08

    申请号：EP13726752.2

    申请日：2013-05-29

    Applicant: BASF SE

    Inventor： BOU CHEDID, Roland ,  MELDER, Johann-Peter ,  ABEL, Ulrich ,  DOSTALEK, Roman ,  STEIN, Bernd

    IPC: C07D295/088

    CPC classification number: C07D295/088 ,  B01J23/83 ,  B01J35/023 ,  B01J37/0009 ,  B01J37/031 ,  B01J37/08 ,  B01J37/18 ,  B01J2523/00 ,  C07D295/03 ,  B01J2523/17 ,  B01J2523/31 ,  B01J2523/3706

    Abstract: The invention relates to a method for producing a mono-N-alkyl piperazine of formula (I), where R1 represents C1 - C5 alkyl or 2-(2-hydroxy-ethoxy) ethyl, by reacting diethanolamine (DEOA) of formula (II) with a primary amine of formula H
    2 N-R
    1 (III) in the presence of hydrogen and a catalyst moulded body. The reaction is carried out in the liquid phase at an absolute pressure ranging from 150 to 250 bar and the amination is carried out using a catalyst moulded body, the precursor of which can be produced according to a method in which (i) an oxidic material comprising copper oxide, aluminium oxide and lanthanum oxide is provided, (ii) powdered metallic copper and/or copper flakes and optionally graphite are added to the oxidic material, (iii) the mixture resulting from step (ii) is moulded into a moulded body. The oxidic material can be obtained by the simultaneous or successive precipitation of the components copper oxide, aluminium oxide and lanthanum oxide and by subsequent drying and calcination and the catalyst moulded body is calcined once again after the moulding process in step (iii).

    Abstract translation: 本发明涉及制备式（I）的单-N-烷基哌嗪的方法，其中R 1表示C 1 -C 5烷基或2-（2-羟基 - 乙氧基）乙基，通过使式（II）的二乙醇胺 ）与式H 2 N-R 1（III）的伯胺在氢和催化剂成型体的存在下反应来制备。 反应在150-250巴的绝对压力下在液相中进行，并且使用催化剂成型体进行胺化，其前体可以根据以下方法制备：（i）氧化物质 其包含氧化铜，氧化铝和氧化镧，（ii）将粉末状金属铜和/或铜片和任选的石墨加入氧化材料中，（iii）将由步骤（ii）得到的混合物模塑成模制体 。 氧化材料可以通过同时或连续沉淀氧化铜，氧化铝和氧化镧组分并随后干燥和煅烧而获得，并且在步骤（iii）中的模制过程之后将催化剂成型体再次煅烧。

    VERFAHREN ZUR HERSTELLUNG EINES MONO-N-ALKYL-PIPERAZINS
    6.
    发明公开
    VERFAHREN ZUR HERSTELLUNG EINES MONO-N-ALKYL-PIPERAZINS 有权
    VERFAHREN ZUR HERSTELLUNG EINES单-N-烷基哌嗪

    公开(公告)号：EP2855442A1

    公开(公告)日：2015-04-08

    申请号：EP13724592.4

    申请日：2013-05-23

    Applicant: BASF SE

    Inventor： BOU CHEDID, Roland ,  MELDER, Johann-Peter ,  ABEL, Ulrich ,  DOSTALEK, Roman ,  STEIN, Bernd

    IPC: C07D295/088

    CPC classification number: C07D295/088 ,  C07D295/023 ,  C07D295/03

    Abstract: The invention relates to a method for producing a mono-N-alkyl piperazine of formula (I), where R
    1 represents C
    1 to C
    5 alkyl or 2-(2-hydroxy-ethoxy) ethyl, by reacting diethanolamine (DEOA) of formula (II) with a primary amine of formula H
    2 N-R
    1 (III) in the presence of hydrogen and a supported catalyst containing metal. The catalytically active mass of the catalyst, before reduction of the latter using hydrogen, contains oxygenic compounds of aluminum, copper, nickel and cobalt and between 0.2 and 5.0 wt. % oxygenic compounds of tin, calculated as SnO, and the reaction is carried out in the liquid phase at an absolute pressure ranging from 95 to 145 bar.

    Abstract translation: 本发明涉及制备式（I）的单-N-烷基哌嗪的方法，其中R 1表示C 1至C 5烷基或2-（2-羟基 - 乙氧基）乙基，通过使二乙醇胺（DEOA）与 （II）与式H 2 N-R 1（III）的伯胺在氢气和含金属的负载型催化剂存在下反应。 在使用氢气还原后，催化剂的催化活性物质包含铝，铜，镍和钴的含氧化合物以及0.2-5.0wt。 以SnO计算的锡的％氧化合物，并且反应在95至145bar的绝对压力下在液相中进行。

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