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    PROCESS FOR SEPARATING METHYLCYCLOPENTANONE FROM CYCLOHEXANONE
    5.
    发明公开
    PROCESS FOR SEPARATING METHYLCYCLOPENTANONE FROM CYCLOHEXANONE 有权
    VERFAHREN ZUR TRENNUNG冯甲基环戊烷AUS CYCLOHEXANON

    公开(公告)号：EP2895454A1

    公开(公告)日：2015-07-22

    申请号：EP13766432.2

    申请日：2013-09-06

    申请人： ExxonMobil Chemical Patents Inc.

    发明人： DAVIS, Jason, D. ,  KUECHLER, Keith, H. ,  LATTNER, James, R. ,  BECKER, Christopher, L. ,  HEIDMAN, John, L.

    IPC分类号： C07C45/82 ,  C07C49/395 ,  C07C49/403

    CPC分类号： C07C45/80 ,  B01D3/143 ,  C07C45/28 ,  C07C45/82 ,  C07C2601/08 ,  C07C2601/14 ,  C07D223/10 ,  C07C49/403 ,  C07C49/395

    摘要： In a process for separating methylcyclopentanone from a mixture comprising methylcyclopentanone and cyclohexanone, a feedstock comprising cyclohexanone, methylcyclopentanone, water at a concentration of at least 0.10 wt%, and optionally phenol is fed into a fractionation distillation column, where a lower effluent rich in cyclohexanone and an upper effluent rich in methylcyclopentanone are produced. Due to the inclusion of water at a relatively high concentration in the feedstock, efficient separation of methylcyclopentanone is achieved. In certain particularly desirable embodiments, the lower effluent is substantially free of methylcyclopentanone. The thus produced cyclohexanone may be used to make, e.g., high-purity caprolactam, which, in turn, may be used for fabricating, e.g., high-performance nylon-6 material.

    摘要翻译： 在从甲基环戊酮和环己酮的混合物中分离甲基环戊酮的方法中，将包含环己酮，甲基环戊酮，至少0.10wt％浓度的水和任选的苯酚的原料进料到分馏塔中，其中富含环己酮的较低流出物 并产生富含甲基环戊酮的上部流出物。 由于在原料中含有较高浓度的水，因此可实现甲基环戊酮的有效分离。 在某些特别理想的实施方案中，较低的流出物基本上不含甲基环戊酮。 由此生产的环己酮可用于制备例如高纯度己内酰胺，其又可用于制造例如高性能尼龙-6材料。

    PROCESS FOR PRODUCING PHENOL AND/OR CYCLOHEXANONE FROM CYCLOHEXYLBENZENE
    6.
    发明公开
    PROCESS FOR PRODUCING PHENOL AND/OR CYCLOHEXANONE FROM CYCLOHEXYLBENZENE 审中-公开
    由环己基苯制备苯酚和/或环己酮的方法

    公开(公告)号：EP2895444A1

    公开(公告)日：2015-07-22

    申请号：EP13766442.1

    申请日：2013-09-12

    申请人： ExxonMobil Chemical Patents Inc.

    发明人： KUECHLER, Keith, H. ,  DAKKA, Jihad, M. ,  LATTNER, James, R. ,  BECKER, Christopher, L. ,  MOZELESKI, Edmund, J.

    IPC分类号： C07C1/24 ,  C07C2/74 ,  C07C5/03 ,  C07C13/28 ,  C07C37/08 ,  C07C39/04 ,  C07C45/53 ,  C07C49/403 ,  C07C407/00 ,  C07C409/14

    CPC分类号： C07C45/53 ,  C07C1/24 ,  C07C2/66 ,  C07C2/74 ,  C07C5/03 ,  C07C29/60 ,  C07C29/80 ,  C07C37/08 ,  C07C407/00 ,  C07C2529/70 ,  C07C2601/14 ,  C07C409/14 ,  C07C39/04 ,  C07C49/403 ,  C07C35/21 ,  C07C13/28

    摘要： In a process for producing phenol and/or cyclohexanone, cyclohexylbenzene is contacted with an oxygen-containing gas to produce an oxidation effluent containing cyclohexylbenzene hydroperoxide. At least a portion of the cyclohexylbenzene hydroperoxide is then contacted with a cleavage catalyst to produce a cleavage effluent containing phenol and cyclohexanone and by¬ products including phenylcyclohexanol. The cleavage effluent or a neutralized product thereof also comprises at least one compound comprising an atom not being carbon, hydrogen or oxygen, which is separated from the cleavage effluent and/or the neutralized product thereof to leave a cleavage fraction lean in the compound comprising an atom not being carbon, hydrogen or oxygen and containing at least a portion of the phenylcyclohexanol. At least a portion of the phenylcyclohexanol is then contacted with a dehydration catalyst comprising a molecular sieve of the MCM-22 type to convert at least a portion of the phenylcyclohexanol to phenylcyclohexene.

    摘要翻译： 在生产苯酚和/或环己酮的方法中，环己基苯与含氧气体接触以产生含环己基苯氢过氧化物的氧化流出物。 然后使至少一部分环己基苯氢过氧化物与裂解催化剂接触以产生含有苯酚和环己酮的裂解流出物和包括苯基环己醇的副产物。 裂解流出物或其中和产物还包含至少一种包含不是碳，氢或氧的原子的化合物，其从裂解流出物和/或其中和产物中分离出来，以使裂解馏分贫含在包含 原子不是碳，氢或氧并且含有至少一部分苯基环己醇。 然后使苯基环己醇的至少一部分与包含MCM-22型分子筛的脱水催化剂接触以将至少一部分苯基环己醇转化为苯基环己烯。

    PROCESS FOR PRODUCING PHENOL
    8.
    发明公开
    PROCESS FOR PRODUCING PHENOL 有权
    VERFAHREN ZUR HERSTELLUNG VON PHENOL

    公开(公告)号：EP2401248A2

    公开(公告)日：2012-01-04

    申请号：EP10701605.7

    申请日：2010-01-25

    申请人： ExxonMobil Chemical Patents Inc.

    发明人： WANG, Kun ,  BENITEZ, Francisco, M. ,  LATTNER, James, R. ,  DAKKA, Jihad, M. ,  MOZELESKI, Edmund, J. ,  ZUSHMA, Stephen

    IPC分类号： C07C37/08 ,  C07C407/00 ,  C07C45/53

    CPC分类号： C07C37/08 ,  C07C45/53 ,  C07C407/00 ,  C07C409/08 ,  C07C409/10 ,  C07C409/14 ,  C07C2601/08 ,  C07C2601/14 ,  C07C49/403 ,  C07C49/10 ,  C07C49/395 ,  C07C49/08 ,  C07C39/04

    摘要： Disclosed is a process for producing phenol or a substituted phenol and a co-product comprising the steps of (i) contacting a first stream comprising an alkylaromatic compound with a second stream comprising an oxygen-containing gas in the presence of a first catalyst comprising a cyclic imide under conditions to convert at least a portion of said alkylaromatic compound to an alkylaromatic hydroperoxide, (ii) producing an effluent stream comprising said cyclic imide, said alkylaromatic hydroperoxide, and said alkylaromatic compound wherein said effluent stream has an alkylaromatic hydroperoxide concentration of from 10 to 40 wt%; and (iii) contacting in a second reactor at least a portion of said effluent stream with a second catalyst to convert said alkylaromatic hydroperoxide to a product stream comprising phenol and said co-product.

    摘要翻译： 公开了一种生产苯酚或取代苯酚和副产物的方法，包括以下步骤：（i）在包含含氧气体的第一催化剂的存在下，将包含烷基芳族化合物的第一物流与包含含氧气体的第二物流接触，所述第一催化剂包含 环状酰亚胺在将至少一部分所述烷基芳族化合物转化为烷基芳香族氢过氧化物的条件下，（ii）产生包含所述环状酰亚胺，所述烷基芳族氢过氧化物和所述烷基芳族化合物的流出物流，其中所述流出物流具有烷基芳香族氢过氧化物浓度 10〜40重量％ 和（iii）在第二反应器中将至少一部分所述流出物流与第二催化剂接触，以将所述烷基芳香族氢过氧化物转化成包含苯酚和所述副产物的产物流。