Abstract:
The invention relates to a method for the production of melamine by reaction of urea in the presence of a solid catalyst in one or more serial reactors in the temperature range 370 °C to 430 °C, cooling and filtering the gases produced in the urea reaction, separation of the melamine by desublimation and recycling a part of the gases produced after separation of the melamine ('recycle gas') into the reactor or reactors, characterised in that all given steps are carried out at a pressure in the range 4 bar to 10 bar.
Abstract:
The invention relates to a method for producing a turbine wheel for an exhaust gas turbocharger by means of metal injection molding, comprising the following steps: (a) providing a feedstock containing a metal powder and a binder material, (b) providing a tool, which comprises a negative mold of the turbine wheel to be produced, for metal injection molding of the turbine wheel, (c) introducing a rotationally symmetrical core composed of the binder material into the negative mold of the tool provided in method step (b) and orienting the core so that the core is oriented symmetrically to the rotational axis of the turbine wheel to be produced, (d) producing a green body by means of metal injection molding of the feedstock provided in method step (a) around the core, (e) performing a binder removal step to remove the binder from the green body to obtain a molded body in the form of the turbine wheel, and (f) sintering the molded body.
Abstract:
Disclosed are a catalyst precursor or catalyst and a method for the production thereof. According to said method, a) a suspension is produced which contains a vanadium, phosphorus, and oxygen-containing precursor (VPO precursor), the ultrasonically dispersed particles of which have an average diameter d50, primary particles of less than 1.3 µm in an aqueous solution and which are provided in the form of agglomerates having an average diameter d50, agglomerates of 2 to 20 µm in water, the average diameters of the primary particles and the agglomerates of the VPO precursor being determined by means of laser diffraction according to ISO 13320, b) the suspension is spray dried, and c) if necessary, the catalyst precursor obtained in step b) is transformed into the catalyst by means of a thermal treatment. Also disclosed is the use of said catalyst for gas phase oxidation of hydrocarbons.
Abstract:
Es wird ein Verfahren zur Abtrennung von C 5 -C 8 -Kohlenwasserstoffen und Sauergasen aus einem Fluidstrom beschrieben, bei dem man a) den Fluidstrom in einer Absorptionszone mit einem Absorptionsmittel in Kontakt bringt, das mindestens ein Amin enthält, wobei man einen entsäuerten Fluidstrom und ein mit Sauergasen beladenes Absorptionsmittel erhält, b) das beladene Absorptionsmittel in einem ersten Wärmetauscher erwärmt und in eine Dekompressionszone auf einen Druck von 5 bis 10 bar entspannt, wobei man eine C 5 -C 8 -Kohlenwasserstoffe enthaltende Gasphase und ein Kohlenwasserstoff-abgereichertes beladenes Absorptionsmittel erhält, c) das Kohlenwasserstoff-abgereicherte beladene Absorptionsmittel in einem optionalen zweiten Wärmetauscher erwärmt und in einen Stripper leitet, in dem die Sauergase bei einem Druck von 1 bis 2,5 bar durch Zufuhr von Wärme zumindest teilweise freigesetzt werden, wobei man ein regeneriertes Absorptionsmittel und einen Sauergas enthaltenden Strom erhält, und d) das regenerierte Absorptionsmittel in die Absorptionszone zurückführt, wobei man als Heizmedium im zweiten Wärmetauscher das regenerierte Absorptionsmittel verwendet und als Heizmedium im ersten Wärmetauscher das regenerierte Absorptionsmittel nach dem Passieren des zweiten Wärmetauschers verwendet, und die im ersten Wärmetauscher und im zweiten Wärmetauscher übertragenen relativen Wärmemengen so gewichtet, dass die C 5 -C 8 -Kohlenwasserstoffe enthaltende Gasphase 50 bis 97 Vol.-% Sauergase enthält.
Abstract:
The invention relates to a method for the continuous thermal debinding of a metal and/or ceramic molded body produced by injection molding, extruding or pressing using a thermoplastic compound, as a binding agent comprising at least one polyoxymethylene homopolymer or copolymer, and in a debinding furnace comprising the following steps: (a) debinding the molded body in a debinding oven at a temperature that is 5 to 20ºC, preferably 10 to 15ºC, below the temperature of a second temperature stage, over a period of 4 to 12 hours in a first temperature stage in an oxygen-containing atmosphere, (b) debinding the molded body at a temperature in the range of > 160 to 200ºC over a period of 4 to 12 hours in an oxygen-containing atmosphere in a second temperature stage, and (c) debinding the molded body at a temperature in the range of 200 to 600ºC over a period of 2 to 8 hours in a third temperature stage in an oxygen-containing, or in a neutral or reducing, atmosphere, wherein the molded body is transported through the debinding oven during steps (a) and (b).
Abstract:
The invention relates to a method for producing melamine by the decomposition of urea using a catalyst, said catalyst containing a) 10 - 90% by weight of a zeolite, b) 10 - 90% by weight of a matrix containing silicon dioxide, aluminum oxide, silicon-aluminum oxides and/or clay minerals, and c) 0 - 10% by weight of additives, and the total nickel and vanadium content in the catalyst being less than 500 ppm.