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1.发明公开
公开(公告)号：EP0755375A1
公开(公告)日：1997-01-29
申请号：EP95915609.0
申请日：1995-04-07
CPC分类号： C07C231/02 , Y02P20/582
摘要： This invention relates to a process for preparing amido-carboxylic acids in water. The process involves four steps. Step (A) involves hydrolyzing a lactam at a temperature of 150 °C - 300 °C to form a mixture containing an amino acid. Step (B) involves cooling the reaction mixture formed in step (A) to a temperature of 25 °C - 100 °C. Step (C) involves reacting a carboxylic acid anhydride with the amino acid formed in step (A) to form a reaction mixture containing an organic layer which contains an amido-carboxylic acid and an aqueous layer. Step (D) involves separating the amido-carboxylic acid containing organic layer from the aqueous layer. The presence of water aids in product isolation by phase separation and recycle of the reactants. Amido-carboxylic acids are used to make bleach activators for detergents.
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公开(公告)号：EP0755376B1
公开(公告)日：2004-07-14
申请号：EP95916254.6
申请日：1995-04-07
IPC分类号： C07C231/08
CPC分类号： C07C231/08 , C07C231/02 , Y02P20/582
摘要： This invention relates to a process for preparing amido-carboxylic acids in water wherein hydrolysis and amidation reactions are conducted simultaneously in a single vessel. The process involves three steps. The first step involves heating at a temperature of 150 DEG C-300 DEG C for 2 to 10 hours, a mixture containing water, a nitrogen containing compound selected from the group consisting of a lactam and an amino acid, and a carboxylic acid or ester. The second step involves cooling the reaction mixture to obtain a two-phase system containing an aqueous layer and an organic layer. The third step involves separating the amido-carboxylic acid containing organic layer from the aqueous layer. The presence of water aids in product isolation by phase separation and recycle of the reactants. Amido-carboxylic acids are used to make bleach activators for detergents.
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3.发明授权AQUEOUS PROCESS FOR PREPARING AMIDO-CARBOXYLIC ACIDS BY REACTING AN AMINO ACID WITH A CARBOXYLIC ACID ANHYDRIDE 失效含水工艺用于生产酰胺基羧酸BY氨基酸和羧酸的实现
公开(公告)号：EP0755375B1
公开(公告)日：1999-10-13
申请号：EP95915609.2
申请日：1995-04-07
IPC分类号： C07C231/02 , C07C227/22
CPC分类号： C07C231/02 , Y02P20/582
摘要： This invention relates to a process for preparing amido-carboxylic acids in water. The process involves four steps. Step (A) involves hydrolyzing a lactam at a temperature of 150 DEG C - 300 DEG C to form a mixture containing an amino acid. Step (B) involves cooling the reaction mixture formed in step (A) to a temperature of 25 DEG C - 100 DEG C. Step (C) involves reacting a carboxylic acid anhydride with the amino acid formed in step (A) to form a reaction mixture containing an organic layer which contains an amido-carboxylic acid and an aqueous layer. Step (D) involves separating the amido-carboxylic acid containing organic layer from the aqueous layer. The presence of water aids in product isolation by phase separation and recycle of the reactants. Amido-carboxylic acids are used to make bleach activators for detergents.
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4.发明公开
公开(公告)号：EP0790978A1
公开(公告)日：1997-08-27
申请号：EP95938873.0
申请日：1995-10-26
CPC分类号： C08G69/16 , C07C231/02 , C08G69/46
摘要： This invention relates to a process for recycling waste material selected from amino-carboxylic acid oligomers or polymers and amido-carboxylic acid oligomers or polymers into amido-carboxylic acids. A mixture containing water, an oligomeric or polymeric waste material, and a carboxylic acid is heated. The mixture is cooled to obtain a two phase system containing an aqueous phase and an organic phase which are separated. Carboxylic acids, unreacted starting materials, and the monomeric amido-carboxylic acid product are distilled from the organic phase. The remaining solid residue composed of high boiling oligomeric amino-carboxylic acids is recycled into Step (A).
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公开(公告)号：EP0672077A1
公开(公告)日：1995-09-20
申请号：EP94902401.0
申请日：1993-11-24
发明人： GOTT, Samuel, Leroy , CARTER, Thomas, Edward , PETROSKEY, Wade, Timothy , WILLIAMS, Thomas, Hugh , ZIMA, George, Chester
IPC分类号： C08G18
CPC分类号： C08G18/40 , C08G2101/0008 , C08G2101/0016 , C08G2101/0025
摘要： The present invention relates to a process for preparing flexible, semi-flexible or rigid polyurethane foam plastics from a polyfunctional isocyanate and a polyhydric compound. More specifically, the invention involves the substitution of some portion of the hydroxy groups on the polyhydric compound with acetoacetate groups. Such substitution reduces the viscosity of the polyhydric resin without affecting the performance properties of the foams. Various substitution levels can be used depending on the desired level of viscosity reduction.
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6.发明授权PROCESS FOR PREPARING AMIDO-CARBOXYLIC ACID ESTERS HAVING INTERNAL AMIDE LINKAGES 失效制备具有内酰胺键的酰氨基羧酸酯的方法
公开(公告)号：EP0874803B1
公开(公告)日：2000-12-27
申请号：EP96929114.5
申请日：1996-09-04
IPC分类号： C07C231/02 , C07C231/08
CPC分类号： C07C231/08 , C07C231/02
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7.发明授权
公开(公告)号：EP0790978B1
公开(公告)日：1999-04-21
申请号：EP95938873.7
申请日：1995-10-26
IPC分类号： C07C231/02 , C08G69/46 , C07C233/47 , C07C233/51
CPC分类号： C08G69/16 , C07C231/02 , C08G69/46
摘要： This invention relates to a process for recycling waste material selected from amino-carboxylic acid oligomers or polymers and amido-carboxylic acid oligomers or polymers into amido-carboxylic acids. A mixture containing water, an oligomeric or polymeric waste material, and a carboxylic acid is heated. The mixture is cooled to obtain a two phase system containing an aqueous phase and an organic phase which are separated. Carboxylic acids, unreacted starting materials, and the monomeric amido-carboxylic acid product are distilled from the organic phase. The remaining solid residue composed of high boiling oligomeric amino-carboxylic acids is recycled into Step (A).
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8.发明公开
公开(公告)号：EP0755377A1
公开(公告)日：1997-01-29
申请号：EP95916250.0
申请日：1995-04-07
CPC分类号： C07C231/24
摘要： This invention relates to a four step process for purifying amido-carboxylic acids by liquid/liquid extraction from a reaction mixture containing an amido-carboxylic acid. The first step involves distilling impurities from a reaction mixture containing an amido-carboxylic acid to form a distillate residue. The second step involves mixing the distillate residue with a nonpolar hydrocarbon solvent wherein the mixture is maintained above the freezing point of the distillate residue. The third step involves allowing the hydrocarbon solvent and distillate residue to achieve phase separation of an organic phase containing the amido-carboxylic acid and an organic phase containing the nonpolar hydrocarbon solvent. The fourth step involves separating the organic phase containing the nonpolar hydrocarbon solvent from the organic phase containing the amido-carboxylic acid.
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9.发明公开
公开(公告)号：EP1802679A1
公开(公告)日：2007-07-04
申请号：EP05796760.6
申请日：2005-09-15
IPC分类号： C08G63/00 , C08G63/688
CPC分类号： A61Q5/06 , A61K8/85 , C08G63/672 , C08G63/6886 , C08K5/05 , C09J167/025 , C08L67/00
摘要： A branched sulfopolyester mixture useful in adhesive and personal care product formulations. The branched sulfopolyester mixture includes: I) from 65 to 95 weight % of a branched water-dispersible polyester; and II) from 5 to 35 weight % of an alcohol. The branched sulfopolyester mixture is pourable at room temperatures.
摘要翻译： 用于粘合剂和个人护理产品配方的支化磺基聚酯混合物。 支化磺基聚酯混合物包括：I）65-95重量％的支化水分散性聚酯; 和II）5至35重量％的醇。 支化的磺基聚酯混合物在室温下可倾倒。
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10.发明公开PROCESS FOR PREPARING AMIDO-CARBOXYLIC ACID ESTERS HAVING INTERNAL AMIDE LINKAGES 失效制备具有内酰胺键的酰氨基羧酸酯的方法
公开(公告)号：EP0874803A1
公开(公告)日：1998-11-04
申请号：EP96929114.0
申请日：1996-09-04
CPC分类号： C07C231/08 , C07C231/02
摘要： The present invention relates to a one-step process for preparing amido-carboxylic acid esters having the amide nitrogen positioned between two carbonyl carbons by reacting a carboxylic acid or carboxylic acid ester with a monohydric alcohol and either a lactam, amino-carboxylic acid or a polymeric amino-carboxylic acid. In this process, amidation, esterification, alcoholysis, and hydrolysis reactions occur simultaneously.
摘要翻译： 本发明涉及一种通过使羧酸或羧酸酯与一元醇和内酰胺，氨基羧酸或羧酸反应而制备具有位于两个羰基碳之间的酰胺氮的酰胺 - 羧酸酯的一步法 聚合氨基羧酸。 在这个过程中，酰胺化，酯化，醇解和水解反应同时发生。
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