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    KONTINUIERLICHES VERFAHREN UND REAKTOR ZUR HYDRIERUNG ORGANISCHER VERBINDUNGEN
    1.
    发明公开
    KONTINUIERLICHES VERFAHREN UND REAKTOR ZUR HYDRIERUNG ORGANISCHER VERBINDUNGEN 有权
    VERFAHREN ZUR HYDRIERUNG有机化学家VERBINDUNGEN

    公开(公告)号：EP2285481A1

    公开(公告)日：2011-02-23

    申请号：EP09765703.5

    申请日：2009-05-20

    Applicant: BASF SE

    Inventor： PFEFFINGER, Joachim

    IPC: B01J8/04 ,  B01J8/22 ,  B01J19/24

    CPC classification number: B01J4/002 ,  B01J8/025 ,  B01J8/226 ,  B01J8/228 ,  B01J19/246 ,  B01J19/2465 ,  B01J19/30 ,  B01J19/32 ,  B01J2219/00777 ,  C07C29/147 ,  C07C29/19 ,  C07C209/72 ,  C07C2601/14 ,  C07C211/36

    Abstract: The present invention relates to a continuous method for hydrogenating organic compounds in a multiphase system in the presence of a homogeneous or heterogeneous catalyst, characterized in that the method is carried out in two stages, wherein the first stage is carried out in a loop reactor having an external heat exchanger and the second stage is carried out in a bubble column reactor having restricted backmixing. In addition, the present invention relates to a hydrogenation reactor (1) in a high-columnar shape having a concentric guide tube (2) arranged in the lower reactor region and an upwards-directed mixing nozzle (3) via which the starting materials and reaction mixture can be fed, a pump (4) and also a heat exchanger (5) which are situated in an external pump circuit which leads from the reactor to the mixing pump and having one or more gas- and liquid-permeable internals (10) which are mounted in the upper region of the reactor, wherein the ratio of the total length to diameter of the hydrogenation reactor (1) is in the range from 5:1 to 100:1 and the ratio of the volume of the upper region of the reactor to the volume of the lower region of the reactor is 0.05:1 to 10:1.

    Abstract translation: 本发明涉及一种用于在均相或非均相催化剂存在下在多相体系中氢化有机化合物的连续方法，其包括在两个阶段中进行该过程，第一阶段在具有外部热交换器的环管反应器中进行， 泡沫塔式反应器的第二阶段有限的回混。 本发明还涉及一种具有高圆柱形设计的氢化反应器（1），其包括布置在下部反应区域中的同心引导管（2）和向上的混合喷嘴（3），通过该混合喷嘴可以提供反应物和反应混合物 ，存在于从反应器引导到混合泵的外部泵循环系统中的泵（4）和热交换器（5），以及一个或多个气体和液体可渗透内部件（10），其安装在 反应器的上部区域，其中氢化反应器（1）的总长度与直径的比率在5:1至100:1的范围内，反应器的上部区域的体积与体积的比例 的反应器的下部区域为0.05:1至10:1。

    3,5-DIETHYL-2-PROPYL-TETRAHYDROPYRAN AND STEREOISOMERS THEREOF FOR USE AS AROMA CHEMICALS
    3.
    发明公开
    3,5-DIETHYL-2-PROPYL-TETRAHYDROPYRAN AND STEREOISOMERS THEREOF FOR USE AS AROMA CHEMICALS 审中-公开

    公开(公告)号：EP3466938A1

    公开(公告)日：2019-04-10

    申请号：EP17194908.4

    申请日：2017-10-05

    Applicant: BASF SE

    Inventor： MARION, Nicolas ,  PINKOS, Rolf ,  RUEDENAUER, Stefan ,  GARLICHS, Florian ,  PELZER, Ralf ,  DOSTALEK, Roman ,  PFEFFINGER, Joachim ,  VINCKIER, Anja

    IPC: C07D309/04

    Abstract: The present invention relates to 3,5-diethyl-2-propyl-tetrahydropyran of formula (I)

    and its stereoisomers and mixtures thereof, to a method for preparing 3,5-diethyl-2-propyl-tetrahydropyran or a stereoisomer thereof or a mixture of stereoisomers thereof, to the composition obtainable by this method, to the use of 3,5-diethyl-2-propyl-tetrahydropyran or of a stereoisomer or of a mixture of stereoisomers thereof or of said composition as an aroma chemical and to the use thereof for modifying the scent character of a fragranced composition, to an aroma chemical containing 3,5-diethyl-2-propyl-tetrahydropyran or a stereoisomer or a mixture of stereoisomers thereof or said composition, and to a method of preparing a fragranced composition or for modifying the scent character of a fragranced composition.

    VERFAHREN ZUR FÖRDERUNG VON FLÜSSIGKEITEN
    10.
    发明公开
    VERFAHREN ZUR FÖRDERUNG VON FLÜSSIGKEITEN 有权
    程序对于液体促进

    公开(公告)号：EP2452071A1

    公开(公告)日：2012-05-16

    申请号：EP10728254.3

    申请日：2010-07-06

    Applicant: BASF SE

    Inventor： PFEFFINGER, Joachim ,  GILCHER, Willi ,  MORELL, Jürgen

    IPC: F04B15/04 ,  F04B39/00 ,  F04B43/02 ,  F04B53/14 ,  F04F1/02 ,  F04F1/14 ,  F04F1/18

    CPC classification number: F04B53/141 ,  F04B15/04 ,  F04B39/0011 ,  F04B43/02 ,  F04F1/02 ,  F04F1/14 ,  F04F1/18 ,  Y10T137/0318 ,  Y10T436/2575

    Abstract: The present invention relates to a method for continuously delivering a fluid used as a feedstock in a chemical reaction by means of a positive displacement pump comprising spatially separated delivery valves and a fluid-filled transfer line between the positive displacement pump and delivery valves, characterized in that an auxiliary fluid, which is a product or a reactant of the chemical reaction and has a melting point that is below the melting point or below the saturation temperature of the fluid to be delivered, is present in the transfer line. The present invention further relates to the use of a product of an aromatic compound resulting from hydrogenation as an auxiliary fluid for delivering an aromatic compound, and to the use of an alcohol or an ester of alcohol and carboxylic acid as an auxiliary fluid for delivering carboxylic acids or carboxylic acid derivatives.

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