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    A PROCESS FOR PREPARING PROPYLENE OXIDE
    2.
    发明公开
    A PROCESS FOR PREPARING PROPYLENE OXIDE 审中-公开
    VERFAHREN ZUR HERSTELLUNG VON PROPYLENOXID

    公开(公告)号：EP3024579A1

    公开(公告)日：2016-06-01

    申请号：EP14739188.2

    申请日：2014-07-16

    申请人： BASF SE ,  Dow Global Technologies LLC

    发明人： TELES, Joaquim Henrique ,  SEELIG, Bianca ,  RIEDEL, Dominic ,  KAMPE, Philip ,  URBANCZYK, Daniel ,  WEBER, Markus ,  MÜLLER, Ulrich ,  PARVULESCU, Andrei-Nicolae ,  GUMLICH, Kai ,  BASSLER, Peter ,  BARTOSCH, Christian ,  JACUBINAS, Richard ,  WEIDENBACH, Meinolf ,  WITZL, Werner

    IPC分类号： B01J29/89 ,  B01J37/02 ,  C07D301/12 ,  B01J27/16

    CPC分类号： C07D301/12 ,  B01J27/18 ,  B01J27/188 ,  B01J29/7038 ,  B01J29/7088 ,  B01J35/002 ,  B01J35/1019 ,  B01J2229/186 ,  Y02P20/52

    摘要： A continuous process for the preparation of propylene oxide, comprising (i) providing a liquid feed stream comprising propene, hydrogen peroxide, acetonitrile, water, optionally propane, and at least one dissolved potassium salt of a phosphorus oxyacid wherein the molar ratio of potassium relative to phosphorus in the at least one potassium salt of a phosphorus oxyacid is in the range of from 0.6 to 1.4; (ii) passing the liquid feed stream provided in (i) into an epoxidation reactor comprising a catalyst comprising a titanium zeolite of structure type MWW comprising zinc, and subjecting the liquid feed stream to epoxidation reaction conditions in the epoxidation reactor, obtaining a reaction mixture comprising propylene oxide, acetonitrile, water, the at least one dissolved potassium salt of a phosphorus oxyacid, optionally propene, and optionally propane; (iii) removing an effluent stream from the epoxidation reactor, the effluent stream comprising propylene oxide, acetonitrile, water, at least a portion of the at least one dissolved potassium salt of a phosphorus oxyacid, optionally propene, and optionally propane.

    摘要翻译： 一种用于制备环氧丙烷的连续方法，包括（i）提供包含丙烯，过氧化氢，乙腈，水，任选的丙烷和至少一种溶解的含磷酸的钾盐的液体进料流，其中钾相对的摩尔比 至少一种含磷酸的钾盐中的磷在0.6至1.4的范围内; （ii）将（i）中提供的液体进料流送入包含催化剂的环氧化反应器中，所述催化剂包括含锌的结构型MVVW的钛沸石，并使该液体进料流在环氧化反应器中进行环氧化反应条件，得到反应混合物 包括环氧丙烷，乙腈，水，至少一种溶解的含磷酸的钾盐，任选的丙烯，以及任选的丙烷; （iii）从环氧化反应器中除去流出物流，流出物流包含环氧丙烷，乙腈，水，至少一部分溶解的磷酸钾盐，任选的丙烯和任选的丙烷。

    VERFAHREN ZUR HERSTELLUNG VON GLYCIDYLESTERN
    6.
    发明公开
    VERFAHREN ZUR HERSTELLUNG VON GLYCIDYLESTERN 有权

    公开(公告)号：EP2297126A1

    公开(公告)日：2011-03-23

    申请号：EP09765774.6

    申请日：2009-06-10

    申请人： BASF SE

    发明人： GUMLICH, Kai ,  TELES, Joaquim Henrique ,  MERTEN, Roland

    IPC分类号： C07D303/16

    CPC分类号： C07D303/16

    摘要： Method for producing glycidyl esters, characterized in that carbonate esters of the formula I are converted to glycidyl esters of the formula II in the presence of a homogeneous catalyst with the cleaving of carbon dioxide, where R in the above formulas stands for an organic radical with 1 to 20 C atoms.

    摘要翻译： 制备缩水甘油酯的方法，其特征在于式I的碳酸酯在均相催化剂存在下与二氧化碳裂解转化为式II的缩水甘油酯，其中上式中的R代表有机基团，其中 1至20个C原子。