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    VERFAHREN ZUR HERSTELLUNG VON TRI-N-PROPYLAMIN (TPA)
    2.
    发明公开
    VERFAHREN ZUR HERSTELLUNG VON TRI-N-PROPYLAMIN (TPA) 有权
    用于生产三正丙胺（TPA）

    公开(公告)号：EP2588442A1

    公开(公告)日：2013-05-08

    申请号：EP11730932.8

    申请日：2011-06-28

    Applicant: BASF SE

    Inventor： HUYGHE, Kevin ,  BRUGHMANS, Steven ,  SIMON, Falk ,  MELDER, Johann-Peter ,  RAATZ, Peter

    IPC: C07C209/64 ,  C07C211/06

    CPC classification number: C07C209/64 ,  B01J23/72 ,  B01J23/755 ,  C07C209/16 ,  C07C211/06

    Abstract: The invention relates to a method for producing tri-n-propyl amine (TPA), wherein di-n-propyl amine is reacted in the presence of hydrogen and a copper-containing heterogeneous catalyst. The integrated method for producing TPA comprises the following operations: I) reacting n-propanol with ammonia in a reactor in the presence of an amination catalyst and optionally hydrogen to form a mixture of mono-n-propyl amine, DPA and TPA, II) separating unreacted ammonia, unreacted n-propanol and optionally hydrogen from the reaction product and returning at least the ammonia and propanol into the reactor in I); and separating the n-propyl amine mixture by distillation and separating the TPAs, III) reacting the DPAs resulting from the separation by distillation in II) in a reactor in the presence of hydrogen and a copper-containing heterogeneous catalyst to form TPA, and IV) feeding the reaction product from III) into the operation II).

    VERFAHREN ZUR HERSTELLUNG VON PROPEN AUS PROPAN
    6.
    发明公开
    VERFAHREN ZUR HERSTELLUNG VON PROPEN AUS PROPAN 审中-公开

    公开(公告)号：EP2010470A2

    公开(公告)日：2009-01-07

    申请号：EP07726856.3

    申请日：2007-03-13

    Applicant: BASF SE

    Inventor： SCHUBERT, Markus ,  MÜLLER, Ulrich ,  KIENER, Christoph ,  TEICH, Friedhelm ,  CRONE, Sven ,  SIMON, Falk ,  PASTRE, Jörg

    IPC: C07C7/12 ,  C07C7/13

    CPC classification number: C07C5/333 ,  C07C7/12 ,  C07C7/13 ,  C07C11/06

    Abstract: The invention relates to a method for producing propene from propane. Said method comprises the following steps: A) a feed gas stream (a) containing propane is prepared; B) the feed gas stream (a) containing propane, is introduced with optionally water vapour and optionally, an oxygen-containing gas stream into a dehydrogenation zone and then the propane is dehydrogenated to form propene, and a product gas stream (b) containing propane, propene, methane, ethane, ethene, hydrogen, optionally carbon monoxide, carbon dioxide, water vapour and oxygen, is obtained; C) the product gas stream (b) is cooled, optionally compressed and then water vapour is separated by condensation and a product gas stream (c) depleted in water vapour is obtained; D) the product gas stream (c) is brought into contact with a selectively active adsorber which selectively adsorbs propene in the selected adsorption conditions, and an adsorber charged with propene and a gas stream (d2) depleted in propene and containing propane, methane, ethane, ethene and hydrogen, carbon monoxide and carbon dioxide are obtained; E) a gas stream (e1) containing propene is released from the adsorber charged with propene by reducing the pressure and/or heat of the adsorber.

    Abstract translation: 本发明涉及一种由丙烷生产丙烯的方法。 所述方法包括以下步骤：A）制备含有丙烷的进料气流（a）; B）将含有丙烷的进料气流（a）与任选的水蒸气和任选的含氧气流一起引入脱氢区，然后将丙烷脱氢以形成丙烯，并且产物气流（b）含有 丙烷，丙烯，甲烷，乙烷，乙烯，氢气，任选的一氧化碳，二氧化碳，水蒸气和氧气; C）冷却产物气流（b），任选压缩，然后通过冷凝分离水蒸气，并获得贫含水蒸气的产物气流（c）; D）使产物气流（c）与在选择的吸附条件下选择性吸附丙烯的选择性吸附剂接触，以及装载丙烯和贫丙烯气体流（d2）并含有丙烷，甲烷， 乙烷，乙烯和氢气，得到一氧化碳和二氧化碳; E）通过降低吸附器的压力和/或热量，从装有丙烯的吸附器释放含有丙烯的气流（e1）。

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